• 제목/요약/키워드: soaking solution

검색결과 282건 처리시간 0.024초

DIS 공정에 의한 Polyethylene Glycol 함침 알로에 베라 겔의 제조 및 특성화 (Preparation and Characterization of PEG-impregnated Aloe Gel through DIS Processing of Aloe vera Leaf Slice)

  • 권혜미;허원;이신영
    • KSBB Journal
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    • 제28권6호
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    • pp.356-365
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    • 2013
  • The novel Aloe gels were prepared with dewatering and impregnation by soaking (DIS) processing of Aloe vera leaf slice at four different temperatures (25, 35, 45 and $55^{\circ}C$), using dehydration solution of 40% (w/v) polyethylene glycol (PEG4000). The PEG-impregnation to Aloe vera leaf slice during DIS was observed depending on immersion temperature, and the PEG-impregnated Aloe vera gel (PEG-i-AVG) obtained was characterized using $^1H$ NMR, FT-IR, GPC, XRD and TGA. The PEG-i-AVG had the higher levels of Aloe bioactives (glucomannan and O-acetyl contents) and better quality indices by $^1H$ NMR and FT-IR spectroscopy than those of native Aloe gel. Also, the obtained Aloe gel maintained the bimodal patterns in higher molecular weight region by GPC indicating no degradation of polysaccharide from native Aloe gel. The result observed by SEM confirmed a surface modification by forming the porous structure, and TGA result exhibited better thermal stability than that of native Aloe gel. XRD result revealed that the crystalline structure in Aloe gel was led by incorporation of PEG. Significant decrease of %insolubility and high enhancement of water solubility index were observed, respectively, and highly ordered conformation such as a helix structure was also indicated by Congo red reaction. We concluded that the modification effect for enhancing function of native Aloe gel was successfully obtained by DIS process using PEG as a dehydrating agent. These results suggested that this DIS process had a high potential for developing a new minimally processed product from Aloe vera leaf.

Effects of opioid and non-opioid antagonists, pH and enzymes on Corchorus olitorius antinociception in mice

  • Zakaria Zainul Amiruddin;Neelendran M;Pubalan S;Sulaiman MR;Fatimah CA
    • Advances in Traditional Medicine
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    • 제6권3호
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    • pp.186-195
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    • 2006
  • The present study was carried out to determine the involvement of opioid and non-opioid receptor and the effect of pH and enzymes on the recently reported antinociceptive activity of aqueous extract of Corchorus olitorius (AECO) leaves using the abdominal constriction test. The extract was prepared by soaking the dried powdered leaves of Corchorus (C.) olitorius in distilled water overnight, and the supernatant obtained was considered as a stock solution with 100% concentration/ strength. The extract, administered subcutaneously in the concentrations/ strength of 10, 50 and 100%, was found to show a significant concentration-independent antinociception. The 50% concentration AECO were further used to study on the above mentioned parameters. The extract exhibited: significant (P < 0.05) decreased in activity when pre-treated (s.c.) against 10 mg/kg naloxonazine, bicuculine (10 mg/kg), phenoxybenzamine (10 mg/kg), 10 mg/kg pindolol, and 5 mg/kg mecamylamme, but not 10 mg/kg naltrindole, 10 mg/kg atropine, respectively; significant (P < 0.05) decreased in activity after pre-treatment against 10% a-amylase, but not 1 % protease or 10% lipase and; significant (P < 0.05) decreased in activity after exposure to alkaline condition (pH between 9 and 13) while maintaining the activity at acidic condition, respectively. The C. olitorius leaves antinociception, which involved, at least in part, activation of $\mu-opioid,\;\alpha-and\;\beta-adrenergic$, and nicotinic receptors, was found to decrease under alkaline condition and in the presence of $\alpha-amylase$.

감장아찌의 성분특성 및 관련 미생물 (Associated Microorganisms and Chemical Composition of Persimmon Pickles)

  • 정동옥;정희종
    • 한국식생활문화학회지
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    • 제10권3호
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    • pp.133-137
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    • 1995
  • 우리나라의 남부지방의 대부분 농가에서 대량 생산되고 있으나 농가소득에는 기여하지 못하고 있는 떫은 감의 손쉬운 가공에 의한 대량 소비를 촉진시키기 위하여 감장아찌의 화학적 품질 특성을 규명하고 감장아찌 제조 및 유통과정에서의 품질과 관련된 미생물을 순수분리하여 동정함으로써 감장아찌의 품질관리에 기여코자 하였다. 제조된 감장아찌 완제품의 수분함량은 80.04%, 당질함량은 13.72%로 원료감과 큰 차이가 없었으나 조회분함량은 염액에 침지한 감장아찌의 특성때문에 원료감보다 훨씬 높은 4.26%였다. 수용성 탄닌함량은 81.04mg%로 635.45mg%인 원료감보다 크게 감소되었고 총 비타민 C는 23.76mg%로 약간 감소되었으며 유리당은 포도당, 과당, 자당의 순으로 함유되었다. 유리아미노산은 총 17종이 함유된 것으로 분석되었고 그 함량은 glutamic acid(24.97mg%), aspartic acid(24.02mg%), leucine(22.33mg%)의 순으로 높았으며 methionine이 2.42mg로 가장 낮았다. 감장아찌 제조와 관련된 미생물로는 세균 4균주와 효모 3균주가 각각 동정되었는데 동정된 Bacillus subtilis, B. cereus, B. pumilus, B. thuringiensis였고 효모는 Candida glabrata, C. guilliermondi and Hansenula였으며 진공포장하여 상품화한 감장아찌 완제품의 유통과정에서 포장의 부풀림과 감장아찌 맛의 변화를 일으키는 원인균은 효모인 Candida glabrata인 것으로 확인되었다.

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염료감응형 태양전지의 착색 특성 개선 연구 (A Study on the Improvement of Coloring in Dye-sensitized Solar Cell)

  • 서현웅;김미정;손민규;이경준;홍지태;김희제
    • 한국신재생에너지학회:학술대회논문집
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    • 한국신재생에너지학회 2007년도 추계학술대회 논문집
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    • pp.297-300
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    • 2007
  • In this study, we have attempted a new method to enhance the coloring of dye on the $TiO_2$ surface in the dye sensitized solar cell. In the conventional coloring process in a dye sensitized solar cells, dye is absorbed by the covalent bond between TiO2 and dye molecule while the photo-electrode coated with $TiO_2$ layer is soaked in dye solution for about 12-24 hours. But this process takes long time, so we have researched more effective and faster way than the conventional process by applying electric field. Three kinds of electric power such as direct voltage, alternating voltage and pulse voltage were applied to the transparent conducting oxide during the coloring process. As a result, we achieved improved power, fill factor and efficiency of dye-sensitized solar cell in case of applying direct voltage and pulse voltage. In contrast, alternating voltage tend to reduce the dye adsorption on the $TiO_2$ surface and hence the efficiency. We measured the absorption spectra of dye by UV-VIS spectrophotometer before and after soaking the $TiO_2$ in the dye and found no characteristic change in the dye was observed. In this study, we researched on shortening time of coloring process which spent much time in the whole process.

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BGF/PLA 복합재료를 이용한 골절치료용 고정판의 체액 노출 조건에 따른 성능평가 (Performance Evaluation of Bone Plates Consisted of BGF/PLA Composite Material according to Body Fluid Exposure Conditions)

  • 정경채;한민구;;장승환
    • Composites Research
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    • 제30권1호
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    • pp.21-25
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    • 2017
  • 본 연구에서는 일방향 생분해성 유리섬유(BGF)와 친환경 생분해성 수지인 폴리락트산(PLA)을 이용하여 골절치료용 복합재료 고정판을 제작하고 체액 노출에 따른 고정판의 성능 변화를 확인하고자 $50.0^{\circ}C$ 온도조건으로 설정된 인산완충식염수(PBS)에 제작된 생분해성 고정판을 0~3주 동안 노출시켜 질량 변화를 측정하고 4점 굽힘 실험을 수행하였다. 굽힘 강성, 수분 흡수율, 그리고 질량 감소율과 같은 기계적 특성 변화를 파악하였으며 실험 결과로부터 노출 기간이 증가함에 따라 고정판을 구성하고 있는 생분해성 재료들의 손실로 인해 기계적 물성이 서서히 저하되는 경향을 보이는 것을 확인하였다.

막증류 공정의 전처리 공정으로서 천연 제올라이트 컬럼 적용 (Scalants removal from synthetic RO brine using natural zeolite)

  • 정성필;정하윤;윤택근;이석헌
    • 상하수도학회지
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    • 제30권3호
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    • pp.279-284
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    • 2016
  • Membrane distillation (MD) is the thermally driven water separation process based on the vapor pressure difference across the membrane. In order to increase the water recovery of the conventional RO process, the additional MD-PRO pocess was suggested. In this study, the syntheric RO brine was used as a feed solution of the MD process. Due to the high salinity of the RO brine, the MD membrane could be fouled by the scalants. In order to mitigate the scaling on the MD membrane surface, the pre-treatment process using the column filled by natural zeolite was applied. The roughing filter was installed between the pre-treatment process and MD system in order to prevent possible particulate fouling by the debries of the natural zeolite. Moreover, in order to enhance the CEC of the natural zeolite, the NaCl soaking was conducted. The flux and electronic conductivity were monitored under given experimental conditions. And the membrane morphology and the chemical compositions were analyzed by using the SEM-EDX.

Priming Effect of Rice Seeds on Seedling Establishment under Adverse Soil Conditions

  • Lee, Suk-Soon;Kim, Jae-Hyeun;Hong, Seung-Beam;Yun, Sang-Hee;Park, Eui-Ho
    • 한국작물학회지
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    • 제43권3호
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    • pp.194-198
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    • 1998
  • An experiment was carried out to find out the priming effects of rice seeds, Oryza sativa L. (cv. Ilpumbyeo) on. the seedling establishment and early emergence under excess soil moisture conditions. Seeds were primed by soaking in -0.6 MPa polyethylene glycol (PEG) solution at $25^{\circ}C$ for 4 days. The primed seeds were sown in soils with various soil moistures (60, 80, 100, 120, and 140% field capacity) at 17 and $25^{\circ}C$, respectively. Germination and emergence rates, plumule height, and radicle length of primed seeds were higher than those of untreated seeds at any soil moisture and temperature examined. The time from planting to 50% germination ($T_{50}$) of primed seeds was less than that of untreated seeds by 0.9~3.7 days. Germination rate, emergence rate, plumule height, and radicle length were highest at the soil moisture of 80% field capacity among the soil moistures. Priming effects of rice seeds on germination and emergence rates were more prominent under the unfavorable soil moistures (60, 100, 120, and 140% field capacity) than those under the optimum soil moisture condition (80% field capacity). However, priming effects on seedling growth were greater at near optimum soil moisture compared with too lower or higher soil moistures. Therefore, these findings suggest that priming of rice seeds may be a useful way for better seedling establishment under the adverse soil conditions.

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Effect of Propionic Acid in the Germination of Rice Genotypes

  • Kopp, Mauricio Marini;Luz, Viviane Kopp da;Maia, Luciano Carlos da;Sousa, Rogerio Oliveira de;Oliveira, Antonio Costa de
    • Journal of Crop Science and Biotechnology
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    • 제11권4호
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    • pp.249-256
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    • 2008
  • The objective of this work was to evaluate the germination of 12 rice genotypes under propionic acid stress, a phytotoxic compound produced in low drainage soils with high organic matter content. The tests were conducted with the first count of germination (PCG) and germination (G) of the genotypes subjective to 0, 3, 6, and 9 mM propionic acid concentrations. The seeds of each genotype were placed in germitest paper pre-soaked in treatment solutions forming individual bags. The germination was performed at $25^{\circ}C$ and the counts were carried out at 7 (PCG) and 14 days (G). A factorial random block design was performed with four replications of 50 seeds per genotype. Our study revealed that doses up to 9 mM propionic acid in the pre-soaking solution were efficient for genetic variability studies involving the character germination in rice; genetic variability for germination was detected in the collection of rice genotypes when subjected to propionic acid toxic effects. The genotypes Guichow, Dawn, and Toride-1 showed germination stability when subjected to increasing levels of propionic acid, and genotypes originated from irrigated system-cultivation performed better when subjected to propionic acid stress. These three genotypes will be a good biological material to for enhance the resistance to phytotoxic compounds in rice.

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TiO2 고정화 지지체를 이용한 Chlorothalonil의 광촉매분해 (Photocatalytic Degradation of Chlorothalonil using TiO2 Supported in Matrices)

  • 김종향;남춘동;김병관
    • 공업화학
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    • 제7권4호
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    • pp.750-756
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    • 1996
  • $TiO_2$ 고정화 물질은 Titanium tetraisopropoxide-isopropanol 용액에 제오라이트와 glass filter를 담지한 후, 이것을 공기중에 건조시켜 $500^{\circ}C$에서 소결하여 얻었다. Chlorothalnoil의 분석은 ECD가 부착된 가스크로마토그래피로 분석하였다. Chlorothalnoil에 대한 분해효율은 $TiO_2$로 지지된 광촉매가 효과적이었고, 3시간 후 완전히 분해되었다. 반응 생성물들은 $TiO_2$로 지지된 제오라이트에서는 $Cl^-$가 5.0ppm, $TiO_2$로 지지된 glass filter에서는 $Cl^-$가 7.5ppm,그리고 $TiO_2$ 분말에서는 $Cl^-$가 2.0ppm 각각 생성되었다. 그러나, $CN^-$는 지지체의 종류에 관계없이 검출한계이하였다.

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응고제 종류가 감 분말 첨가 두부의 품질과 저장성에 미치는 영향 (Effect of Different Coagulants on Quality of Tofu Incorporated with Persimmon Fruit Powder)

  • 이윤래;정헌식;성종환;문광덕
    • 한국식품저장유통학회지
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    • 제18권5호
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    • pp.678-683
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    • 2011
  • 떫은감 분말 첨가 두부의 수율, 품질 및 저장성에 응고제의 종류(magnesium chloride, calcium chloride, calcium sulfate, glucono-${\delta}$-lactone)가 미치는 영향을 조사하였다. Glucono-${\delta}$-lactone으로 응고시킨 두부가 가장 높은 수율, hardness, chewness, crispness, overall acceptability 및 가장 낮은 L값, b값, pH, 침지저장액 탁도, 총균수를 보였다. Calcium sulfate와 calcium chloride으로 응고시킨 두부는 비교적 높은 L과 b값을 나타내었다. Magnesium chloride로 응고시킨 두부는 관능적 품질특성(firmness, taste, overall acceptability)이 glucono-${\delta}$-lactone 응고 두부와 상호 유의적인 차이가 없이 비교적 높게 평가되었다. 이러한 결과로써 glucono-${\delta}$-lactone과 magnesium chloride가 떫은감 분말 첨가 두부 제조에 적합한 응고제로 판단된다.