• Resources Recycling
• /
• v.19 no.3
• /
• pp.16-23
• /
• 2010

Coal briquette use has dramatically increased because of high oil prices. Hence, it is necessary to develop an environment-friendly recycling technique of the coal briquette ash. The coal briquette ash contains a large amount of an unburned carbon content and a mullite with high thermal property, so it is considered to be used as raw materials of sintered eco-brick. This study aimed to investigate on how the unburned carbon affects properties of the sintered eco-brick. The eco-brick was mixed with the ratio of 50 wt% coal briquette ash having the unburned carbon 10.5 wt% and 50 wt% cullet, then being sintered at $950^{\circ}C$, which of the compressive strength was in line with the first class of the sintered clay brick standard(KS L 4201). In particular, the compressive strength of the sintered eco-brick was equal to the first class of the KS L 4201 despite the increase of mixing ratio for coal briquette ash with 1.0 wt% unburned carbon to 70 wt%.

• Journal of Powder Materials
• /
• v.22 no.4
• /
• pp.271-277
• /
• 2015

As wrought stainless steel, sintered stainless steel (STS) has excellent high-temperature anti-corrosion even at high temperature of $800^{\circ}C$ and exhibit corrosion resistance in air. The oxidation behavior and oxidation mechanism of the sintered 316L stainless was reported at the high temperature in our previous study. In this study, the effects of additives on high-temperature corrosion resistances were investigated above $800^{\circ}C$ at the various oxides ($SiO_2$, $Al_2O_3$, MgO and $Y_2O_3$) added STS respectively as an oxidation inhibitor. The morphology of the oxide layers were observed by SEM and the oxides phase and composition were confirmed by XRD and EDX. As a result, the weight of STS 316L sintered body increased sharply at $1000^{\circ}C$ and the relative density of specimen decreased as metallic oxide addition increased. Compared with STS 316L sintered parts, weight change ratio corresponding to different oxidation time at $900^{\circ}C$ and $1000^{\circ}C$, decreased gradually with the addition of metallic oxide. The best corrosion resistance properties of STS could be improved in case of using $Y_2O_3$. The oxidation rate was diminished dramatically by suppression the peeling on oxide layers at $Y_2O_3$ added sintered stainless steel.

• Journal of Powder Materials
• /
• v.23 no.4
• /
• pp.282-286
• /
• 2016

A sintered body of $TiB_2$-reinforced iron matrix composite ($Fe-TiB_2$) is fabricated by pressureless-sintering of a mixture of titanium hydride ($TiH_2$) and iron boride (FeB) powders. The powder mixture is prepared in a planetary ball-mill at 700 rpm for 3 h and then pressurelessly sintered at 1300, 1350 and $1400^{\circ}C$ for 0-2 h. The optimal sintering temperature for high densities (above 95% relative density) is between 1350 and $1400^{\circ}C$, where the holding time can be varied from 0.25 to 2 h. A maximum relative density of 96.0% is obtained from the ($FeB+TiH_2$) powder compacts sintered at $1400^{\circ}C$ for 2 h. Sintered compacts have two main phases of Fe and $TiB_2$ along with traces of TiB, which seems to be formed through the reaction of TiB2 formed at lower temperatures during the heating stage with the excess Ti that is intentionally added to complete the reaction for $TiB_2$ formation. Nearly fully densified sintered compacts show a homogeneous microstructure composed of fine $TiB_2$ particulates with submicron sizes and an Fe-matrix. A maximum hardness of 71.2 HRC is obtained from the specimen sintered at $1400^{\circ}C$ for 0.5 h, which is nearly equivalent to the HRC of conventional WC-Co hardmetals containing 20 wt% Co.

• Journal of Powder Materials
• /
• v.25 no.4
• /
• pp.302-308
• /
• 2018

A lean alloy is defined as a low alloy steel that minimizes the content of the alloying elements, while maintaining the characteristics of the sintered alloy. The purpose of this study is to determine the change in microstructure and mechanical properties due to the addition of silicon or tin in Fe-Mo-P, Fe-Mn-P, and Fe-Mo-Mn-P alloys. Silicon- or tin-added F-Mo-P, Fe-Mn-P, and Fe-Mo-Mn-P master alloys were compacted at 700 MPa and subsequently sintered under a $H_2-N_2$ atmosphere at $1120^{\circ}C$. The sintered density of three alloy systems decreases under the same compacting pressure due to dimensional expansion with increasing Si content. As the diffusion rate in the Fe-P-Mo system is higher than that in the Fe-P-Mn system, the decrease in the sintered density is the largest in the Fe-P-Mn system. The sintered density of Sn added alloys does not change with the increasing Sn content due to the effect of non-dimensional changes. However, the effect of Si addition on the transverse rupture strengthening enhancement is stronger than that of Sn addition in these lean alloys.

• Journal of the Korean Ceramic Society
• /
• v.35 no.1
• /
• pp.97-105
• /
• 1998

20mol% Gd-doped CeO2 ultrafine powders as a promising electrolyte for the low temperature solid ox-ide fuel cells were synthesized with particle sizes of 15-20 nm using glycine nitrate process(GNP) fol-lowed by sintering their pellets at 150$0^{\circ}C$ for various times in air and then the electrical properties of the sintered pellets were investigated. The sintering behaviors and electrical properties for the sintered 20 sintered mol% Gd-doped CeO2 pellets were analyzed using dilatometer and SEM and AC two-terminal impedance technique respectively. As the heating temperature increased the synthesized powder had the sintering behaviors to show the start of the significant shrink at temperature of about $700^{\circ}C$ and to show the end of the shrink at the temperature of about 147$0^{\circ}C$. When the pellets were sintered with the vaious times at 150$0^{\circ}C$ the temperatuer which the shrink had been already completed the grain sizes in the sintered 20 mol% Gd-doped GeO2 pellets increased with the increase of the sintering time but their electrical resis-tivities showed the minimum value at the sintering time of 10h. It is due that the pellet sintered for 10h had the minimum activation energy fior the electtrical conduction. Thus it is thought that the decrease of the activation energy with the increase of the sintering time to 10h is induced by the enhanced mi-crostructure like the decrease of pore amount and the grain growth and its increase with the sintering times more than 10h is induced by the increase of the amounts of the impurities such as Mg. Al and Si from the sintering atmosphere.

• Tribology and Lubricants
• /
• v.11 no.4
• /
• pp.21-27
• /
• 1995

The effects of interface boundary strength on wear and wear transition during sliding have been investigated in silicon carbide ceramics. Three different microstructures, i.e., solid state sintered silicon carbide, liquid phase sintered silicon carbide and liquid phase sintered silicon carbide composite reinforced with TiB$_{2}$ particulates, were designed by hot pressing. Examinations of crack patterns and fracture modes indicated that interface boundaries were relatively strong between silicon carbide grains in the solid state sintered silicon carbide, intermediate in the liquid phase sintered silicon carbide and weak between silicon carbide grains and TiB$_{2}$ particles in the composite. Wear data and examinations of worn surfaces revealed that the wear behavior of these silicon carbide ceramics could be significantly affected by the interface strength. In the solid state sintered silicon carbide, the wear occurred by a grooving process. In the liquid phase sintered silicon carbide and composite, on the other hand, an abrupt transition in wear mechanism from initial grooving to grain pull-out process occurred during the test. The transition occurred significantly earlier in the composite than in the carbide.

• Journal of the Korea Institute of Building Construction
• /
• v.23 no.4
• /
• pp.359-367
• /
• 2023

This experimental study investigates the replacement of conventional Portland cement and sand with non-sintered cement and ferro-nickel slag to formulate eco-friendly cement mortar. The examination aimed to understand the strength properties of non-sintered cement mortar using ferro-nickel slag as fine aggregate by classifying mortar production types, fine aggregates, and curing methodologies. From flexural and compressive strength tests, it was observed that non-sintered cement mortars, incorporating ferro-nickel slag as fine aggregate, exhibited superior strength when compared to both plain mortar and steam-cured non-sintered mortar. This increased strength is attributed to the influence of the particle size, density, and absorption capabilities of the ferro-nickel slag. Furthermore, X-ray Diffraction(XRD) analyses of the mortars verified the presence of MgO, a component of ferro-nickel slag, in the form of a composite oxide. This finding substantiates the consistent strength manifestation of non-sintered cement mortars utilizing ferro-nickel slag as a fine aggregate.

• Journal of the Korean Magnetics Society
• /
• v.10 no.6
• /
• pp.269-273
• /
• 2000

Fe-l7Cr-2M(M=Si, Nb, Mo) alloy powder was prepared by plasma electrode rotating atomizer and than the alloy powder was formed and sintered. The particle shape of the Fe-l7Cr-2M(M=Si, Nb, Mo) alloy power is spherical. The saturation magnetization of the sintered Fe-17Cr-2Mo and Fe-l7Cr-2Nb alloy are 155 emu/g. The saturation magnetization of the sintered Fe-l7Cr-2Si alloy is less than that of the sintered Fe-l7Cr-2Mo and Fe-l7Cr-2Nb alloy. The amplitude relative permeability of the sintered Fe-l7Cr-2M(M=Si, Nb, Mo) alloy has the maximum value in the range of 3∼5 Oe applied field at forming pressure 12 ton/cm$^2$, sintering temperature 1200$^{\circ}C$, and frequency 1 kHz. Power loss of the sintered Fe-l7Cr-2Nb alloy is 40 mW/cc at applied field, H$\sub$a/=5 Oe, and frequency, f=1 kHz. The power loss of the sintered Fe-l7Cr-2Nb alloy is a half of that of the sintered Fe-l7Cr-2Si and Fe-l7Cr-2Mo alloy.

• Proceedings of the KSME Conference
• /
• 2007.05b
• /
• pp.2136-2141
• /
• 2007

The Loop Heat Pipe(LHP) system uses capillary forces so as to pump the working fluid from heat acquisition to heat rejecting systems. The performance of the LHP systems depends mainly upon the operating performance of the wick structure. The capillary pressure increases with decreasing the pore size of the wick structure. By the way, the wick structure's permeability decreases with decreasing the pore size and the porosity. To obtain an ideal wick, the wick structure should possess several characteristics such as the small pore size, high porosity and chemical compatibility with working fluid. Sintered metal wicks have been mainly used as the capillary wick structure mounted in LHP because of the fact that the sintered metal wick has some advantages like convenient selection of wick material, smaller pore size and so on as well as high reliability. In this study, sintered metal wicks were developed to meet required several parameters to design the high performance LHP systems for obtaining even more effective cooling technologies.

• Tribology and Lubricants
• /
• v.23 no.6
• /
• pp.266-271
• /
• 2007

The brake performance of sintered friction materials for the high speed train was studied. In this study, newly developed sintered materials based on copper were compared with the commercial products for high speed trains. They were tested on a 1/5 scale dynamometer using low carbon steel disks. Effectiveness, fade, and recovery tests were carried out to examine friction performance and the change of disk thickness variation (DTV) during brake applications and noise propensity were also evaluated. Results showed that the two sintered friction materials exhibit similar friction coefficients and braking performance, whereas the newly developed friction material was superior in terms of DTV generation and noise propensity to the commercial friction material. The improvement of the newly developed friction material was attributed to the high graphite content which reduced the stick-slip phenomena and prevented uneven disk wear by producing friction films on the counter disk.