• Journal of the Korean Ceramic Society
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• v.54 no.1
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• pp.33-37
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• 2017

Single phase niobium nitride (NbN) coatings were deposited using asymmetric bipolar pulsed dc sputtering by varying pulse frequency and duty cycle of pulsed plasmas. Crystal structure, microstructure, morphology and mechanical properties were examined using XRD, FE-SEM, AFM and nanoindentation. Upon increasing pulse frequencies and decreasing duty cycles, the coating morphology was changed from a pyramidal-shaped columnar structure to a round-shaped dense structure with finer grains. Asymmetric bipolar pulsed dc sputtered NbN coatings deposited at pulse frequency of 25 kHz is characterized by higher hardness up to 17.4 GPa, elastic modulus up to 193.9 GPa, residual compressive stress and a smaller grain size down to 27.5 nm compared with dc sputtered NbN coatings at pulse frequency of 0 kHz. The results suggest that the asymmetric bipolar pulsed dc sputtering technique is very beneficial to reactive deposition of transition-metal nitrides such as NbN coatings.

• 한국정보디스플레이학회:학술대회논문집
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• 2006.08a
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• pp.1775-1778
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• 2006

Through baking process on an interlayer, known as hole transporting layer, varying baking temperature up to 300 degree, which is considered as extremely high for polymer light emitting device (PLED) system, we found interesting relationship between packing density and morphology affecting device performance. Granular morphology shows that as temperature increases, grain size is getting smaller to pack closely and make interlayer harden. Such denser interlayer has temperature dependency of its own mobility, even without clear evidence of degradation of material itself. Its fact proven in a single film also reflects on multilayered PLED's performance like IVL, efficiency, lifetime. It's found that, especially, to enhance lifetime is related with thermal stability of interlayer and its mobility dependency to meet better charge balance. Therefore, it gives us understanding not only baking effect of interlayer, but also material & device designing guide to enhance lifetime.

• Journal of the Korean Institute of Telematics and Electronics A
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• v.29A no.2
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• pp.55-62
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• 1992

Polycrystalline silicon ingots were manufactured using the casting method for polycrystalline silicon solar cells. These ingots were cut into wafers and ten n$^{+}$p type solar cells were made through the following simple process` surface etching, n$^{+}$p junction formation, metalization and annealing. For the grain boundary passivation, the samples were oxidized in O$_2$ for 5 min. at 80$0^{\circ}C$ prior to diffusion in Ar for 100 min. at 95$0^{\circ}C$. The conversion efficiency of polycrystalline silicon solar cells made from these wafers showed about 70-80% of those of the single crystalline silicon solar cell and superior conversion efficiency, compared to those of commercial polycrystalline wafers of Wacker Chemie. The maximum conversion efficiency of our wafers was indicated about 8%(without AR coating) in spite of such a simple fabrication method.

• Proceedings of the Korean Society For Composite Materials Conference
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• 2004.10a
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• pp.23-26
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• 2004

Ag/Ni multilayers with different bilayer thickness between 3 and 100 nm produced by DC magnetron puttering have been studied by cross-sectional TEM and nanoindentation. The micrograph shows perfect layered structure with sharp interfaces between Ag and Ni layers. Absolute hardness is calculated as a reference value to compare hardness of specimens regardless of indent depth. A hardness enhancement of nearly $100\%$ over the rule-of-mixtures values, calculated from the measured hardness of single Ag and Ni thin films, is observed. The hardness increases with decreasing bilayer thickness until 8nm. This enhancement shows a good agreement with Hall-Petch relation using grain size (one half of the bilayer thickness) confined within a layer. The deformation behavior can be explained by dislocation pile-up in smaller grains.

• Smart Structures and Systems
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• v.4 no.2
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• pp.103-121
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• 2008

Shape memory alloys (SMA) have been emphasized, studied and understood in the controlled world of the laboratory. Any attempt to implement one of these alloys in engineered products requires a jump from the controlled world of the laboratory to the actual environment of the application. The first step is to move from single grain specimens to multigrain samples. One works with a material for which any stock is different from that previously available. This paper reviews the milestones in the familiarization process the authors had to overcome during their cooperation within a project funded by the European Union. The main items cover transformation temperatures, thermal treatment and properties understanding.

• Journal of the Korean Crystal Growth and Crystal Technology
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• v.12 no.3
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• pp.120-125
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• 2002

Si-wafers for solar cells were cast in a size of $50{\times}46{\times}0.5{\textrm}{mm}^3$ by vacuum casting method. The graphite mold coated by BN powder, which was to prevent the reaction of carbon with the molten silicon, was used. Without coating, the wetting and reaction of Si melt to graphite mold was very severe. In the case of BN coating, SiC was formed in the shape of tiny islands at the surface of Si wafer by the reaction between Si-melt and carbon of the graphite mold on the high temperature. The grain size was about 1 mm. The efficiency of Si solar cell was lower than that of Si solar cell fabricated on commercial single and poly crystalline Si wafer. The reason of low efficiency was discussed.

• Journal of the Korean Ceramic Society
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• v.27 no.4
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• pp.548-552
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• 1990

Effects of binder addition method during compacting on microstructural change and magnetic characteristics of Sr-ferrite system was investigated. Used binders were PVA and PEG, which were added separately or simultaneously. After compacts were heated at 50$0^{\circ}C$ for 3hr in air for burning out all the binders, they were sintered at 125$0^{\circ}C$ for 2h. Based on results, in the case of using the two binders simultaneously, comparing to single binder system, compacted density was somewhat higher but sintered density was rather lower, and abnormal grain growth was accelerated. According to these sintering characteristics, remanent magnetization and coercive force were also diminished.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 1994.11a
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• pp.65-66
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• 1994

This paper describes study on the preparation of ferrite powder for bonded mallets. The specimen which has the basic composition of SrO$.$nF$_2$O$_3$ with n=5.9 is in nonstoichiomatric region. Calcination is performed under N$_2$ atmosphere 1175$^{\circ}C$, 1200$^{\circ}C$, 1225$^{\circ}C$, 1250$^{\circ}C$ and 1275$^{\circ}C$ respectively. Then, Cooling is carried out in the furnace. In order to increase coecivity and obtain uniform grain size, we add to the specimen 0.7wt%CaCO$_3$, 0.3wt % SiO$_2$, 0.5wt%Na$_2$SiO$_3$ and 0.5wr% Al$_2$O$_3$. Also, in order to increase milling effect, carbon coating on sample particles is tried. As the result, single magnetic domain partic1e with Size of 1$\mu\textrm{m}$ in obtained and magnetic properties are improved.

• Journal of the Korean Institute of Electrical and Electronic Material Engineers
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• v.14 no.5
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• pp.410-416
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• 2001

KLN thin films were fabricated on Pt coated Si(100) wafer using an rf-magnetron sputtering method. The grown KLN thin film consists of 4-fold grains. In this experiment, the structure of 4-fold grained thin film was investigated using XRD and SEM measurements. Pt layer was also deposited using the rf-magnetron sputtering method,. XRD measurement showed that he Pt thin film has Gaussian distribution form with strong (111) direction orientation. The KLN thin film has preferred-orientation of (001) direction, and the peak consists of 2 separate peaks; one with broad FWHM and the other with narrow FWHM. The sharp peak is due to single crystal, and combining with Em results, the 4-fold grain consists of singel crystals with c-axis normal to substrate.

• Journal of the Korean Wood Science and Technology
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• v.17 no.4
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• pp.83-88
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• 1989

목재의 섬유방향에 경사진 균열의 모-드I과 모-드II의 혼합모-드파괴시의 파괴거동을 조사하기 위하여 라왕(Shorea Spp.)의 LA시스템에 있어서 서로 다른 경사각도를 가진 SEN시험편(Single edge notch specimen)에 대하여 휨 시험을 행하였다. 얻이진 결과는 혼합모-드파괴시, 모-드I응력확대계수$K_I$과 모-드II응력확대계수$K_II$간에 일정한 상호작용이 존재한다는 것을 나타내었다. 또한, 모-드I과 모-드II의 임계응력확대계수(Critical stress intensity factor) $K_{IC}$와 $K_{IIC}$ 이용하여 혼합모-드파괴시의 $K_I$과 $K_II$간의 상호관계를 규정할 수 있었으며, 이미 보고된 여러 실험식과 본 실험결과를 비교하여 가장 적합한 관계로서 아래와 같은 관계를 얻을 수 있었다.