• Title/Summary/Keyword: size reduction

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Activation of Spinel Phase Magnetite by Hydrogen Reduction (스피넬상 마그네타이트의 수소환원에 의한 활성화)

  • 류대선;이동석;이풍헌;김순태
    • Journal of the Korean Ceramic Society
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    • v.37 no.6
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    • pp.559-563
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    • 2000
  • To decompose carbon dioxide, magnetite was synthesized with 0.2M-FeSO4$.$7H2O and 0.5 M-NaOH by coprecipitation. The deoxidized magnetite was prepared from the magnetite by hydrogen reduction for 1, 1.5, 2 hr. The degree of hydrogen reduction and the decomposition rate of carbon dioxide were investigated with hydrogen reduction time. The crystal structure of the magnetite was identified spinel structute by the X-ray powder diffractions. After magnetite was reduced by hydrogen, magnetite reduced by hydrogen become new phae(${\alpha}$-Fe2O3, ${\alpha}$-Fe) and spinel type simultaneously. After decomposing of carbon dioxide at 350$^{\circ}C$, new phse(${\alpha}$-Fe2O3, ${\alpha}$-Fe) were removed and the spinel type only existed. The specific surface area of the synthesized magnetite was 46.69㎡/g. With the increase of the hydrogen reduction time, the grain size, the hydrogen reduction degree and the decomposition rate of carbon dioxide was increased.

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A Study on the Effect of Setup Time Reduction on Production Lot Sizes (생산준비시간 단축과 생산로트사이즈에 대한 연구)

  • 구일섭;김진수
    • Journal of Korean Society of Industrial and Systems Engineering
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    • v.17 no.32
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    • pp.121-126
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    • 1994
  • Setup Time Reduction is an important aspect of the Just-in-Time(JIT) and Zero Inventory(Zl) Concepts since it supports reductions in manufacturing lead times and inventories. It also enables small lot sizes and kanban systems implementation for material flow - achieving major improvements in production floor management. One concept fundamental to the pursuit of JIT production in Japan and other countries is adoption of a setup time reduction. This paper looks at the necessities of setup time reduction and the relations to machine utilization. By using an EOQ model for evaluate the effect of setup time reduction, we get the results that over 75 % reduction in setup time is obtain the desired results in the lot size reduction.

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Preparation of BaTiO3 Powder in $BaO2-TiO2-Reduction Agent-PSCA (Particle Size Control Agent) System by SHS and Its Dielectric Properties (B3O2-TiO2-환원제-입자제어제계에서 자전연소합성법에 의한 BaTiO3분말의 제조 및 유전특성)

  • Yun, Ki-Seok;Lim, Sung-Jae;Nersisyan, Hayk;Won, Chang-Whan
    • Journal of the Korean Ceramic Society
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    • v.41 no.11
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    • pp.842-850
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    • 2004
  • We have investigated on the preparation of BaTiO$_3$ powder at the system of BaO$_2$-TiO$_2$-Reduction ag.-PSCA by SHS. C and Mg were used as reduction agent, and NaCl was used as PSCA (Particle Size Control Agent). The effects of the various reduction agent and its concentration, particle size control agent, reaction mixture mass on the product in the preparation of BaTiO$_3$ powder at the optimum system by SHS were investigated. The optimum conditions for reaction system and composition were BaO$_2$+TiO$_2$+0.11 Mg +0.2C+0.75NaCl in the As atmosphere. NaCl as PSCA showed the effect of controlling the particle size of product as well as the combustion temperature. The particle size of BaTiO$_3$ synthesized at the optimum condition was about 0.5 ${\mu}{\textrm}{m}$. And as the mixture mass for the reaction was increased, the more stable combustion wave appeared. We have conducted the sintering experiment at the temperature of 130$0^{\circ}C$, the time of 2 h and the atmosphere of air to measure the dielectric properties of BaTiO$_3$ synthesised in this work, and the sample sintered in this condition showed 2,290 of dielectric constant at 10$0^{\circ}C$ and 13,890 at curie point (129$^{\circ}C$).

Fabrication of Tungsten Powder Mixtures with Nano and Micro Size by Reduction of Tungsten Oxides (텅스텐 산화물의 환원을 이용한 나노/마이크로 크기 텅스텐 혼합분말 제조)

  • Kwon, Na-Yeon;Jeong, Young-Keun;Oh, Sung-Tag
    • Korean Journal of Materials Research
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    • v.27 no.10
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    • pp.513-517
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    • 2017
  • An optimum route to fabricate a hybrid-structured W powder composed of nano and micro size powders was investigated. The mixture of nano and micro W powders was prepared by a ball milling and hydrogen reduction process for $WO_3$ and W powders. Microstructural observation for the ball-milled powder mixtures revealed that the nano-sized $WO_3$ particles were homogeneously distributed on the surface of large W powders. The reduction behavior of $WO_3$ powder was analyzed by a temperature programmed reduction method with different heating rates in Ar-10% $H_2$ atmosphere. The activation energies for the reduction of $WO_3$, estimated by the slope of the Kissinger plot from the amount of reaction peak shift with heating rates, were measured as 117.4 kJ/mol and 94.6 kJ/mol depending on reduction steps from $WO_3$ to $WO_2$ and from $WO_2$ to W, respectively. SEM and XRD analysis for the hydrogen-reduced powder mixture showed that the nano-sized W particles were well distributed on the surface of the micro-sized W powders.

High Fastness Dyeing Technology of Polyester Microfiber with Several Disperse Dyes and Vat dye (수종의 분산 염료 및 환원염료에 의한 Polyester microfiber의 고견뢰 염색기술)

  • 백진주;권오대;손아름;이난형;김삼수
    • Textile Coloration and Finishing
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    • v.15 no.6
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    • pp.1-7
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    • 2003
  • Polyester microfiber has usually greater dye uptake than normal denier polyester fiber in same dyeing condition. In spite of this high dye uptake dyed microfiber fabric has not only low visual colour depth but also poor washing fastness property. In order to study high colouring dyeing technology and high washing fastness of polyester microfiber, dyeing property of polyester microfiber was investigated according to the dye solubility and particle size of used disperse dyes in aqueous dye solution. After disperse dyeing, dyed fabric with disperse dye was redyed with a vat dye without reduction clearing in order to obtain a high washing fastness property. The result were as followings ; A small particle sized disperse dyes such as C. I. Disperse Blue 56 and Red 60 showed high rate of initial exhaution compared with a large particle sized disperse dyes like C. I. Disperse Blue 165 and Red 343. In study of dyeing property of polyester microfiber with C. I. Vat Blue 1, polyester microfiber could achieve high dye uptake at a given optimum vatting process conditions. On the other hand, in consecutive dyeing with disperse and vat dye, K/S value of polyester microfiber with a small particle sized disperse dye increased without reduction clearings, but K/S value of polyester microfiber with a large particle sized disperse dye decreased with reduction clearings.

Numerical Analysis on the Blade Tip Clearance Flow in the Axial Rotor (III) - Evaluation of Tip Leakage Loss and Reduction of Efficiency near Blade Tip Clearance Region of a Rotor - (축류 회전차 익말단 틈새유동에 대한 수치해석 (III) - 회전차 익말단의 누설손실과 효율저하에 대한 평가 -)

  • Ro, Soo-Hyuk;Cho, Kang-Rae
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.23 no.9
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    • pp.1113-1120
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    • 1999
  • Leakage vortices fonned near the blade tip cause an increase of total pressure loss near the casing endwall region and as a result, the efficiency of rotor decreases. The reduction of rotor efficiency is related to the size of tip clearance. In this study, the three-dimensional flow fields in an axial flow rotor were calculated with varying tip clearance under various flow rates, and the numerical results were compared with experimental ones. The effects of tip clearance and the of attack on the leakage vortex and overall performance, and the los9 distributions were investigated through numerical calculations. In this study, tip leakage flow rate and total pressure loss due to the tip clearance were evaluated using numerical results and approximate equations were presented to evaluate the reduction of rotor efficiency due to the tip leakage flow.

Spherical Bi2Te3 Powder Synthesized by Oxide-Reduction Process via Ultrasonic Spray Pyrolysis (초음파 분무 열분해법에 의한 산화물 환원 공정의 구형 Bi2Te3 분말 합성)

  • Song, Chul-Han;Jang, Dae-Hwan;Jin, Yun-Ho;Kong, Man-Sik
    • Journal of the Korean institute of surface engineering
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    • v.50 no.2
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    • pp.114-118
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    • 2017
  • Bismuth telluride ($Bi_2Te_3$) and its alloys are well-known thermoelectric materials for ambient temperature applications. In this study, the dissolved Bi-Te precursor solution was used to synthesis metallic $Bi_2Te_3$ powder via ultrasonic spray pyrolysis and reduction process. The droplets of the Bi-Te precursor solution were decomposed to Bi-Te oxide powders by ultrasonic spray pyrolysis. The spherical $Bi_2Te_3$ powders were synthesized by reduction reaction in atmosphere of hydrogen gas at the temperature above $375^{\circ}C$ for 6h. The reduced $Bi_2Te_3$ powders have a mean particle size of $1.5{\mu}m$. The crystal structure of the powder was evaluated by X-Ray diffraction(XRD), and the microstructure with size and shape powders was observed by fieldemission scanning electron microscope(FE-SEM) and transmission electron microscope(TEM).

Greenhouse Gas Emission Analysis by LNG Fuel Tank Size through Life Cycle

  • Park, Eunyoung;Choi, Jungho
    • Journal of Ocean Engineering and Technology
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    • v.35 no.6
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    • pp.393-402
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    • 2021
  • As greenhouse gas emissions from maritime transport are increasing, the International Maritime Organization is continuously working to strengthen emission regulations. Liquefied natural gas (LNG) fuel is less advantageous as a point of CO2 reduction due to the methane leakage that occurs during the bunkering and operation of marine engines. In this study, greenhouse gas emissions from an LNG-fueled ship were analyzed from the perspective of the life cycle. The amount ofmethane emission during the bunkering and operation procedures with various boil-off gas (BOG) treatment methods and gas engine specifications was analyzed by dynamic simulation. The results were also compared with those of other liquid fuel engines. As a result, small LNG-fueled ships without a BOG treatment facility emitted 32% more greenhouse gas than ships utilizing marine gas oil or heavy fuel oil. To achieve a greenhouse gas reduction via a BOG treatment method, a gas combustion unit or re-liquefaction system must be mounted, which results in a greenhouse gas reduction effect of about 25% and 30%. As a result of comparing the amount of greenhouse gas generated according to the BOG treatment method used with each tank size from the perspective of the operating cycle with the amounts from using existing marine fuels, the BOG treatment method showed superior effects of greenhouse gas reduction.

Low Noise Vacuum Cleaner Design (저소음 청소기 개발)

  • Joo, Jae-Man;Lee, Jun-Hwa;Hong, Seun-Gee;Oh, Jang-Keun;Song, Hwa-Gyu
    • Proceedings of the Korean Society for Noise and Vibration Engineering Conference
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    • 2007.11a
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    • pp.939-942
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    • 2007
  • Vacuum cleaner is a close life product that can remove various dusts from our surroundings. However well vacuum cleaner clean our environments, many people are looking away from it, due to its loud noise. Its noise causes a big trouble in the usual life, for example, catch calls, TV watching and discussing etc. To reduce these inconveniences, noise reduction methods and systematic design of low noise vacuum cleaner are studied in this paper. At first, sound quality investigation is performed to get the noise level and quality that make people TV watching and catch calls available. Based on the European and domestic customer SQ survey result, sound power, peak noise level and target sound spectrum guideline are studied and introduced. As a second, precise product sound spectrums are designed into each part based on the sound quality result. Fan-motor, brush, mainbody, cyclone spectrums are decided to get the final target sound based on the contribution level. Fan-motor is the major noise source of vacuum cleaner. Specially, its peak sound, RPM peak and BPF Peak, cause the people nervous. To reduce these peak sounds, high rotating impeller and diffuser are focused due to its interaction. A lot of experimental and numerical tests, operation points are investigated and optimization of flow path area between diffusers is performed. As a bagless device, cyclones are one of the major noise sources of vacuum cleaner. To reduce its noise, previous research is used and adopted well. Brush is the most difficult part to reduce noise. Its noise sources are all comes from aero-acoustic phenomena. Numerical analysis helps the understanding of flow structure and pattern, and a lot of experimental test are performed to reduce the noise. Gaps between the carpet and brush are optimized and flow paths are re-designed to lower the noise. Reduction is performed with keeping the cleaning efficiency and handling power together and much reduction of noise is acquired. With all above parts, main-body design is studied. To do a systematic design, configuration design developments technique is introduced from airplane design and evolved with each component design. As a first configuration, fan-motor installation position is investigated and 10 configuration ideas are developed and tested. As a second step, reduced size and compressed configuration candidates are tested and evaluated by a lot of major factor. Noise, power, mass production availability, size, flow path are evaluated together. If noise reduction configuration results in other performance degrade, the noise reduction configuration is ineffective. As a third configuration, cyclones are introduced and the size is reduced one more time and fourth, fifth, sixth, seventh configuration are evolved with size and design image with noise and other performance indexes. Finally we can get a overall much noise level reduction configuration. All above investigations are adopted into vacuum cleaner design and final customer satisfaction tests in Europe are performed. 1st grade sound quality and lowest noise level of bagless vacuum cleaner are achieved.

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The Differential Effects of Acupuncture on Postures of Healthy Subjects (정상인의 자세에 따른 자침 효과의 차이)

  • Kim, Ji-Eun;Park, Kyung-Mo
    • Journal of Biomedical Engineering Research
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    • v.28 no.1
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    • pp.46-54
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    • 2007
  • Objective: The first aim of this study is to determine the effects of acupuncture on the autonomic nervous system (ANS) via Heart Rate (HR) and Pupil Size (PS), and to compare the effects of acupuncture on the subjects' ANS when they are in a sitting position with the effects when they are in a supine position. Methods: Ten healthy male subjects were randomized to receive either verum acupuncture stimulation in a sitting position (SitV), verum acupuncture stimulation in a supine position (SupV), sham acupuncture stimulation in a sitting position (SitS), and sham acupuncture stimulation in a supine position (SupS). Acupuncture stimulation was applied to Neguan point (PC6) on the forearm. The subject's electrocardiogram (ECG) and pupil size were recorded continuously from 5 min before stimulation to 12 min after stimulation. Results: Verum and sham acupuncture stimulation were found to have reduced heart rate (p<0.01) and to have increased pupil size (p<0.01) in all the subjects. But when the reduction in HR and the increment in PS after verum acupuncture stimulation (both sitting and supine position) were compared with those after sham acupuncture stimulation, it was found that the reduction in HR (74.48 and 73.47 bpm, p<0.063) and the increment of PS (7.32 and, 6.10 mm, p<0.001) after verum acupuncture stimulation were greater than those after sham acupuncture stimulation, and that the corresponding values were statistically significant. In addition, at the baseline, it was found that the subjects had a larger PS and a faster HR in a sitting position than when they did so in a supine position. And then the reduction and increment ratio in the subject's HR and PS when they underwent acupuncture stimulation in a sitting position was significantly different from the reduction and increment in their HR and PS when they underwent the procedure in a supine position-i.e., the reduction ratio in HR was greater when they underwent the procedure in a sitting position, and such reduction ratio was statistically significant (p<0.05). As for the increment in PS, it was greater when the subjects underwent the procedure in a supine position, and such increment was significant (p<0.05). Conclusion: Manual acupuncture stimulation on Neguan point (PC6) has more significant influence on the autonomic nervous system rather than sham acupuncture (tactile stimulation). And the position-induced different states of ANS have different influence on the acupuncture effect.