• Title/Summary/Keyword: smart composite materials

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The effect of dentin desensitizers and Nd:YAG laser pre-treatment on microtensile bond strength of self-adhesive resin cement to dentin

  • Acar, Ozlem;Tuncer, Duygu;Yuzugullu, Bulem;Celik, Cigdem
    • The Journal of Advanced Prosthodontics
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    • v.6 no.2
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    • pp.88-95
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    • 2014
  • PURPOSE. The purpose of this study is to evaluate if pre-treatment with desensitizers have a negative effect on microtensile bond strength before cementing a restoration using recently introduced self-adhesive resin cement to dentin. MATERIALS AND METHODS. Thirty-five human molars' occlusal surfaces were ground to expose dentin; and were randomly grouped as (n=5); 1) Gluma-(Glutaraldehyde/HEMA) 2) Aqua-Prep F-(Fluoride), 3) Bisblock-(Oxalate), 4) Cervitec Plus-(Clorhexidine), 5) Smart protect-(Triclosan), 6) Nd:YAG laser, 7) No treatment (control). After applying the selected agent, RelyX U200 self-adhesive resin cement was used to bond composite resin blocks to dentin. All groups were subjected to thermocycling for 1000 cycles between $5-55^{\circ}C$. Each bonded specimen was sectioned to microbars ($6mm{\times}1mm{\times}1mm$) (n=20). Specimens were submitted to microtensile bond strength test at a crosshead speed of 0.5 mm/min. Kolmogorov-Smirnov, Levene's test, Kruskal-Wallis One-way Analysis of Variance, and Conover's nonparametric statistical analysis were used (P<.05). RESULTS. Gluma, Smart Protect and Nd:YAG laser treatments showed comparable microtensile bond strengths compared with the control group (P>.05). The microtensile bond strengths of Aqua-Prep F, and Cervitec Plus were similar to each other but significantly lower than the control group (P<.05). Bisblock showed the lowest microtensile bond strength among all groups (P<.001). Most groups showed adhesive failure. CONCLUSION. Within the limitation of this study, it is not recommended to use Aqua-prep F, Cervitec Plus and Bisblock on dentin when used with a self-adhesive resin cement due to the decrease they cause in bond strength. Beside, pre-treatment of dentin with Gluma, Smart protect, and Nd:YAG laser do not have a negative effect.

Nonlinear magneto-electro-mechanical vibration analysis of double-bonded sandwich Timoshenko microbeams based on MSGT using GDQM

  • Mohammadimehr, M.;Shahedi, S.
    • Steel and Composite Structures
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    • v.21 no.1
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    • pp.1-36
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    • 2016
  • In the present study, the nonlinear magneto-electro-mechanical free vibration behavior of rectangular double-bonded sandwich microbeams based on the modified strain gradient theory (MSGT) is investigated. It is noted that the top and bottom sandwich microbeams are considered with boron nitride nanotube reinforced composite face sheets (BNNTRC-SB) with electrical properties and carbon nanotube reinforced composite face sheets (CNTRC-SB) with magnetic fields, respectively, and also the homogenous core is used for both sandwich beams. The connections of every sandwich beam with its surrounding medium and also between them have been carried out by considering Pasternak foundations. To take size effect into account, the MSGT is introduced into the classical Timoshenko beam theory (CT) to develop a size-dependent beam model containing three additional material length scale parameters. For the CNTRC and BNNTRC face sheets of sandwich microbeams, uniform distribution (UD) and functionally graded (FG) distribution patterns of CNTs or BNNTs in four cases FG-X, FG-O, FG-A, and FG-V are employed. It is assumed that the material properties of face sheets for both sandwich beams are varied in the thickness direction and estimated through the extended rule of mixture. On the basis of the Hamilton's principle, the size-dependent nonlinear governing differential equations of motion and associated boundary conditions are derived and then discretized by using generalized differential quadrature method (GDQM). A detailed parametric study is presented to indicate the influences of electric and magnetic fields, slenderness ratio, thickness ratio of both sandwich microbeams, thickness ratio of every sandwich microbeam, dimensionless three material length scale parameters, Winkler spring modulus and various distribution types of face sheets on the first two natural frequencies of double-bonded sandwich microbeams. Furthermore, a comparison between the various beam models on the basis of the CT, modified couple stress theory (MCST), and MSGT is performed. It is illustrated that the thickness ratio of sandwich microbeams plays an important role in the vibrational behavior of the double-bonded sandwich microstructures. Meanwhile, it is concluded that by increasing H/lm, the values of first two natural frequencies tend to decrease for all amounts of the Winkler spring modulus.

Basic Study on P(VDF-TrFE) Smart Sensor for Monitoring Composite Structure Behaviors (복합재료구조물 거동 관찰을 위한 P(VDF-TrFE) 스마트센서의 기초연구)

  • Bae, Ji-Hun;Chang, Seung-Hwan
    • Composites Research
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    • v.28 no.3
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    • pp.75-80
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    • 2015
  • Poly(vinylidene fluoride-trifluoroethylene; P(VDF-TrFE)) is one of the most promising electroactive polymers with numerous application potentials in many fields of industry. Because of its good electro-mechanical properties P(VDF-TrFE) has been used for a number of sensors and actuators and also can be used for monitoring composite structure behaviors as a sensor. Three different ways (Electrical poling, annealing-cooling, and pressing) to enhance ${\beta}$-phase of P(VDF-TrFE) film were carried out. A microscopic analysis was conducted using X-ray diffraction to investigate the effect of such treatments on piezoelectric properties of P(VDF-TrFE) film. From the results, poling, annealing-cooling, and pressing were all effective to enhance ${\beta}$ crystallinity of P(VDF-TrFE) film and the maximum increase rate was 62.80% from 45.29% of the control group.

Enhanced Electric Conductivity of Cement Composites by Functionalizing Graphene Oxide (산화그래핀 기능화에 의한 시멘트 복합체의 전기전도 특성 개선)

  • Jung-Geun Han;Jae-Hyeon Jeon;Young-Ho Kim;Jin Kim;Jong-Young Lee
    • Journal of the Korean Geosynthetics Society
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    • v.22 no.1
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    • pp.1-7
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    • 2023
  • This study has utilized self-assembled monolayers technology to improve electrical property of graphene-oxide, which has been seperated graphine powder through a chemical exfoliation. Aluminum sulfate (Al2(SO4)3) was applied on graphene-oxide as a reactant, and the fundamental research was carried out to apply on the self-sensing of cement-based construction structures. Electric resistance measurement result has shown that cement-composites with GO and Al-GO can be used as a conductor, electric resistance of GO and Al-GO contained composites improved by 10.2% and 15.9% respectively when compared to the standard cement-composite. Microstructure analyzation shown the formation of Al(OH)3 gel when Al-GO was added, which is speculated to result the smooth flow of current by improving the density of cement-composite. This implies that graphene-oxide has a possibility to be utilized as smart building materials and construction structure itself rather than just a structure.

Wearable Textile Strain Sensors (웨어러블 텍스타일 스트레인 센서 리뷰)

  • Roh, Jung-Sim
    • Fashion & Textile Research Journal
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    • v.18 no.6
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    • pp.733-745
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    • 2016
  • This paper provides a review of wearable textile strain sensors that can measure the deformation of the body surface according to the movements of the wearer. In previous studies, the requirements of textile strain sensors, materials and fabrication methods, as well as the principle of the strain sensing according to sensor structures were understood; furthermore, the factors that affect the sensing performance were critically reviewed and application studies were examined. Textile strain sensors should be able to show piezoresistive effects with consistent resistance-extension in response to the extensional deformations that are repeated when they are worn. Textile strain sensors with piezoresistivity are typically made using conductive yarn knit structures or carbon-based fillers or conducting polymer filler composite materials. For the accuracy and reliability of textile strain sensors, fabrication technologies that would minimize deformation hysteresis should be developed and processes to complement and analyze sensing results based on accurate understanding of the sensors' resistance-strain behavior are necessary. Since light-weighted, flexible, and highly elastic textile strain sensors can be worn by users without any inconvenience so that to enable the users to continuously collect data related to body movements, textile strain sensors are expected to become the core of human interface technologies with a wide range of applications in diverse areas.

Thermal and Creep Analysis of an Exhaust Duct of Smart UAV with FGM (경사기능재료를 사용한 스마트 무인기 덕트의 열해석과 크리프 해석)

  • Im, Jong-Bin;Park, Jeong-Seon;Yun, Dong-Yeong;Lee, Jeong-Jin
    • Journal of the Korean Society for Aeronautical & Space Sciences
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    • v.34 no.1
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    • pp.65-73
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    • 2006
  • The high temperature occurs due to the combustion gas from engine in unmanned aerial vehicles (UAV). The high temperature may cause serious damages in UAV structure. The Functionally Graded Material (FGM) is chosen as a candidate material of the engine duct structure. A functionally graded material (FGM) is a two- component mixture composed by compositional gradient materials from one material to the other. In contrast, traditional composite materials are homogeneous mixtures, and involve compositions between the desirable properties of the component materials. Since significant proportions of an FGM contain the pure form of each material, the need for compromise is eliminated. The properties of both components can be fully utilized. Thermal stress analysis of FGM layers (20, 40, 60, 80 and 100) is performed in this paper. In addition, the creep behavior of FGM applied in duct structure of an engine is analyzed for better understanding of FGM characteristics.

Wettability and Intermetallic Compounds of Sn-Ag-Cu-based Solder Pastes with Addition of Nano-additives (나노 첨가제에 따른 Sn-Ag-Cu계 솔더페이스트의 젖음성 및 금속간화합물)

  • Seo, Seong Min;Sri Harini, Rajendran;Jung, Jae Pil
    • Journal of the Microelectronics and Packaging Society
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    • v.29 no.1
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    • pp.35-41
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    • 2022
  • In the era of Fifth-Generation (5G), technology requirements such as Artificial Intelligence (AI), Cloud computing, automatic vehicles, and smart manufacturing are increasing. For high efficiency of electronic devices, research on high-intensity circuits and packaging for miniaturized electronic components is important. A solder paste which consists of small solder powders is one of common solder for high density packaging, whereas an electroplated solder has limitation of uniformity of bump composition. Researches are underway to improve wettability through the addition of nanoparticles into a solder paste or the surface finish of a substrate, and to suppress the formation of IMC growth at the metal pad interface. This paper describes the principles of improving the wettability of solder paste and suppressing interfacial IMC growth by addition of nanoparticles.

Measurements of the Adhesion Energy of CVD-grown Monolayer Graphene on Dielectric Substrates (단일층 CVD 그래핀과 유전체 사이의 접착에너지 측정)

  • Bong Hyun Seo;Yonas Tsegaye Megra;Ji Won Suk
    • Composites Research
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    • v.36 no.5
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    • pp.377-382
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    • 2023
  • To enhance the performance of graphene-based devices, it is of great importance to better understand the interfacial interaction of graphene with its underlying substrates. In this study, the adhesion energy of monolayer graphene placed on dielectric substrates was characterized using mode I fracture tests. Large-area monolayer graphene was synthesized on copper foil using chemical vapor deposition (CVD) with methane and hydrogen. The synthesized graphene was placed on target dielectric substrates using polymer-assisted wet transfer technique. The monolayer graphene placed on a substrate was mechanically delaminated from the dielectric substrate by mode I fracture tests using double cantilever beam configuration. The obtained force-displacement curves were analyzed to estimate the adhesion energies, showing 1.13 ± 0.12 J/m2 for silicon dioxide and 2.90 ± 0.08 J/m2 for silicon nitride. This work provides the quantitative measurement of the interfacial interactions of CVD-grown graphene with dielectric substrates.

Effects of Matrix Strength, Fiber Type, and Fiber Content on the Electrical Resistivity of Steel-Fiber-Reinforced Cement Composites During Fiber Pullout (매트릭스 강도, 섬유 형식 및 보강량에 강섬유 보강 시멘트 복합재료의 인발시 전기저항에 미치는 영향)

  • Le, Huy Viet;Kim, Dong Joo
    • KSCE Journal of Civil and Environmental Engineering Research
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    • v.39 no.6
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    • pp.675-689
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    • 2019
  • Development of smart construction materials with both self-strain and self-damage sensing capacities is still difficult because of little information about the self-damage sensing source. Herein, we investigate the effects of the matrix strength, fiber geometry, and fiber content on the electrical resistivity of steel-fiber-reinforced cement composites by multi-fiber pullout testing combined with electrical resistivity measurements. The results reveal that the electrical resistivity of steel-fiber-reinforced cement composites clearly decreased during fiber-matrix debonding. A higher fiber-matrix interfacial bonding generally leads to a higher reduction in the electrical resistivity of the composite during fiber debonding due to the change in high electrical resistivity phase at the fiber-matrix interface. Higher matrix strengths, brass-coated steel fibers, and deformed steel fibers generally produced higher interfacial bond strengths and, consequently, a greater reduction in electrical resistivity during fiber debonding.

A Milli-Scale Double-sided Crawling Robot (양면 주행이 가능한 소형 12족 주행 로봇)

  • Kim, Sung-Hyun;Jung, Gwang-Pil
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.21 no.4
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    • pp.356-361
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    • 2020
  • This paper presents a lightweight milli-scale crawling robot that can crawl on both sides, which was inspired by the movement of insects. This robot has an excellent ability to overcome obstacles, such as the narrow gaps and the rough terrain. In addition, the robot can crawl steadily and rapidly through triangular alternation, such as ants or cockroaches. The process of smart composite microstructures (SCM) was employed to make a lightweight robot structure. The SCM process replaced the conventional mechanical parts with flexure joints and composite links, which allows the weight of the robot to be reduced. In addition, the robot structure was robust against external impacts owing to the compliance of the constituent materials. Using the SCM process, the robot weighed only 32g with twelve legs in total on both sides. The robot showed a crawling speed of 0.52m/s on the front side and 0.42m/s on the backside.