• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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• pp.599-600
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• 2006

This paper described the state of art of porous metal materials, the typical manufacturing technologies and performances of sintered metal porous materials, with emphasis on the recent research achievements of CISRI in development of porous metal materials. High performance porous metal materials, such as metallic membrane, sub-micron asymmetric composite porous metal, large dimensional and structure complicated porous metal aeration cones and tube, metallic catalytic filter elements, lotus-type porous materials, etc, have been developed. Their applications in energy industry, petrochemical industry, clean coal process and other industrial fields were introduced and discussed.

• 한국레이저가공학회지
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• 제3권3호
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• pp.21-29
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• 2000

For the direct metal shape processing the powder feed device which is different from the widely used in rapid prototyping. is developed, The three dimensional object is shaped with the melting metal powder. The developed research has applied to rapid prototyping in ultraprecision for MEMS and medical science fields required of rapid manufacture of complex shape. The goal of this study make 3D model which has precision accuracy. Powder spreading apparatus has been more improved because that the control of powder spread is very important in layer manufacturing. It consists of the vibration motor, nozzle and tube which supplies various metal powder. This apparatus could control the spreading velocity that could control powder spreading thickness. Laser on/off switch was adapted because laser scanning velocity must be preserved constantly to prevent heat transformation of laser overheating. The error between sintered thickness md experimental one occurred by shrinkage in sintering melting process. The problem of heat transformation was solved by On/Off switching system.

• 대한기계학회논문집A
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• 제30권11호
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• pp.1376-1383
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• 2006

Densification behavior of various metal and ceramic powders was investigated under cold compaction. The Cap model was proposed by using the parameters involved in the yield function for sintered metal powder and volumetric strain evolution under cold isostatic pressing. The parameters for ceramic powder can also be obtained from experimental data under triaxial compression. The Cap model was implemented into a finite element program (ABAQUS) to compare with experimental data for densification behavior of various metal and ceramic powders under cold compaction. The agreement between finite element calculations from the Cap model and experimental data is very good for metal and ceramic powder under cold compaction.

• 한국분말재료학회지
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• 제5권2호
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• pp.145-153
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• 1998

W-Cu alloy is attractive to thermal managing materials in microelectronic devices because of its good thermal properties. The metal injection molding (MIM) of W-Cu systems can satisfy the need for mass production of the complex shaped W-Cu parts in semiconductor devices. In this study, the application of MIM process of the mechanically alloyed (MA) W-Cu composite powders, which had higher sinterability were investigated. The MA W-Cu powders and reduction treated (RT) powders were injected by using of the multicomponent binder system. The multi-stage debinding cycles were adopted in $N_2$ and $H_2$ atmosphere. The isostatic repressing treatment was carried out in order to improve the relative density of brown parts. The brown part of RT W-Cu composite powder sintered at 110$0^{\circ}C$ had shown the higher sinterability compared to that of MA powder. The relative sintered density of all specimens increased to 96% by sintering at 120$0^{\circ}C$ for 1 hour. The relationship between green density and the sintering behavior of MA W-Cu composite powder was analyzed and discussed on the basis of the nanostructured characteristics of the MA W-Cu composite powder.

• Archives of Metallurgy and Materials
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• 제67권4호
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• pp.1547-1550
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• 2022

In this study, a flake-shaped metal powder was coated on a tube shaped pre-sintered 316L stainless steel support using a wet powder spraying process to fabricate a double pore structure, and the pore characteristics were analyzed according to coating time and tube rotation speed. The thickness of the coated layer was checked via optical microscopy, and porosity was measured using image analysis software. Air permeability was measured using a capillary flow porometer. As a result of the experiment, the optimal rotation speed of the support tube was established as 200 rpm. When the rotation speed was fixed, the coating thickness and the coating amount of the double pore structure increased as the coating time increased. The porosity of the double pore structure was increased due to the irregular arrangement of the flake-shaped powder. The air permeability of the double pore structure decreased with increasing fine pore layer thickness.

• 한국분말재료학회지
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• 제11권4호
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• pp.288-293
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• 2004

The application concept of using a fail safety filter on the filtering system is to prevent the particle leakage when the main filter element is broken at high temperature. In this study, the metal filters were fabricated by pressureless sintering method. The mixture of stainless steel powders and filler metal binder solved in the water solutions of 5% PVA was compacted to form the cylindrical filter without pressure. The compacted filter were sintered in the vacuum sintering furnace at 120$0^{\circ}C$ for 1 hour. The metal filter(produced with powder of 640-840 ${\mu}m$ size) having more than above 50% porosity, 500${\mu}m$ pore size, and permeability of 7.3${\times}$10$^{-11}$m$^{2}$ plugged within 2.5 minute to prevent the leakage of maximum slip particle size of less than 3${\mu}m$.

• 한국결정성장학회지
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• 제30권6호
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• pp.220-225
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• 2020

반응부, 이송부, 포집부로 이루어진 기상합성장치를 구축하여 Oxide TFT의 대표적인 물질인 IGZO 반도체용 타겟의 기초 소재인 산화갈륨 나노분말을 기상합성법으로 제조하였다. 반응부에서 갈륨 금속을 증발시켜 1150℃ 이상의 온도에서 산화갈륨 나노분말이 만들어지는 것을 확인하였다. 갈륨 금속은 증발 즉시 반응부에서 산화갈륨 나노분말로 합성되었으며, 반응부의 온도가 증가함에 따라 높은 결정도와 큰 입자 크기를 보였다. 또한, 합성된 산화갈륨 나노분말은 구형의 모양을 가지면서 매우 낮은 응집성을 가졌다. 기상합성법으로 얻은 산화갈륨 나노분말을 상용 산화인듐, 산화아연 분말(몰비 = 1 : 1 : 1)과 혼합하여 소결을 시행한 결과, 소결온도 1450℃에서 5.83 g/㎤의 최대밀도를 얻어 같은 조건하에서 상용 산화갈륨 분말을 이용해 만든 IGZO 소결체(5.61 g/㎤)보다 높은 밀도를 얻음을 볼 수 있었다.

• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part2
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• pp.712-713
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• 2006

We successfully developed Al-Si-Transition Metal (TM) -Rare Earth (RE) Powder Metallurgy (P/M) alloy with fine microstructure, which has high strength at high temperature. This material was compacted rapidly solidified powder and directly consolidated by hot extruding or forging. Before consolidating, rapid heating was performed on powder compaction in order to keep the fine microstructure in powder state. We have also investigated the processing conditions of this new alloy by computing simulations and experiments.

• 한국분말재료학회지
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• 제11권6호
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• pp.472-476
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• 2004

The Fe-Ni compact bodies were fabricated using Fe-Ni mixed powders with 50 nm in diameter by injection molding process. The relationship between microstructure and material properties was characterized with respect to the volume ratio of powder/binder and sintering temperature with SEM and TEM. In the compact body having the volume percent ratio of 45(Fe-Ni) : 55(binder), which was sintered at $900^{\circ}C$ the values of relative density and hardness were low about 97.7% and 277.1 Hv, respectively. Using the composition of 50(Fe Ni) : 50(binder) and sintered at $900^{\circ}C$, the values of relative density and hardness were 98.5%, 294.4 Hv, respec-tively. The grain size of sintered bodies strongly depended on the sintering temperature. In both samples sintered at $600^{\circ}C$ and $900^{\circ}C$, the average grain sizes were about 150 nm and 500 nm in diameter, respectively.

• 한국세라믹학회지
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• 제22권6호
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• pp.58-70
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• 1985

The bond strength of metal to ceramic sealing in Mo-Mn metallizing was investigated by examining the effects of flux composition in alumina ceramics particle size of molybdenum metal powder wet hydrogen atmosphere and temperature in metallizing. The maximum bond strength was obtained when the glass phase filled almost all the microstructural cavities around the interfacial area with few micropores. Such a favorable microstrcutre waas formed and maximum bond strength was observed between 130$0^{\circ}C$. Also the metal to ceramic bond strength was increased using finer molybdenum metal powder than coarse powder. When content of $SiO_2$ in the flux of alumina ceramics was constant metal to ceramic bond strength was improved with increasing the ratio of CaO to MgO in the flux.