• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 2010.06a
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• pp.56-56
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• 2010

Single-walled carbon nanotubes (SWCNTs) have attracted much attention as a promising material for transparent conducting films (TCFs), due to their superior electrical conductivity, high mechanical strength, and complete flexibility as well as their one-dimensional morphological features of extremely high length-to-diameter ratios. This study investigated three kinds of SWCNTs with different purities: as-produced SWCNTs (AP-SWCNTs), thermally purified SWCNTs (TH-SWCNTs), thermally and acid purified SWCNTs (TA-SWCNTs). The purity of each SWCNT sample was assessed by considering absorption peaks in the semiconducting ($S_{22}$) and metallic ($M_{11}$) tubes with UV-Vis NIR spectroscopy and a metal content with thermogravimetric analysis (TGA). The purity increased as proceeding the purification stages from the AP-SWCNTs through the thermal purification to the acid purification. The samples containing different contents of SWCNTs were dispersed in water using sodium dodecyl benzensulfate (SDBS). Aqueous suspensions of different purities of SWCNTs were prepared to have similar absorbances in UV-Vis absorption measurements so that one can make the TCFs possess similar optical transmittances irrespective of the SWCNT purity. Transparent conductive SWCNT networks were formed by spraying an SWCNT suspension onto a poly(ethyleneterephthalate) (PET) substrate. As expected, the TCFs fabricated with AP-SWCNTs showed very high sheet resistances. Interestingly, the TH-SWCNTs gave lower sheet resistances to the TFCs than the TA-SWCNTs although the latter was of higher purity in the SWCNT content than the former. The TA-SWCNTs would be shortened in length and be more bundled by the acid purification, relative to the TH-SWCNTs. For both purified (TH, TA) samples, the subsequent nitric acid ($HNO_3$) treatment greatly lowered the sheet resistances of the TCFs, but almost eliminated the difference of sheet resistances between them. This seems to be because the electrical conductivity increased not only due to further removal of surfactants but also due to p-type doping upon the acid treatment. The doping effect was likely to overwhelm the effect of surfactant removal. Although the nitric acid treatment resulted in the similar. electrical properties to the two samples, the TCFs of TH-SWCNTs showed much lower sheet resistances than those of the TA-SWCNTs prior to the acid treatment.

• Journal of radiological science and technology
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• v.33 no.3
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• pp.245-252
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• 2010

This study analyzed speed of sound, impedance, attenuation coefficient in accordance with acoustic characteristic standard of body soft tissue corresponding with Annex DD of IEC standard 60601-2-37(2007) which is about tissue mimicking materials (TMM) synthesized by polyurethane as a main material and new type of n-type scatter materials. This study reached the following conclusion after analyzing and evaluating image characteristic with SONOACE 9900 c PRIME (MEDESON Co.) and brightness, maximum penetration with convex probe (2.5~5.0 MHz). When n-type scatter materials are increasingly synthesised 0~8% with prepolymer as a main material and polyol mixture as a catalyst, 1. The more scatter materials are increased, the more sound speed of TMM becomes closely similar to soft tissue. 2. The more scatter materials are decreased, the more acoustic impedance becomes closely similar to soft tissue. 3. The more scatter materials are increased, the more attenuation coefficient is increased. 4. The more scatter materials are increased, the more average brightness of images is increased, but there is threshold. 5. The maximum penetration becomes closely similar to soft tissue at the 6% TMM as a scatter material.

• Journal of the Korean Society of Safety
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• v.27 no.4
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• pp.7-12
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• 2012

In this study, the solidification characteristics inside the AC7A casting material was analyzed using the numerical analysis method and was verified using the experimental method by the pre-heated temperature conditions of metal casting device. For the numerical analysis, "COMSOL Multiphysics", the commercial code based on the finite element analysis(FEA), was used in order to predict the thermal deformation of the AC7A casting material including temperature, displacement and stress distribution. Also, in order to verify the results calculated by the numerical analysis, the experiment for temperature measurement inside the AC7A casting material was performed using the K-type thermocouple under the same condition of numerical analysis method. In the numerical results, thermal deformation inside AC7A casting material was well-suited for manufacturing products when the pre-heated temperatures of the metal casting device was $250^{\circ}C$. When the results of the temperature distribution were experimentally measured and were compared with those of the numerical result, it appeared that there was some temperature difference because of the latent heat by phase change heat transfer. However, the result of cooling temperature and patterns were almost similar except for the latent heat interval. The solidification characteristics was closely related to the temperature difference between the surface and inside of the casting.

• Geomechanics and Engineering
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• v.22 no.6
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• pp.541-552
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• 2020

With the increasing tension of current coal resources and the increasing depth of coal mining, the gob-side entry retaining technology has become a preferred coal mining method in underground coal mines. Among them, the technology of the gob-side entry retaining with the high-water filling material can not only improve the recovery rate of coal resources, but also reduce the amount of roadway excavation. In this paper, based on the characteristics of the high-water filling material, the technological process of gob-side entry retaining with the high-water filling material is introduced. The early and late stress states of the filling body formed by the high-water filling materials are analyzed and studied. Taking the 8th floor No.3 working face of Xin'an coal mine as engineering background, the stress and displacement of surrounding rock of roadway with different filling body width are analyzed through the FLAC^3D numerical simulation software. As the filling body width increases, the supporting ability of the filling body increases and the deformation of the surrounding rock decreases. According to the theoretical calculation and numerical simulation of the filling body width, the filling body width is finally determined to be 3.5m. Through the field observation, the deformation of the surrounding rock of the roadway is within the reasonable range. It is concluded that the gob-side entry retaining with the high-water filling material can control the deformation of the surrounding rock, which provides a reference for gob-side entry retaining technology with similar geological conditions.

• Journal of Welding and Joining
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• v.10 no.4
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• pp.230-239
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• 1992

The specimens of two base metals and material friction-welded with hetrogeneous steels of SM40C and STS304 have been prepared and the characteristics of rupture and crack propagation of them have been examined. In the friction-welded material, the width of HAZ is 3.0mm for STS304 and 3.4mm for SM40C. The hardness distribution in HAZ of SM40C is decreased gradually as being getting off interface, but that in HAZ of STS304 is decreased remarkedly and the value of hardness becomes a little lower than that of the base metal in region of 1mm from interface and becomes a little higher than that of the base metal. The tensile strength of the friction-welded material appeared a little lower than that of the base metal and rupture by tensile load is developed in HAZ of STS304 and the position of rupture is at region of low hardness(1mm from interface). The crack propagation rates(da/dN) in both HAZ of the friction-welded material are a little higher than those in both base metals, but the difference are less except for the case of SM45C in low .DELTA. K value. It has been ascertained that the crack in the interface propagates selectively along the HAZ of SM40C and consequently the crack propagation rate is almost similar to that in the HAZ of SM40C.

• Journal of the Korea Institute of Building Construction
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• v.16 no.6
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• pp.529-534
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• 2016

Calcium silicate inorganic insulating material is a porous material which is made of 90 wt% of cement. Unlike existing inorganic insulation materials, it is produced without high temperature curing process and also it costs much less than existing inorganic insulation materials. It is an innovative insulation material that supplemented disadvantages of conventional inorganic insulation material. Researches and developments about inorganic insulation materials have been actively researched abroad. Calcium silicate insulation has $0.13g/cm^3$ of specific gravity. Its heat conductivity is under 0.050W/mK, which it similar to conventional inorganic insulation. However, it has weak compressive strength compared to other inorganic insulation. The point of this research is to manifest that calcium silicate inorganic insulating material can have certain compressive strength after curing process with high insulating performance and to find out the proper curing methods and period.

• Journal of the Korean Institute of Electrical and Electronic Material Engineers
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• v.22 no.10
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• pp.890-896
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• 2009

Li(Ni, Co, Mn)$O_2$ has been known as one of the most promising cathode materials for lithium secondary batteries. However, it has some problems to overcome for commercialization such as inferior rate capability and unstable thermal stability. In order to address these problems, surface modification of cathode materials by coating has been investigated. In the coating techniques, selection of coating material is a key factor of obtaining enhanced properties of cathode materials. In this work, we introduced solid electrolyte (Li-La-Ti-O) as a coating material on the surface of $Li[Ni_{0.3}Co_{0.4}Mn_{0.3}]O_2$ cathode. Specially, we focused on a rate performance of Li-La-Ti-O coated $Li[Ni_{0.3}Co_{0.4}Mn_{0.3}]O_2$ cathode. Both bare and Li-La-Ti-O 2 wt.% coated sample showed similar discharge capacity at 0.5C rate. However, as the increase of charge-discharge rate to 3C, the coated samples displayed better discharge capacity and cyclic performance than those of bare sample.

• Tunnel and Underground Space
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• v.17 no.3 s.68
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• pp.175-185
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• 2007

When filling material such as clay is included along the discontinuity, it may cause instability on a slope even if the direction of discontinuity works in a positive way. In the study area, slope sliding occurred at the boundary between a clay filling material and weathered soil because the physical properties differ across the boundary; and this is very similar to the situation where foliation in a rock works as a weak zone during a structural behavior, causing an inter-layer slip. In most analysis, if there exists a clay filling material, a single discontinuity is assumed to perform analysis. In those cases, the discontinuity is modeled as a slip surface within clay. Therefore, the characteristics of the boundary are not considered in the analysis, so that ultimately the physical property of clay usually prevails. The result of evaluating the slope stability affected by clay filling material shows the significant difference in the safety level due to the strength parameter depending on the failure type of the discontinuity by a filling material.

• Restorative Dentistry and Endodontics
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• v.44 no.2
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• pp.18.1-18.9
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• 2019

Objective: This study evaluated the presence of residual root canal filling material after retreatment using micro-computed tomography (micro-CT). Materials and Methods: Extracted human teeth (single- and double-rooted, n = 21/each; C-shaped, n = 15) were prepared with ProFile and randomly assigned to three subgroups for obturation with gutta-percha and three different sealers (EndoSeal MTA, EndoSequence BC sealer, and AH Plus). After 10 days, the filling material was removed and the root canals were instrumented one size up from the previous master apical file size. The teeth were scanned using micro-CT before and after retreatment. The percentage of remaining filling material after retreatment was calculated at the coronal, middle, and apical thirds. Data were analyzed using the Kruskal-Wallis test and Mann-Whitney U test with Bonferroni post hoc correction. Results: The tested sealers showed no significant differences in the percentage of remaining filling material in single- and double-rooted teeth, although EndoSeal MTA showed the highest value in C-shaped roots (p < 0.05). The percentage of remaining filling material of AH Plus and EndoSeal MTA was significantly higher in C-shaped roots than in single- or double-roots (p < 0.05), while that of BC sealer was similar across all root types. EndoSeal MTA showed the highest values at the apical thirds of single- and double-roots (p < 0.05); otherwise, no significant differences were observed among the coronal, middle, and apical thirds. Conclusions: Within the limitations of this study, a large amount of EndoSeal MTA remained after retreatment, especially in C-shaped root canals.

• Coupled systems mechanics
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• v.10 no.6
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• pp.509-520
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• 2021

Fiber-reinforced concrete (FRC) is a composite material where small fibers made from steel or polypropylene or similar material are embedded into concrete matrix. In a material model each constituent should be adequately described, especially the interface between the matrix and fibers that is determined with the 'bond-slip' law. 'Bond-slip' law describes relation between the force in a fiber and its displacement. Bond-slip relation is usually obtained from tension laboratory experiments where a fiber is pulled out from a matrix (concrete) block. However, theoretically bond-slip relation could be determined from bending experiments since in bending the fibers in FRC get pulled-out from the concrete matrix. We have performed specially designed laboratory experiments of three-point beam bending with an intention of using experimental data for determination of material parameters. In addition, we have formulated simple layered model for description of the behavior of beams in the three-point bending test. It is not possible to use this 'forward' beam model for extraction of material parameters so an inverse model has been devised. This model is a basis for formulation of an inverse model that could be used for parameter extraction from laboratory tests. The key assumption in the developed inverse solution procedure is that some values in the formulation are known and comprised in the experimental data. The procedure includes measured data and its derivative, the formulation is nonlinear and solution is obtained from an iterative procedure. The proposed method is numerically validated in the example at the end of the paper and it is demonstrated that material parameters could be successfully recovered from measured data.