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A Study on Tribological Characteristics of DLC Films Considering Hardness of Mating Materials (상대 재료의 경도를 고려한 DLC필름의 트라이볼로지 특성)

  • Na, Byeong-Cheol;Tanaka, Akihiro
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.26 no.2
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    • pp.260-266
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    • 2002
  • DLC films were deposited on Si wafer by RF plasma assisted CVD using CH4 gas. Tribological tests were conducted using rotating type ball on disk friction tester in dry air. Four kinds of mating balls were used. The mating balls were made with stainless steel but apply different annealing conditions to achieve different hardness conditions. Testing results in all load conditions showed that the harder the mating materials, the lower the friction coefficient among the three kind of martensite mating balls. In case of austenite balls, the friction coefficients were lower than fully annealed martensite ball. The high friction coefficient in soft martensite balls seems to be caused by the larger contact area between DLC film and ball. The wear tracks of DLC films and mating balls could have proven that effect. Measuring the wear track of both DLC films and mating balls have similar tendency comparing to the results of friction coefficients. Wear rate of austenite balls were also smaller than that of fully annealed martensite ball. The results of effect of applying load showed, the friction coefficients were become decrease when the applying loads exceed critical load conditions. The wear track of mating balls showed that some material transfer occurs from DLC film to mating ball during the high friction process. Raman spectra analysis showed that transferred material was a kind of graphite and contact surface of DLC film seems to undergo phase transition from carbon to graphite during the high friction process.

An Analysis on the Competence and the Methods of Problem Solving of Children at the Before of School Age in Four Operations Word Problems (학령 전 아이들의 사칙연산 문장제 해결 능력과 방법 분석)

  • Lee, Dae-Hyun
    • Journal of the Korean School Mathematics Society
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    • v.13 no.3
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    • pp.381-395
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    • 2010
  • The purpose of this paper is to examine the competence and the methods of problem solving in four operations word problems based on the informal knowledges by five-year-old children. The numbers which are contained in problems consist of the numbers bigger than 5 and smaller than 10. The subjects were 21 five-year-old children who didn't learn four operations. The interview with observation was used in this research. Researcher gave the various materials to children and permitted to use them for problem solving. And researcher read the word problems to children and children solved the problems. The results are as follows: five-year-old children have the competence of problem solving in four operations word problems. They used mental computation or counting all materials strategy in addition problem. The methods of problem solving were similar to that of addition in subtraction, multiplication and division, but the rate of success was different. Children performed poor1y in division word problems. According to this research, we know that kindergarten educators should be interested in children's informal knowledges of four operations including shapes, patterns, statistics and probability. For this, it is needed to developed the curriculum and programs for informal mathematical experiences.

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A Study on the Shear Characteristics of Adhesives in Primary Mirror Supports of Satellite Camera (인공위성 카메라 주반사경 지지부에 적용되는 접착제의 전단 특성 연구)

  • Kim, Hyun-Jung;Seo, Yu-Deok;Park, Sang-Hoon;Youn, Sung-Kie;Lee, Seung-Hoon;Lee, Deog-Gyu;Lee, Eung-Shik
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.31 no.7 s.262
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    • pp.808-815
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    • 2007
  • The optical performance of the mirror fur satellite camera is highly dependent on the adhesive properties between the mirror and its support. Therefore, in order to design a mirror with high optical performance, the mechanical properties of adhesives should be well defined. In this research, the mechanical properties of three kinds of space adhesives are studied. In case of the materials which show nearly incompressible behavior such as space adhesives, it is important to measure shear modulus which governs deviatoric stress components. Also the experiment should be performed in circumstances similar to real manufacturing process of mirror, because extra factors such as size effects, the adhesion effects of primer and reactions between adhesive and primer affect the properties of adhesive regions. In this research shear moduli of the adhesives are determined by using a single lap adhesively bonded joint. For the shear tests, several temperatures have been selected from $-20^{\circ}C$ to $55^{\circ}C$ which is operating temperature range of the adhesive. In the case of linear behavior materials, shear moduli are calculated through a linear curve fitting. Shear stress-strain relation is obtained by using an exponential curve fitting for material which shows non-linear behavior. The shear modulus of each adhesive is expressed as a function of temperature. Characteristics and adaptability of the adhesives are discussed regarding their temperature sensitivity.

Engineering Properties of Red Shale and Black Shale of the Daegu Area, Korea (대구지역 적색 셰일과 흑색 셰일의 공학적 특성)

  • Kwag, Seong-Min;Jung, Yong-Wook;Kim, Gyo-Won
    • The Journal of Engineering Geology
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    • v.23 no.4
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    • pp.341-352
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    • 2013
  • The physical and mechanical properties of red shale and black shale exposed in the Daegu area were investigated in tests conducted to determine unit weight, absorption ratio, porosity, ultrasonic velocity, unconfined compressive strength, point load strength, slake durability index, and deterioration characteristics. XRD, XRF, and SEM analyses were also performed on the shale specimens. While the unit weights of the two shales were similar, the absorption ratio and porosity were higher in the red shale than in the black shale. Despite the higher porosity of the red shale, the ultrasonic velocity, compressive strength, and point load strength were higher in the red shale, which is an unexpected result that may be due to the presence of fine laminations in the black shale. The deterioration rate, as determined from the point load strength and the slake durability index, increased with increasing immersion time and with the acidity of the immersion liquid. The deterioration rate was higher for the red shale than for the black shale because of the higher porosity of the former.

Petrology of the Igneous Rocks in the Goseong area, Gyeongsang Basin II. Trace Element Geochemistry and Rb-Sr Radiometric Age (경상분지 고성지역의 화성암류에 대한 암석학적 연구 II. 미량원소 지구화학과 Rb-Sr 방사성 연대)

  • Jwa, Yong-Joo
    • Economic and Environmental Geology
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    • v.31 no.6
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    • pp.473-483
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    • 1998
  • The igneous rocks in the Goseong area are composed of the volcanic rocks (andesitic lapilli tuff and rhyodacite), Bulgugsa granites (Hornblende-biotite granite and two pyroxene granite) and intrusive andesites. In the variation diagrams of the trace and rare earth element contents and elemental ratios as well as the REE patterns, the three igneous rock types show different variational trends and patterns. The geochemical features represent that the igneous rocks in the area were formed from three different magmatic pulses. Two independently carried out Rb-Sr isotope experiments for the Goseong granites show that the whole rock ages and Sr initial ratios of the granites are $66.4{\pm}6.2Ma$, $0.70517{\pm}22(2{\sigma})$ and $71.3{\pm}6.8Ma$, $0.70506{\pm}18(2{\sigma})$, respectively. These results suggest that the granites magma originated from the lower crustal materials of igneous origin intruded into the area during the late Cretaceous period. Masan hornblende-biotite granite emplaced at the vicinity of the Goseong area is very similar to the Goseong granite in its mineral compositions, major, trace and rare earth element contents and patterns. The intruding age (100 Ma) of the Masan granite is order than that of the Geseong granite, however. The similarity of the geochemical natures but the contrast of the intruding ages between the Masan and Goseong granites possibly indicate that the magma generation from the same source materials occurred at a temporal interval of ca. 30 Ma.

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The Effects of Health Education on Treatment Compliance of Patients with High Blood Pressure and Diabetes in Private Clinics (개인 의료기관에 내원한 고혈압 및 당뇨병환자에게 실시한 건강교육이 치료 순응도에 미치는 영향)

  • Lee, Tae-Yong;Kim, Kwang-Hwan
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.10 no.2
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    • pp.425-431
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    • 2009
  • To provide fundamental educational materials for the effective management of patients with high blood pressure and diabetes in korea, and to expand the scope of such educational businesses the survey was administered between September 2007 and February 2008 to 1,213 consenting patients suffering from high blood pressure and diabetes in private medical centers within Daejeon in Korea. The patients were provided with standardized education materials and were monitored whether they were conducting a controlled management of their blood pressure and diabetes level as well as monitoring changes in their daily routine. Out of the 1,213 patients, 51.3% of the patients suffered only from high blood pressure, 26.3% suffered only from diabetes and 22.4% suffered from both high blood pressure and diabetes (Condor difference was not considered in this research). Physical education was the most commonly used education upon visitation to these medical centers, which was then followed by eating habits and weight management, respectively. The education demanded and preferred from the patients was similar to the education provided during the visitations. 56.7% of the medical doctors responded that the majority of the patients were passive in controlling and managing their illnesses. 63.7% of the participants believed that the education provided through this research was effective.

Surface Topography and Photoluminescence of Chemically Etched Porous Si (화학식각법에 의해 형성된 다공질실리콘의 표면형상 및 발광특성)

  • Kim, Hyeon-Su;Min, Seok-Gi
    • Korean Journal of Materials Research
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    • v.4 no.4
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    • pp.379-384
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    • 1994
  • Room-temperature photoluminescent porous Si has been formed by etching Si wafer u-ith the solution of $HF:HNO_{3}: H_{2}O$=l : 5 : 10. We have observed photoluminescence(PL) spectra similar to those reported recently for porous-Si films formed by anodic etching with HF solutions. We have also investigated the dependence of PI, spectra on the etching time which was varied from 1 to 10 minutes. We found that 5-minute etching gave us the strongest PL intensity. We also found by atomic force microscopy( AFM) measurements that the surface fearure size became smaller for longer etching time and the average feature size of the etched Si wafer for 5-minute was about 1, 500~2, 000$\AA$. This indicates that the surface feature of the etched porous Si affects the PL intensity of the sample.

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A Study of the Bezel Settings of a JinjuseonUsed for Joseon Royal Weddings Based on an Examination of the Washers (제조선시대 궁중혼례용 '진주선(眞珠扇)'의 받침못을 통해 본 감장(嵌裝) 기법 고찰)

  • Sim, Myung Bo;Kim, Sun Young
    • Conservation Science in Museum
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    • v.21
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    • pp.17-28
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    • 2019
  • The term jinjuseon(眞珠扇), meaning literally a pearl fan, refers to a fan decorated with precious stones for use in royal wedding ceremonies. This study examined a jinjuseon housed in the National Palace Museum of Korea (NPMK) which currently lacks jeweled ornaments. In order to determine whether pearls or other gemstone settings originally ornamented the fan,the surface and composition of the gray materials remaining on the washers were investigated and the fan was compared with other artifacts decorated using similar techniques. The analysis revealed that the gray materials visible around the round rims of the washers contain tin-lead alloys. The traces of folded nails suggest that soldering was not applied. The remains of the infill observed in other artifacts with bezel settings indicate that this jinjuseon in the NPMK collection was produced using abezel setting technique wherein pearls or other gemstones were affixed by filling cylindrical bezels with tin-lead alloys.

Finite Element Simulation and Experimental Study on the Electrochemical Etching Process for Fabrication of Micro Metal Mold (미세금형 가공을 위한 전기화학식각 공정의 유한요소 해석 및 실험결과 비교)

  • Ryu, Heon-Yul;Im, Hyeon-Seung;Cho, Si-Hyeong;Hwang, Byeong-Jun;Lee, Sung-Ho;Park, Jin-Goo
    • Korean Journal of Materials Research
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    • v.22 no.9
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    • pp.482-488
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    • 2012
  • To fabricate a precise micro metal mold, the electrochemical etching process has been researched. We investigated the electrochemical etching process numerically and experimentally to determine the etching tendency of the process, focusing on the current density, which is a major parameter of the process. The finite element method, a kind of numerical analysis, was used to determine the current density distribution on the workpiece. Stainless steel(SS304) substrate with various sized square and circular array patterns as an anode and copper(Cu) plate as a cathode were used for the electrochemical experiments. A mixture of $H_2SO_4$, $H_3PO_4$, and DIW was used as an electrolyte. In this paper, comparison of the results from the experiment and the numerical simulation is presented, including the current density distribution and line profile from the simulation, and the etching profile and surface morphology from the experiment. Etching profile and surface morphology were characterized using a 3D-profiler and FE-SEM measurement. From a comparison of the data, it was confirmed that the current density distribution and the line profile of the simulation were similar to the surface morphology and the etching profile of the experiment, respectively. The current density is more concentrated at the vertex of the square pattern and circumference of the circular pattern. And, the depth of the etched area is proportional to the current density.

Effects of Surface Oxide Film on Massive Hydriding of Zr Alloy (지르코늄 합금의 대량수소화에 미치는 표면산화막의 영향)

  • Kim, Sun-Ki;Bang, Je-Geon;Kim, Dae-Ho;Lim, Ik-Sung;Yang, Yong-Sik;Song, Kun-Woo;Kim, Yong-Soo
    • Korean Journal of Materials Research
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    • v.18 no.11
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    • pp.597-603
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    • 2008
  • Oxide effects experiments on massive hydriding reactions of Zr alloy with hydrogen gas were carried out at $400^{\circ}C$ under 1 atm in a $H_2$ environment with a thermo-gravimetric apparatus (TGA). Experimental results for oxide effects on massive hydriding kinetics show that incubation time is not proportional to oxide thickness. The results also show that the massive hydriding kinetics of pre-filmed Zr alloys follows linear kinetic law and that the hydriding rates are similar to that of oxide-free Zr alloys once massive hydriding is initiated. Unlikely microstructure of the oxide during incubation time, physical defects such as micro-cracks and pores were observed in the oxide after incubation time. Therefore, it seems that the massive hydriding of Zr alloys can be ascribed to short circuit paths and mechanical or physical defects, such as micro-cracks and pores in the oxide, rather than to hydrogen diffusion through the oxide resulting from the increase of oxygen vacancies in the hypo-stoichiometric oxide.