• Title/Summary/Keyword: sintered

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Microstructure and Mechanical Properties of Infiltrated Zirconia-Mullite Composite (침투된 지르코니아-뮬라이트 복합체의 미세구조 및 기계적 성질)

  • 손영권;이윤복;김영우;오기동;박홍채
    • Journal of the Korean Ceramic Society
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    • v.37 no.2
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    • pp.174-180
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    • 2000
  • Y-TZP/mullite composites were prepared by the infiltration of Y-TZP precursor into partially reaction-sintered mullite. The addition of Y-TZP(~7.2 wt%) increased the bend strength(207 MPa), fracture toughness(4.6MPa.m1/2) and Vickers microhardness(853kg/$\textrm{mm}^2$) of the uninfiltrated mullite sintered at 162$0^{\circ}C$ for 10h by more than 75, 70 and 105%, respectively. Residual alumina-rich glass was observed at a mullite/mullite junction, due to the mullitization reaction of silica melt with crystalline $\alpha$-Al2O3 during a final sintering. Although ZrO2 inclusions improved the final sintered density of mullite they did not effectively prevent its grain growth.

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Photovoltaic Properties of Sintered CdS/CdTe Solar Cell (소결체 ITO/CdS/CdTe 태양전지의 광전압특성)

  • 김동섭;조은철;안병태;임호빈
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1994.11a
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    • pp.216-220
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    • 1994
  • Polycrystalline CdS films have been prepared by coating a slurry, which consisted of CdS, 11w% CdCl$_2$ and appropriate amount of propylene glycol, on glass substrate and glass substrate coated with indium tin oxide(ITO) followed by sintering in a nitrogen atmosphere. CdTe slurries consisting of Te powder and Cd powder were coated on the sintered CdS films and ITO/CdS films and were sintered in nitrogen to prepare sintered CdS/CdTe and ITO/CdS/CdTe solar cells. The value of fill factor increased due to low series resistance and open circuit voltage decreased due to low shunt resistance in the ITO/CdS/CdTe solar cells.

Study of sound absorption characteristics using the sintered aluminium plate (알루미늄 소결재를 이용한 흡음 특성 연구)

  • 노대호;김재수;윤진국;강현주;신종철;김원용
    • Proceedings of the Korean Society for Noise and Vibration Engineering Conference
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    • 2002.05a
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    • pp.1071-1076
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    • 2002
  • The purpose of this paper is to examine sound absorption characteristics of sintered Al(aluminum) plate. Comparison between experiment and theoretical analysts by using empirical formula are made. Based on comparison. it is found that Voronina model gives more reasonable explanation for sound absorption characteristics of sintered Al plates. Effect of air gap with varying the thickness of plates are also investigated, which concludes that the air gap generally increase absorption but for too thick thickness of Al plates. Al plates with air gap shows 0.85∼0.9 of NRC(Noise Reduction Coefficient) measured in reverberation room. which is comparable to glass wool. Comparison between normal and random Incident absorption shows that random incident absorption is higher than normal incident absorption.

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Thermoelctric Propretries of Bi2Te3 Fabricated by Mechanical Grinding-Mixing Process (기계적분쇄-혼합공정에 의해 제조된 Bi2Te3 소결체의 열전특성)

  • 이근길
    • Journal of Powder Materials
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    • v.7 no.1
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    • pp.6-11
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    • 2000
  • Two kinds of Bi2Te3 powders, pure Bi2Te3/2vol.%ZrO2, have been prepared by a mechanical grinding process process. Effect of mixing of the powders on thermoelectric of the sintered body has been investigated by measuring Seebeck Coeffcient, specific electric resistivity and thermal conductivity. With an increase in the weight fraction of the Bi2Te3/2vol.%ZrO2 powder from 0 to 40wt.%. Especially, the figure of merit of the mixedBi2Te3 sintered body increases and thereafter dedreases above 40wt.%. Especially. the figure of merit of the mixed Bi2Te3 sintered bodies with mixing of Bi2Te3/2vol.%ZrO2 powder increased about 1.3time in comparison with the value of the specimen before mixing. Mixing of two kinds of Bi2Te3 powders which have different theramal and electric propertries with each other seemed to be useful methob to increase the figure of merit of Bi2Te3 sintered body.

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The Microstructure and Mechanical Properties of Y2O3-Dispersed Fe-C and Fe-CNT Sintered Steels (Y2O3가 분산된 Fe-C 및 Fe-CNT 소결체의 미세구조 및 기계적 특성)

  • Lim, Jin Young;Ahn, Jung-Ho
    • Journal of Powder Materials
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    • v.24 no.4
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    • pp.298-301
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    • 2017
  • In the present work, we use multiwall carbon nanotubes (MWCNT) as the starting material for the fabrication of sintered carbon steel. A comparison is made with conventionally sintered carbon steel, where graphite is used as the starting material. Milling is performed using a horizontal mill sintered in a vacuum furnace. We analyze the grain size, number of pores, X-ray diffraction patterns, and microstructure. Changes in the physical properties are determined by using the Archimedes method and Vickers hardness measurements. The result shows that the use of MWCNTs instead of graphite significantly reduces the size and volume of the pores as well as the grain size after sintering. The addition of $Y_2O_3$.to the Fe-MWCNT samples further inhibits the growth of grains.

Effect of Screen Printing and Sintering Conditions on Properties of Thick Film Resistor on AlN Substrate (인쇄 및 소결조건이 AlN 기판용 후막저항체의 특성에 미치는 영향)

  • Koo, Bon Keup
    • Journal of the Korean Ceramic Society
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    • v.51 no.4
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    • pp.344-349
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    • 2014
  • $RuO_2$-based high frequency thick-film resistor paste was printed at the speed of 10, 100, 300 mm/sec on the AlN substrate, and then sintered at between 750 and $900^{\circ}C$. The sintered thick films were characterized in terms of printing and sintering conditions. With increasing printing speed, the thickness and roughness of sintered film increased. The resistance of the thick film resistor was reduced by increasing the printing speed from 10 to 100 mm/sec, but did not significantly change at 300 mm/sec speed. With increasing sintering temperature, the surface roughness and thickness of sintered resistor film decreased. The reduction rate was large in case of fast printed resistor. The resistance of the resistor increased up to $800^{\circ}C$ with sintering temperature, but again decreased at the higher sintering temperature.

Processability study of dental zirconia block using scratch test (스크래치 시험을 이용한 치과용 지르코니아 블록의 가공성 연구)

  • Kim, Yung-Hoon
    • Journal of Technologic Dentistry
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    • v.40 no.1
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    • pp.27-32
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    • 2018
  • Purpose: This study was performed to investigate processability of the dental zirconia block. Most of the CAD/CAM zirconia restorations utilize the partially sintered blocks, which are sintered at a temperature lower than $1100^{\circ}C$. Methods: Partially sintered zirconia samples were prepared $40{\times}30{\times}10mm$ and surface treatment by #2000 sandpaper. Scratch hardness was determined by the procedure of ASTM G171-03 using a scratch hardness tester(KS TECH, Korea) equipped with a real time load detector to measure tangential force during scratching. The scratch rate was 30 mm/min. Results: Scratch hardness(Hs) increases steeply with increase in the loads. The highest Hs was sampl 1.42 GPa and lowest was sample 0.42 GPa. Conclusion : The machinability of partially sintered CAD/CAM zirconia blocks can be optivized by manipulation of Hs.

Effect of Calcination Temperature on Densification of Magnesia (하소온도가 Magnesia의 치밀화에 미치는 영향)

  • Chon, Uong;Jeong, Dae-Sik;Kim, Hyo-Joon
    • Journal of the Korean Ceramic Society
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    • v.34 no.6
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    • pp.659-667
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    • 1997
  • The effect of calcination temperature of Mg(OH)2 on the green density and densification of MgO was investigated. It was observed that the impure magnesium hydroxide powder showed a higher crystallization rate while it had a lower tendency of agglomeration between periclae crystallites, as compared to that of the pure magnesium hydroxide powder. In the case of calcination of the powders under 85$0^{\circ}C$, the impure powder showed the higher green and sintered density. In spite of higher green density upon the calcination over 100$0^{\circ}C$, the impure powder showed the lower sintered density, caused by exaggerated growth of the periclase crystallites. The highest sintered densities in the both powders were obtained at the calcination temperature of 100$0^{\circ}C$. And the green density was inversely proportional to the sintered density at the calcination over 100$0^{\circ}C$.

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Comparative Study on the Quality of Sintered Zirconia Block Fabricated by Using Domestic Powder and Global-Brand Powder (국산 지르코니아 분말 소결체 품질의 글로벌 제품과의 비교 연구)

  • Kim, Yong-In;Lee, Seung-Mi;Byeon, Jai-Won
    • Journal of Applied Reliability
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    • v.15 no.3
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    • pp.216-221
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    • 2015
  • Sintering behavior of 3%yttria-stabilized zirconia was comparatively studied using a spray-dried powder produced by a domestic and global company. Quality of the sintered block was analysed in terms of relative density, shrinkage rate, grain growth, hardness, and fracture toughness. Relative density, shrinkage rate, and hardness value of the finally sintered block was similar between domestic and global zirconia powder, respectively. But, flexural strength of the domestic powder specimen was about 70% of the sintered block produced by using a global powder. The poor sintering quality of the domestic powder was discussed in relation with compressibility of the spray-dried granule-type powder and the amount of monoclinic phase in the as-received powder.

Establishment of Process of Manufacture of Ti-6Al-4V Alloy Sintering Body by MIM

  • Otsuka, A.;Suzuki, K.;Achikita, M.
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09b
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    • pp.759-760
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    • 2006
  • Ti-6Al-4V has low specific gravity, high corrosion resistance and superior mechanical properties but it is very difficult to control oxygen content in MIM process. It is necessary to use powders with coarse particle size to decrease oxygen content of powders, so feedstocks with poor fluidity and sintered bodies with lower density are obtained in such cases. Fine titanium hydride-dehydride powders were blended with atomized powders to accomplish higher fluidity and sintered density. Sintered bodies had higher sintered density and mechanical properties equivalent to those of wrought materials by controlling oxygen content less than 0.35mass%.

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