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The Physical Properties of UV-curable Resin for the Restoration of Glass Cultural Properties and Its Application in Conservation Treatment (유리제 문화재 복원용 광경화성 수지의 물성 연구 및 적용)

  • Lee, Hae Soon;Na, Ah Young
    • Conservation Science in Museum
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    • v.21
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    • pp.1-16
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    • 2019
  • This study investigated the material properties of UV-curable Resin in order to identify stable materials for use in the restoration of glass cultural properties. Tested samples were based on acrylic UV-curable Resin (SECURE CP-7321®), to which urethane UV-curable Resin (FLGPCL04 Clear®) was added in 10% increments to produce eleven samples. The results showed that all eleven samples had similar properties in terms of refractive index, density, adhesive strength, and anti-yellowing. But the surface hardness and compressive strength were optimal and effective for maintaining the shape of artifacts after restoration treatment when the proportion of urethane resin was in the range of 10-20%. Based on these findings, the mixing sample [acrylic UV-curable Resin(9) : urethane UV-curable Resin(1)] was applied in the conservation treatment of a glass cultural propertie (Hwangbuk 519) excavated from the North Mound of Hwangnamdaechong, Tomb in Gyeongju.

Reports of Drawida (Oligochaeta: Moniligastridae) from far East Asia

  • Blakemore, Robert J.;Lee, Seunghan;Seo, Hong-Yul
    • Journal of Species Research
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    • v.3 no.2
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    • pp.127-166
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    • 2014
  • Moniligastrids are an important yet often ignored earthworm group commonly found in cultivated soils, especially paddy, in the tropical East. Seven new taxa are: Drawida koreana austri, D. koreana nanjiro, D. koreana shindo, D. odaesan, D. jeombongsan, D. companio and D. csuzdii Blakemore spp. or sub-spp. nov. from Korea. Drawida csuzdii is the first new species from North Korea since Lumbricidae Eisenia koreana (Zicsi, 1972). Historical East Asian moniligastrids are reviewed chronologically and Drawida barwelli (Beddard, 1886), D. japonica (Michaelsen, 1892) and D. siemsseni Michaelsen, 1910 are compared on their museum types. These three taxa were thought similar and related to D. nepalensis Michaelsen, 1907 and its possible synonym D. burchardi Michaelsen, 1903 (priority!) and both of these to prior D. uniqua (Bourne, 1887). Indian Drawida calebi Gates, 1945 is compared to new material of D. japonica from Japan, and D. willsi Michaelsen, 1907 to the new sub-species of D. koreana Kobayashi, 1938 from Korea. Where available, mtDNA COI gene barcodes are provided to help objective determinations and a phylogram is provided with outgroup Ocnerodrilidae Eukerria saltensis (Beddard, 1895) itself found in rice paddy/irrigation. The challenge now is comparison of all early taxa in their various homelands in order to assess the genetic variability and taxonomic boundaries acceptable, especially for unpigmented D. barwelli and also for pink/grey D. japonica and blue/grey D. koreana. A checklist of moniligastrids is appended showing 22 species from China (including Hainan and Taiwan), 21 from Korea, nine from Japan and the Drawida ghilarovi Gates, 1969 species-complex from far eastern Russian (Siberia). Recent Drawida dandongensis Zhang & Sun, 2014 from Sino-Korean border is misdescribed and cannot be meaningfully compared to any other Drawidas.

Microstructure-Sound Absorption Relationships of Polyurethane Foam and Application of Low Monos Polyol (폴리우레탄 폼의 미세구조와 흡음 관계 밑 Low Monos 폴리올의 응용)

  • Lee, Boo-Youn;Kim, So-Yeon;Lee, Kwang-Hee;Jin, Byung-Suk
    • Polymer(Korea)
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    • v.31 no.4
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    • pp.289-296
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    • 2007
  • The material factors influencing the sound absorption of the polyurethane foam were investigated with FT-IR, small-angle X-ray scattering (SAXS), and dynamic mechanical thermal analyzer (DMTA). The measurements were performed using the samples which had a similar cell structure but different absorption coefficients. It was found that the ability of the sound absorption of the polyurethane foams was closely related to the damping behavior over the transition range. In order to confirm the use of the low monol polyol (LMP) in high-performance applications, the polyurethanes based on LMP and polypropylene oxide polyol (PPG) were prepared by the solution polymerization method. The microstructure and the physical properties of these polyurethanes were compared. The PPG-based polyurethane showed a higher level of the phase-separated structure because the considerable amount of monol presented in PPG made a contribution to the increased chain mobility. However the short chains formed due to the monol species deteriorated the damping property. As a result, the LMP-based polyurethane showed the superior damping behavior as compared with the PPG-based one.

MATURE INSTRUMENT, IMMATURE TECHNOLOGY : IS NIR ANALYSIS OF HIGH MOISTURE MATERIALS A SERIOUS PROPOSITION\ulcorner

  • Berding, Nils
    • Proceedings of the Korean Society of Near Infrared Spectroscopy Conference
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    • 2001.06a
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    • pp.3124-3124
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    • 2001
  • The development and evolution of near infra-red spectroscopic (NIS) calibrations for high-moisture materials is an expensive proposition. Such investment is suspect unless the instrument, or instruments, on which calibrations were developed can be preserved intact or re-standardized as component replacements occurs. The objective of this paper is to detail the changes in performance of a six-year old instrument after maintenance in years five and six resulted in collection of spectral data that was increasingly removed from the calibration population. Calibrations for the analysis of mature sugarcane stalks, a high-moisture material, were developed successfully in 1995 using a broad sample population in terms of genetics, and spectral and temporal variation. The spectral library was further broadened in 1996. In 1997, 1999, 1999, and 2000, additional samples constituting 10% of the laboratories throughput were subjected to full component analyses using routine laboratory techniques. These samples were primarily random samples, but were complemented with samples that were significant for the spectral H statistic or for the component t statistic. In 1998, an additional calibration was developed for populations consisting of samples of either mature stalks (culms) or sucker culms. Substantial additional samples numbers were collected for this calibration in 1999 and 2000. Attempts to standardize the scanning spectrophotometer used for these calibrations with a second similar instrument in 1999 failed because the instruments were optically different, and standardization could not account for this. Maintenance adjustments were made to the remote reflectance probe of the original instrument in 1999, and replacement of its PbS detectors was done in 2000. Spectral data collected in 1999 and 2000 yielded spectral populations that were increasingly removed from the respective spectral populations on which the calibrations were developed. The mature stalk calibrations benefited marginally from evolutionary calib.

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Compositional analysis by NIRS diode array instrumentation on forage harvesters

  • Andreashaeusler, Michael Rode;Christian, Paul
    • Proceedings of the Korean Society of Near Infrared Spectroscopy Conference
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    • 2001.06a
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    • pp.1619-1619
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    • 2001
  • Ourwork aims to assess the content of dry matter, protein, cell wall parameters and water soluble carbohydrates in forages without having to handle samples, transport them to a laboratory, dry, grind and chemically analyze them. for this purpose, the concept of fresh forage analysis under field conditions by means of compact integrated NIRS InGaAs-diode array instruments on small plot harvesters is being evaluated for plant breeding trials. This work was performed with the world first commercial experimental forage plot harvester equipped with a NIRS module for the collection, compression, and scanning of forage samples (including automatic referencing and dark current measure ments). It was used for harvesting and analyzing a number of typical forage grass and forage legume plot trials. After NIRS measurements in the field each sample was again analyzed in the laboratory by means of a conventional grating spectrometer equipped with Si-and PbS-detectors. Conventional laboratory analysis of the samples was restricted to dry matter (DM) content by means of oven drying at 105. Routine chemometric procedures were then employed to assess the comparative accuracy and precision of the DM assessments in the spectral range between 950 and 1650nm by the NIRS diode array as well as by the conventional NIRS scanning instrument. The results of this study confirmed that the type of NIRS diode array instrument employed here functioned well even in rugged field operations. further refinements proved to be necessary for optimizing the automatic filling of the sample compartment to adjust for the wide variation in forage material under conditions of extremely low or high harvest yields. The error achieved in calibrating the apparatus for forages of typical DM content proved to be satisfactory (SECV < 1.0). Possibly as a consequence of higher sampling errors, its performance in atypical forages with elevated DM contents was less satisfactory. The error level obtained on the conventional grating NIR spectrometer was similar to that of the diode array instrument for both types of forage.

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Thickness and translucency of opaque shade composite resin for masking effect (배경 색조 차단 목적의 불투명 복합 레진의 두께와 반투명도)

  • Baek, Kyung-Won;Kim, Sung-Joon
    • The Journal of the Korean dental association
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    • v.49 no.4
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    • pp.203-210
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    • 2011
  • The aims of this study were to evaluate the adequate thickness of opaque resins for situations such as an oral black cavity and discolored tooth structure, as well as the translucency of each opaque material at various thicknesses. Six opaque-shade composite resins (Z-350 OA3, Amelogen Universal A2O, Esthet-X A2O, Esthet-X A4O, Charmfil UO and Aelite Universal OA3) were prepared in metal molds with a hole of 8 mm in diameter and various thicknesses (0.5mm, 1.0mm, 1.5mm, 2.0mm, 2.5mm, 3.0 mm and 4.0mm). Four backgrounds (white tile, black tile, C4 shade porcelain and opaque resin itself) were used to determine the translucency parameter (between black and white backgrounds). and to mimic a black oral cavity (between black and opaque resin backgrounds) and a discolored tooth structure (between C4 and opaque resin backgrounds). Color measurements were made by a colorimeter to determine the CIELAB values of each specimen with each background and to calculate the translucency parameter and ${\Delta}E^*$ value difference among the specimens on the backgrounds. The translucency parameter and ${\Delta}E^*$ obtained between black and opaque resin backgrounds decreased in similar pattern as thickness increased. A C4 background was masked by resin thicknesses of 0.5-1.0mm, while a black background required thicknesses of 1.0-2.0mm. Adequate knowledge about differences in the optical character like translucency of the materials used is essential, together with the accumulated experience of the individual clinician.

The politic plan research for furniture industrial activation in the northern part of Gyeonggi-Province

  • Im, Kwang-Soon;Kim, Houn-Chul;Park, Byung-Dae
    • Journal of the Korea Furniture Society
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    • v.21 no.6
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    • pp.449-458
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    • 2010
  • This study attempted to investigate the effect of panel thickness on the horizontal density distribution (HDD) of medium density fiberboard (MDF) in a destructive way. Full size MDF panels with five different thicknesses such as 2 mm, 4.5 mm, 9 mm, 18 mm and 30 mm were cut into two different specimen sizes, i.e., $500{\times}500\;mm$ and $120{\times}120\;mm$ to measure the HDD. In general, the overall density of MDF panel diminished as the thickness increased, showing the highest density for the thinnest MDF panels. The HDD variation was significant for the samples of smaller specimen size ($120{\times}120\;mm$). MDF panel thickness significantly influenced to the HDD, which increased as the thickness decreased. In addition, the thinner panels showed much wider range in the HDD than those of thicker panels. The coefficient of variation (COV) of HDD also followed a similar trend to the panel density as the thickness increased. In summary, MDF panel thickness had a significant impact on the HDD within a panel. The sample size also showed a considerable effect to the HDD of MDF panels.

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Effects of Organic Mulches on the Quality of "Niitaka" Pear Trees and Fruit (유기질 멀칭이 배 '신고' 나무의 과실 품질에 미치는 영향)

  • Wu, Xiu-Yu;Kim, Wol-Soo;Choi, Hyun-Suk;Jo, Jung-An
    • Food Science and Preservation
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    • v.17 no.4
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    • pp.466-470
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    • 2010
  • We investigated the effects of organic mulches on the tree and fruit qualities of "Niitaka" (Pyrus pyriforia) pear trees. Trees grown with rice straw mulch had significantly greater potassium (K), magnesium (Mg), and calcium (Ca) concentrations in leaves compared with control trees and those mulched using bark or polyethylene, but the concentrations were below the recommended levels for these nutrients in pear leaves. Bark mulch increased fruit firmness and soluble solid (SS) levels, compared with rice straw mulch. The fruit of trees grown with bark mulch had a higher ratio of SS to total acidity in fresh fruit, and the fruit was dark red in color. The K and Ca concentrations were highest in fruit grown on trees mulched with rice straw and bark, respectively, and competition between the levels of these cations was evident in fresh fruit. Bark and rice straw mulches increased overall fruit quality, and reduced fruit stone size, whereas a polyethylene mulch, devoid of organic material, resulted in a fruit stone size similar to that of the control.

Effect of Extract Agrimonsa Pilosa L. on biological Activity in Rats (선학초(仙鶴草) 추출액이 흰쥐의 생리활성(生理活性)에 미치는 효과)

  • Lee, Yong-Ho;Kim, Man-Bae;Chung, Dae-Soo
    • Korean Journal of Medicinal Crop Science
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    • v.10 no.3
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    • pp.167-170
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    • 2002
  • Agromonia pilosa L. has been used as a medicinal plant in traditional folk remedy, and it shows increasing tendency at various sections such as medicine-making material, functional food, and agricultural chemicals using plant or extract. Dosage effect of extract from Agrimonia pilosa L. plant on rat performance experiments were summarized as follows : Body weight was increased with 0.02% dosage treated-rat by 5% as compared to non-treated one, however, decreasing tendency was observed with 0.04% extract of Agrimonia pilosa L. plant fed rat to control Considering feed efficiency was similar result between extract dosage with 0.02% and non-treated rat. The number of leucocyte was increased by dosage-treated level except 0.02% dosage-treated rat. Number of erythrocyte was increased with 0.06% extract dosage-treated rat by 20% as compared to non-treated one.

Geochemical characteristics of Ogcheon granite in Ogcheon area (옥천화강암의 지구화학적 특성)

  • 윤현수;김대업;박석환
    • The Journal of the Petrological Society of Korea
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    • v.8 no.2
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    • pp.81-91
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    • 1999
  • The area of the study is located in Ogcheon district, middle part of Ogcheon Fold Belt. The area is covered by metasedimentary rocks of Ogcheon Supergroup at northern, eastern and southern part. Jurassic Ogcheon granite which intruded into Ogcheon Supergroup at central part, was intruded by Cretaceous quartz porphyry at western part. The granite consists of quartz, plagioclase, alkali feldspar, biotite, sphene, apatite, epidote, opaque and so on. It is generally characterized by grey to light grey, medium-grained, mafic enclave and partly weak foliation. In terms of geochmical compositions, the granite is felsic, peraluminous, subalkaline and calc-alkaline, and it was differentiated from single granitic magma. It shows parallel LREE enrichment and HREE depletion patterns with 0.84 Eu negative anomaly, which has REE variation trend and anomaly value similar to Jurassic granites in Korea. From charactristics of petrology, mineralogy and geochmistry, it may be interpreted that the Ogcheon granite body was derived from melting of I-type crustal material related to syn-collisional tectonic setting and emplaced more or less rapidly into the Ogcheon Supergroup.

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