• Title/Summary/Keyword: sintered

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An Experimental Study on the Sound Absorption Property of a Sintered Clay Material (점토 소결재의 흡음특성에 관한 실험적 연구)

  • Yang, Yoon-Sang;Lee, Dong-Hoon;Seo, Eun-Sung
    • Transactions of the Korean Society for Noise and Vibration Engineering
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    • v.23 no.4
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    • pp.365-371
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    • 2013
  • The purpose of this study is to develop a sound absorbing material for indoor which manufactured by a clay and binding material. The seven kind of sound absorbing specimens which sintered through a mold process at high temperature were manufactured for the purpose of testing sound absorption performance. The random and normal sound absorption coefficients were measured for the sintered clay sound absorbing specimens with different particle size, density and mixture ratio. From the experimental results, it was found that its particle size was closely related to the sound absorption performance. It was shown that the sintered clay sound absorbing specimen had the sound absorption properties of a fiber-type or a resonance-type sound absorbing material depending on the particle size.

Fabrication of Injection Molded Fe-50%Ni Sintered Bodies (사출성형된 Fe-50%Ni 소결체의 제조)

  • Kim Ki-Hyun;Yoon Hyeong-Chul;Choi Chul-Jin;Lee Byong-Taek
    • Journal of Powder Materials
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    • v.11 no.6 s.47
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    • pp.472-476
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    • 2004
  • The Fe-Ni compact bodies were fabricated using Fe-Ni mixed powders with 50 nm in diameter by injection molding process. The relationship between microstructure and material properties was characterized with respect to the volume ratio of powder/binder and sintering temperature with SEM and TEM. In the compact body having the volume percent ratio of 45(Fe-Ni) : 55(binder), which was sintered at $900^{\circ}C$ the values of relative density and hardness were low about 97.7% and 277.1 Hv, respectively. Using the composition of 50(Fe Ni) : 50(binder) and sintered at $900^{\circ}C$, the values of relative density and hardness were 98.5%, 294.4 Hv, respec-tively. The grain size of sintered bodies strongly depended on the sintering temperature. In both samples sintered at $600^{\circ}C$ and $900^{\circ}C$, the average grain sizes were about 150 nm and 500 nm in diameter, respectively.

Aging Characteristics of 7xxx Series Al Composites with Al2O3 (Al2O3 첨가에 따른 7xxx계 알루미늄 소결체의 시효특성 변화)

  • Min Kyung-Ho;Park Kwang-Hyun;Seo Young-Ik;Chang Si-Young;Kim Young-Do
    • Journal of Powder Materials
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    • v.13 no.3 s.56
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    • pp.172-177
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    • 2006
  • Aging characteristics and mechanical properties of commercial 7xxx series Al composites were investigated from viewpoint of ceramic contents. After sintering process, sintered densities of blended and composite powder were 95 and 97%, respectively. Each part was solution-treated at $475^{\circ}C$ for 60 min and aged $175^{\circ}C$. And two-step aging was also performed form $120^{\circ}C$ to $175^{\circ}C$. The aging behavior of the sintered composite pow-der was different from that of sintered blended powder. The peak aging time of the composite was rapid as well due to strain. Before aging, mechanical properties of sintered composite powder was significantly higher than that of sintered blended powder. These increments of properties were directly affected by ceramic particles. However, after aging, incremental rate of mechanical properties was slowed in the composite.

Fabrication of Gradient Porous Al-Cu Sintered Body (경사 다공성 Al-Cu 소결체의 제조)

  • Byun, Jong-Min;Kim, Se-Hoon;Kim, Jin-Woo;Kim, Young-Moon;Kim, Young-Do
    • Journal of Powder Materials
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    • v.18 no.4
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    • pp.365-371
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    • 2011
  • In this study, gradient porous Al-Cu sintered body was fabricated by powder metallurgy processing. Al-Cu powder mixtures were prepared by low energy ball milling with various milling time. After ball milling for 3h, the shape of powder mixtures changed to spherical type with size of 100~500 ${\mu}m$. Subsequently, Al-Cu powder mixtures were classified (under 150, 150~300 and over 300 ${\mu}m$) and compacted (20, 50 and 100 MPa). Then, they were sintered at $600^{\circ}C$ for various holding time (10, 30, 60 and 120 min) in $N_2$ atmosphere. The sintered bodies had 32~45% of porosity. As a result, the optimum holding time was determined to be 60 min at $600^{\circ}C$ and sintered bodies with various porosity were obtained by controlling the compacting pressure.

Effect of Microstructure on Conductivity of W-Cu Composite (W-CU 복합재료의 전도도에 미치는 미세조직의 영향)

  • Lee Young Jung;Park Kwang Hyun;Lee Byung Hoon;Kim Deok-Soo;Kim Young Do
    • Korean Journal of Materials Research
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    • v.15 no.2
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    • pp.85-88
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    • 2005
  • [ $W-15wt.\%$ ] Cu nanocomposite powders are fabricated by ball-milling and subsequent hydrogen-reduction. The compacted parts of $W-15wt.\%Cu$ nanocomposite powders were sintered at $1200^{\circ}C$ for 1 h with various heating rates of 5 and $20^{\circ}C/min$. The homogeneity of the sintered microstructures was evaluated through homogeneity index by the standard deviation of Victor's hardness test. The W-W contiguities were calculated by using Voronoi diagrams. The sintered microstructure with the heating rate of $20^{\circ}C/min$ was more homogeneous and had lower W-W contiguity than that of $5^{\circ}C/min$. The microstructural homogeneity was directly related to the W-W contiguity. Thermal conductivity of the sintered parts with the heating rate of $20^{\circ}C/min$ was higher than that with heating rate of $5^{\circ}C/min$. This phenomenon indicates that the thermal conductivity is affected by the W-W contiguity resulting from the homogeneity of the sintered microstructure.

A Study on the Variation of Tensile Ductility in Porous Sintered Pure Aluminum (다공성 소결 순 Al에서 인장연성 변화에 관한 연구)

  • Jung, J.Y.
    • Transactions of Materials Processing
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    • v.27 no.2
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    • pp.93-99
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    • 2018
  • An analytical solution for the tensile ductility in porous ductile materials was derived based on an Irwin's approach of the elastic-plastic deformation in fracture mechanics. This was in good agreement with the experimental results of a tensile ductility in a sintered pure Al, and could solve the discrepancies in the Brown and Embury, or the McClintock models. This model was also offered as an advanced analytical solution considering the effect of stress triaxiality of pore tip in addition to pore interactions, material properties of matrix, and local deformation effect around pore. The evaluation of an analytical solution in the sintered pure Al powder compacts showed that the tensile ductility depends not only on the volume fraction of pores, but also on the pore size and on the mechanical properties of the matrix. The tensile ductility of the sintered pure Al compacts decreased rapidly with the increasing of a pore volume fraction, despite of the excellent tensile ductility of the matrix. This significant decrease in the tensile ductility was mainly attributed to the low yield strength of the matrix and small pore size. Particularly, the effects of the large radius and high volume fraction of the pore on the tensile ductility in Al-Form, were thus reasonably predicted by this analytical equation.

Fabrication of Injection Molded Fe Sintered Bodies Using Nano Fe Powder (나노 Fe 분말을 이용하여 사출 성형된 Fe 소결체의 제조)

  • Kim Ki-Hyun;Lim Jae-Hyun;Choi Chul-Jin;Lee Byong-Taek
    • Korean Journal of Materials Research
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    • v.14 no.11
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    • pp.795-801
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    • 2004
  • The injection molded Fe sintered bodies were fabricated using two kinds of Fe powders haying 50 nm and $3\sim5{\mu}m$ in diameter. In the using of Fe powder having 50 nm in diameter, the comparatively dense bodies ($94\sim97\%$) were obtained even at low sintering temperature ($600\sim700^{\circ}C$), while in the sintered bodies ($1000^{\circ}C$) using $3\sim5{\mu}m$ Fe powder, their relative densities showed low values about $93\%$, although they were strongly depend on the sintering temperature and volume ratio of Fe powder and binder. In the sintered bodies using of 50 nm Fe powders, the volume shrinkage and grain size increased as the sintering temperature increased, but the values of hardness decreased. In the sample sintered at $650^{\circ}C$, the values of relative density, volume shrinkage and grain size were $96\%,\;37\%\;and\;0.97{\mu}n$, respectively and the minimum value of wear depth was obtained due to combination of fine grain and comparatively high density.

Effect of Large $\alpha$-Silicon Carbide Seed Grains on Microstructure and Fracture Toughness of Pressureless-Sintered $\alpha$-Silicon Carbide

  • Young-Wook Kim;Kyeong Sik Cho;June-Gunn Lee
    • The Korean Journal of Ceramics
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    • v.2 no.1
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    • pp.39-42
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    • 1996
  • ${\alpha}-SiC$ powder with or without the addition of 0.1 wt% of large ${\alpha}-SiC$ partices(seeds) was pressureless-sintered at $1950^{\circ}C$ for 0.5, 2, and 4 h using $Y_3Al_5 O_{12}$ (yttrium aluminum garnet, YAG) as a sintering aid. The materials without seeds had an equiaxed grain struture. In contrast, the materials with seeds sintered for 2 and 4 h had a duplex microstructure with large elongated grains and amall equiaxed grains. Addition of large ${\alpha}-SiC$ seeds into ${\alpha}-SiC$ accelerated the grain growth of some ${\alpha}-SiC$ grains during sintering and resulted in the increased fracture toughness of the sintered materials. The fracture toughnesses of materials with or without seeds sintered for 4 h were 6.6 and $5.2 MPa \;m^{12}$, respectively.

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Environmental Properties of ZnO Varistors with Variation of Sintering Temperature (소결온도에 따른 ZnO 바리스터의 내환경 특성)

  • Lee, Sung-Gap;Cho, Hyun-Moo;Lee, Jong-Deok;Park, Sang-Man
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.18 no.12
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    • pp.1111-1116
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    • 2005
  • ZnO varistor ceramics added a glass-frit 0.03 $wt\%$ were fabricated with variation of sintering temperature. The sintering temperature and time were $1125^{\circ}C\~1200^{\circ}C$ and 2 h. The average grain sizes increased and the varistor voltage decreased with increasing the sintering temperature. The values of the specimen sintered at $1200^{\circ}C$ were $23.7\;{\mu}m$ and 329 V, respectively. The leakage current of all specimens was less than $1\;{\mu}A$ at DC $82\%$ of varistor voltage. The clamping voltage ratio of the specimen sintered at $1175^{\circ}C$ was 1.37. The endurance of surge current and the deviation of varistor voltage of the specimen sintered at $1175^{\circ}C$ were 6400 $A/cm^2$ and ${\Delta}-2.81\%$, respectively. After the High Temperature Load Test(HTLT) at $85^{\circ}C$ for 1000 h, the specimen sintered at $1175^{\circ}C$ showed the lowest deviation of varistor voltage of ${\Delta}-1.92\%$.

A Study on the Relation Between Expansion and the Characteristics of Surface in the ED-Drilling (방전드릴의 방전갭과 표면특성에 관한 연구)

  • Choi, Jong-Yeun;Kim, Kyeong-Hwan
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.11 no.3
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    • pp.73-79
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    • 2012
  • This paper describes the machining characteristics of the sintered carbide and die steel(STD-11) by electric discharge drilling with various tubular electrodes. Electrical discharge machining(EDM) removes material from the workpiece by a series of electrical sparks that cause localized temperatures high enough to melt or vapourize the vicinity of the charge. In the experiment. four types of electrode which have different diameter are used with the application of continuous direct current and axial electrode feed. The controlled factors include the dimension of the electrode. In drilling by EDM, the dielectric flushed down the interior of the rotating tube electrode, in order to order to facilitate the removal of machining debris the hole. The expansion increase with increasing the thickness of material and the diameter of electrode and the expansion of sintered carbide is 1.75 times large then that of die steel. The taper of machined hole decrease with increasing the thickness of material. The crater sixe of die steel is larger then thet of sintered carbide and the surface roughness of sintered carbide is 1.58 tims larger then that of die steel.