• Toxicological Research
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• v.29 no.2
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• pp.107-114
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• 2013

Mass spectrometry (MS) is a very powerful instrument that can be used to analyze a wide range of materials such as proteins, peptides, DNA, drugs, and polymers. The process typically involves either chemical or electron (impact) ionization of the analyte. The resulting charged species or fragment is subsequently identified by the detector. Usually, single mass uses source-induced dissociation (SID), whereas mass/mass uses collision-induced dissociation (CID) to analyze the chemical fragmentations Each technique has its own advantages and disadvantages. While CID is most effective for the analysis of pure substances, multiple-step MS is a powerful technique to get structural data. Analysis of veterinary drugs ampicillin, chloramphenicol, ciprofloxacin, and oxytetracycline serves to highlight the slight differences between SID and CID. For example, minor differences were observed between ciprofloxacin and oxytetracycline via SID or CID. However, distinct fragmentation patterns were observed for ampicllin depending on the analysis method. Both SID and CID showed similar fragmentation spectra but different signal intensities for chloramphenicol. There are several factors that can influence the fragmentation spectra, such as the collision energy, major precursor ion, electrospray mode (positive or negative), and sample homogeneity. Therefore, one must select a fragmentation method on an empirical and case-by-case basis.

• KOREAN JOURNAL OF PACKAGING SCIENCE & TECHNOLOGY
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• v.11 no.2
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• pp.91-96
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• 2005

Determination of safety factor of corrugated fiberboard boxes used for agricultural products is very complicated process due to nature of living products. Moisture content is one of the most critical factors to determine overall physical strength of paper, so its influences on strength properties of corrugated board made from different raw materials must be quantified. The results obtained from the study were summarized as follows; 1. Results show a detrimental effect on bursting strength and compressive strength of liners with increasing relative humidity of environment and moisture content of liners. 2. The relevance of equilibrium moisture content at varying relative humidity levels was proved and its relationship was used as an important factor to estimate box compression strength. 3. Test results was statistically used for establish the relationship between relative humidity and moisture content of liners. Estimated compression strength of boxes at varying moisture content was similar to results of theoretical equations such as Kellicutt's. Further study could be carried out in order to determine a optimum safety factors of various corrugated board boxes for agricultural products.

• Journal of Korea Technical Association of The Pulp and Paper Industry
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• v.48 no.3
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• pp.99-106
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• 2016

Our aim was to identify the potential of reed stalk as a raw materials for biomass pellet production. Compared to woody biomass, reed stalk contained significant levels of ash. The holocellulose content of reed stalk was similar to that of larch, but the lignin content of reed stalk was lower than that of larch. In the elemental analysis, chlorine content of reed stalk was much higher than that of larch, and satisfied only the mixed biomass pellet B of European non-woody pellet standards(EN 14961-6). In quantitative analysis of the ash, heavy metals contents of reed stalk satisfied European non-woody pellet standards. Higher heating value of oven-dried reed stalk pellet was slightly lower than that of larch wood pellet. The durability of reed stalk pellet was lower than that of larch wood pellet. The results of this study indicate that reed stalk might be used as a raw material of mixed biomass pellet B.

• Conservation Science in Museum
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• v.9
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• pp.51-58
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• 2008

Influence of lighting for exhibition normally used in museum on discoloration of relics and weakening of materials was reviewed, and influence of currently used lightings discoloration of dyed Korean paper similar to relic and change of material quality was directly tested. There were small differences in influence made on dyed Korean paper according to exhibition lighting, and based on these differences, method to select lighting safer for relics were explored. As a result of testing 4 types of fluorescent lamps, one lamp of them showed little influence on discoloration and change of material quality, which is judged to be proper for use in museum.

• Textile Coloration and Finishing
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• v.15 no.4
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• pp.32-38
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• 2003

To get the variety of color by natural dyeing, cotton and silk fabrics were dyed with natural indigo and safflower in turn. The two ways of dyeing processes were carried. First, silk and cotton fabrics were dyed repeatedly in safflower dyebath to five times to get the five fabrics dyed in different shades. And then indigo dyeing process was carried on the top of the dyed fabrics with safflower. In second way, the fabrics were dyed in five stages of shade by repetition of dyeing process in indigo dyebath. And then safflower dyeing was carried on the top of the dyed fabrics with indigo. When indigo dyeing process was added on the top of the fabrics dyed in five shades with safflower, the color differences decreased between five shades of fabrics, their color values got similar in hue, shade and chroma. When safflower dyeing process was added on the top of the fabrics dyed in five shades with indigo, the fabrics showed different hue of colors between red and blue of Munsell color circle such as RP, P and PB. Like almost of fabrics dyed with plants materials, the lightfastness and laundering fastness of dyed samples were poet and drycleaning fastness were good.

• Biotechnology and Bioprocess Engineering:BBE
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• v.6 no.4
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• pp.274-278
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• 2001

Polymer membranes composed of N, N-dimethylaminoethyl methaccrylate(DMAEMA) and acrylamide(AAm)(or ethyl acrylamide(EAAm) were prepared to demonstrated the thermo-control of solute permeation. Poly DMEMA has a lower critical solution temperature(LCST) at around 50$\^{C}$ in water, With the copolymerization of DMAEMA with AAm (or EAAm) a shift in the LCST to a lowere temperature was observed, probably due to the formation of hydrogen bonds between the amide and N-N-dimethylamino groups. However, the temperature-induced phase transition of poly(DMAEMA-co-EAAm) did not show a similar trend to that of poly(DMAEMA- co-AAm) in the gel state. The hydrogen bonds in poly(DMAEMA-co-EAAm) were significantly disrupted with the formation a gel network, which led to a difference in the swilling behavior of polymer gels in response to temperature. To apply these polymers to temperature-sensitive sol-ute permeation, polymer membranes were prepared. The permeation pattern of hydrocortisone, used as the model solute, was explained based on the temperature-sensitive swelling behavior of the polymer membranes.

• Journal of the Korean Society of Tobacco Science
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• v.10 no.1
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• pp.83-91
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• 1988

The effects of tipping paper permeability and plugwrap porosity on the ventilation and the pressure drop of cigarettes have been studied and the results obtained were as follows. 1. The single and the multiple regression equation to estimate tip ventilation were establised. In the equations, the observed values of the tip ventilation with the varieties the plugwrap porosity were content with them by the single regression equation. 2. As based on the statistical consideration of the above equation, the deviation of the observed tip ventilation versus the tipping paper permeability were higher than them to the plugwrap porosity. 3. The regression equations to calculate pressure drop ratio and the total ventilation rate in filter tip from the tea ventilation were obtained. According to the equation, the observed values of the pressure drop ratio were significantly similar to them calculated. 4. It was found that the equations could be applied to the calculation of the ventilation of cigarettes using the mechanical and micro laser perforation tipping paper as well as the electrically perforated tipping paper of this Study.

• Journal of the Korean Ceramic Society
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• v.48 no.4
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• pp.263-268
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• 2011

ZnO hexagonal rods grown in aqueous solution can be changed into a tubular shape by two-step aging in the course of the growing process. In the first step, hexagonal ZnO rods is grown by aging at $90^{\circ}C$ under a highly supersaturated aqueous solution giving rise to a fast precipitation rate. Meanwhile, during the second step aging at $60^{\circ}C$ in the same aqueous solution, the hexagonal polar face (001) having higher surface energy than (010) side planes dissolves to minimize surface energy. Hence the flat (001) face changes to a craterlike face and the hexagonal rod length of ZnO decreases at an initial-stage of this step aging. The formation of the (101) wedge-type faces is ascribed to the resultant of competitive reactions between the dissolution of polar face minimizing the surface energy which is a dominant reaction at the initial stage and the precipitation reaction dissipating supersaturation. At a later stage of the second-step the reaction rates of these two processes in the aqueous solution become similar and the overall reaction is terminated.

• Proceedings of the Korea Concrete Institute Conference
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• 1994.10a
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• pp.99-104
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• 1994

Recently, nonlinear fracture mechanics was applied to analyze concrete structures more accurately, and new materials property such as fracture energy(Gf) was used for its application. The fracture energy was influenced by many parameters, especially the strength of concrete. Many researches on the relation between the strength of concrete and the fracture energy were performed. In spite of many researches on the relation between the strength of concrete and the fracture energy, there is no distinct conclusion. This research includes various the strength levels from low-strength of concrete to high-strength, and then intends to estimate relation between the strength of concrete and the fracture energy. Concrete used crushed sand is also included, which is going to be used much. In this research, the wedge splitting test method proposed by Prof. Linsbauer is adopted to investigate the fracture energy. Fracture behavior of concrete used natrual sand and crushed sand has the similar trend. In the strength range of 200~500 kg/$\textrm{cm}^2$, the fracture energy and the maximum splitting forces(F) increase as the strength of concrete increases. In the range of the higher strength, however, the maximum splitting forces(F) increases but the fracture energy decreases as the strength of concrete increases. Through this investigation the fracture energy of concrete was not proportional to the strength of concrete.

• Journal of Korean Foot and Ankle Society
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• v.24 no.2
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• pp.94-97
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• 2020

Purpose: Fatigue breakage of cortical screws sometimes occurs after syndesmosis fixation, regardless of the period of screw retention. This study compared the fatigue strength of a novel screw design to conventional cortical screws in the fixed state of syndesmosis. Materials and Methods: Twelve sawbone models were tested mechanically to determine the fatigue strength of three screw designs. The first group was composed of cortical screws, while the second and third groups were newly-designed screws. The second group was composed of screws with a 2.4-mm diameter thread-free portion of the mid-shank while the third group had a 2.0-mm diameter thread-free mid-shank. A 400 N load was applied repetitively to a fibula model and the number of cycles until screw failure was recorded. Four screws from each group were tested, giving a total of 12 fatigue tests. Results: The average cycles until screw failure for groups 1, 2, and 3 were 8,134, 63,186, and 2,581, respectively. The second group showed the highest fatigue strength (p=0.018). The other two screw designs showed similar fatigue strength (p=0.401). Conclusion: New screw designs with a thread-free portion in the mid-shank could reduce the occurrence of fatigue breakage after syndesmosis fixation.