• Title/Summary/Keyword: silver powder

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Study for the Film Coating Techniqur of Gilt Bronze Artifacts from Mir ksa Temple (미륵사지 출토 고대 금동유물의도금기법에 관한 연구)

  • Lim, Sun-Ki;Kang, Dai-Ill;Kim, Sun-Dug;Park, Dong-Kyu;Kang, Sung-Goon
    • 보존과학연구
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    • s.14
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    • pp.45-76
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    • 1993
  • Au-Cu alloyed coating layer were found by Hg-amalgam process and it seemed to be used Cu-amalgam process similar to Au-amalgam. Coated layer is dense and unique, Thickness of layer was 1.5 to $18.0\mum$ which had 95.3 to 99.8% purity of gold Matrix metal mostly cosists of forged copper alloy which had high purity and ferrite ($\alpha$) strusture. It showed excellent refining technical level at that time. Aowever, the nail, ferrous matrix used for strength needed, composed of silver foil packed and gold layer for adherence between ferrous matrix and gold layer

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Synthesis of Ag-Pd Alloy Nanoparticles by Chemical Reduction Method (화학환원법을 이용한 Ag-Pd 합금 나노분말의 합성)

  • Seo, Won-Sik;Kim, Yun-Do;Choung, Il-Yeop;Lee, Ho-Seok;Song, Ki-Chang
    • Journal of the Korean Ceramic Society
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    • v.43 no.4 s.287
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    • pp.224-229
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    • 2006
  • Ag-Pd alloy nanoparticles were prepared by a chemical reduction method using hydrazine $(N_2H_4)$ as a reductant in $AgNO_3\;and\;Pd(NO_3)_2$ aqueous solutions. Characterization of these particles by X-ray powder diffraction revealed a bimetallic and crystalline silver-palladium alloy. The average size of the particles was influenced not by the reductant $(N_2H_4)$ concentration, but the concentration of the starting materials $(AgNO_3\;and\;Pd(NO_3)_2)$.

Effect of Metal Powders on the Conductivity of Conductive Inks (금속입자가 전도성 잉크의 전도도에 미치는 영향)

  • Kwon, Doo-Hyo;Jeong, Tae-Eui;Kim, Nam-Soo;Han, Kenneth-N.
    • Transactions of the Korean Society of Machine Tool Engineers
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    • v.17 no.2
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    • pp.97-103
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    • 2008
  • In this investigation, conductivity of conductive inks was measured. A particular attention has been given to the effect of metal powders with various conductivity on the overall conductivity of the bulk ink. The conductivity of various solutions simulating conductive inks consisting of copper and silver was measured and the results have been discussed in relation to various applications of conductive inks in practice. A conductivity model simulating systems consisting of various materials has been introduced and the results were discussed. Materials of good conductivity are adversely affected by mixing with materials of poor conductivity simply through serial connection. However, parallel connection has rather little effect on the overall conductivity. The practical implication of various mixtures of materials on conductive inks has been discussed.

Electrophoretic Deposition of YBCO powder in mixed suspension solution of iso-prophanol and iso-buthanol (이소프로판올과 이소부탄을 용매에서의 YBCO 분말 영동전착)

  • ;;;Korobova N.
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2001.11a
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    • pp.288-291
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    • 2001
  • It is very important to select suspension solution for forming electrophoretic deposited YBCO thick film, because it is heavily affected to its superconducting properties. In this paper, high-temperature superconductor films of YBa$_2$Cu$_3$$O_{7-x}$ were fabricated by electrophoretic deposition (EPD) from alcohol-based suspension such as iso-propanol, iso-butanol, and their mixture. For the formation of YBCO dense and adherent coating on a silver wire by EPD, 1% PEG(1000) 2 $m\ell$, as a additive for making their surface crack-free, was used for electrophoresis. As a results, the cracks were considerably decreased and the superconducting critical current density (J$_{c}$) without/with PEG was 1200 A/$\textrm{cm}^2$ and 2020 A/$\textrm{cm}^2$, which films deposited in mix ism-propanol and iso-butanol suspension.ion.

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Electrochemical Properties of Surface-Modified Silicon as Anode for Lithium Secondary Batteries (실리콘 재료의 표면개질에 따른 리튬이차전지 음극 특성)

  • Park, Cheol-Wan;Doh, Chil-Hoon;Moon, Seong-In;Yun, Mun-Soo
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2003.11a
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    • pp.602-606
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    • 2003
  • Silicon has been developed as an alternate anode material for lithium secondary batteries. A simple approach to improve the electrical contact of silicon powder has described. Carbon-coated and silver-coated silicon have been prepared by chemical vapor deposition and electroless plating respectively. Assembled cells, which consisted of surface modified silicon, lithium foil and $Li^+$ contained organic electrolyte, have been studied using electrochemical methods. Carbon-coated silicon was improved in the electrochemical performance such as reversibility and resistance compared to surface-unmodified silicon.

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Current Collector Effects on High Temperature Electrolysis by NI-YSZ Cermet Supported Solid Oxide Cells (집전체에 따른 NI-YSZ Cermet 기반의 가역적 고체산화물 연료전지를 이용한 고온 수증기 전기분해 특성)

  • Shin, Eui-Chol;Ahn, Pyung-An;Seo, Hyun-Ho;Lee, Jong-Sook;Yu, Ji-Haeng;Woo, Sang-Kuk
    • Journal of Hydrogen and New Energy
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    • v.21 no.6
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    • pp.533-539
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    • 2010
  • Ni-YSZ supported button cells were prepared by spray-coating YSZ and screen-printing YSZ-LSM powder as an electrolyte and oxygen electrode on Ni-YSZ cermet disks. In order to identify the polarization loss mechanism in high temperature electrolysis current-voltage characteristics coupled with electrochemical impedance spectroscopy were investigated as a function of temperature, current load, and the humidity. The effects of the different current collectors of platinum and silver for oxygen electrodes were compared. With Ag current collector two polarization losses were distinguished. The high frequency component was attributed to the Ni-YSZ cermet which was less susceptible to temperature variation but increasing in loss with humidity. The lower frequency component was attributed to the LSM electrode. Platinum current collector led to a much lower polarization loss.

Material Analysis of Black and White Photograph - Photograph from Borobudur - (흑백 사진의 재질 분석 - 보로부두르 사진을 중심으로 -)

  • Yun, Eun Young;Habibi, Modhamad;Jin, Hong Ju
    • Journal of Conservation Science
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    • v.35 no.5
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    • pp.385-391
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    • 2019
  • In order to examine the material characteristics of a black and white photograph of the Borobudur temple, in Indonesia, several analyses were conducted. A sample was taken from a black and white photograph; microscopy, Fourier transform-infrared spectroscopy, scanning electron microscopy/energy dispersive spectroscopy, X-ray diffraction, and X-ray fluorescence analyses showed that the black and white photograph was composed of four layers including a paper substrate, baryta, binder and surface layers. It was confirmed that the substrate was paper made of cellulose fiber from Cannabis sativa, the baryta layer was made of barium sulfate(BaSO4) in powder form, the binder was an emulsion containing silver halide, and the surface protective layer was made of gelatin. Since photographs have different characteristics and require different preservation environments depending on the material of construction, it is necessary to study various black and white photographic material characteristics corresponding to each time period.

Comparing the Effect of Three Processing Methods for Modification of Filament Yarns with Inorganic Nanocomposite Filler and their Bioactivity against Staphylococcus aureus

  • Dastjerdi, Roya;Mojtahedi, M.R.M.;Shoshtari, A.M.
    • Macromolecular Research
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    • v.17 no.6
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    • pp.378-387
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    • 2009
  • This research compared three methods for producing and processing nanocomposite polypropylene filament yarns with permanent antimicrobial efficiency. The three methods used to mix antimicrobial agents based on silver nano particles with PP were as follows: 1) mixing of PP powder and inorganic nanocomposite filler with the appropriate concentration using a twin-screw extruder and preparing granules, 2) method 1 with a singlerather than twin-screw extruder, and 3) producing the masterbatch by a twin-screw extruder and blending it with PP in the melt spinning process. All pure polypropylene samples and other combined samples had an acceptable spinnability at the spinning temperature of $240^{\circ}C$ and take-up speed of 2,000 m/min. After producing as-spun filament yarns by a pilot plant, melt spinning machine, the samples were drawn, textured and finally weft knitted. The physical and structural properties (e.g., linear density, tenacity, breaking elongation, initial modulus, rupture work, shrinkage and crystallinity) of the as-spun and drawn yarns with constant and variable draw ratios (the variable draw ratio was used to gain a constant breaking elongation of 50%) were investigated and compared, while DSC, SEM and FTIR techniques were used to characterize the samples. Finally, the antibacterial efficiency of the knitted samples was evaluated. The experimental results revealed that the crystallinity reduction of the as-spun yarn obtained from method 1 (5%) was more than that of method 2 (3%), while the crystallinity of the modified as-spun yarns obtained with method 3 remained unchanged compared to pure yarn. However, the drawing procedure compensated for this difference. By applying methods 2 and 3, the drawing generally improved the tenacity and modulus of the modified fibers, whereas method 1 degraded the constant draw ratio. Although the biostatic efficiency of the nanocomposite yarns was excellent with all three methods, the modified fabrics obtained from methods 1 and 2 showed a higher bioactivity.

The Effect of CNT Electrode on the Charging and Discharging Characteristics of Supercapacitor (CNT를 이용한 Supercapacitor의 충.방전 특성)

  • Hur, Geun;Myoung, Seong-Jae;Lee, Yong-Hyun;Chun, Myoung-Pyo;Cho, Jeong-Ho;Kim, Byung-Ik;Shim, Kwang-Bo
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2007.11a
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    • pp.275-275
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    • 2007
  • Two sorts of electrode composed of Sulpur/CNT/PVDF and Silver/CNT/PVDF were prepared by in situ chemical method and their electrochemical performance were evaluated by using cyclic voltammetry, impedance measurement and constant-current charge/discharge cycling technique. Also, composite electrodes were characterized by FE-SEM and BET. Raw materials such as CNT/Silver and CNT/Sulfur were mixed in ethanol, dried. These mixed materials were heated at 900 and $320^{\circ}C$ for 2hr, respectively in order to enhance contact among CNT electrodes. Electric double layer capacitor cells were fabricated using these mixed powder with polymer of PVDF. For the charging and discharging characteristics measured at scan rate of 1 mA/s, Supercapacitor of Sulphur-CNT-PVDF electrode showed a better performance than that of Ag-CNT-PVDF, which seems to be related with lower contact resistance of Sulphur-CNT-PVDF electrode.

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Durability and Characteristics of Ag-Pd Rod Heater for Bidet Fabricated by Screen Printing Process (스크린 프린팅 공정에 의해 제조된 비데용 Ag-Pd 봉형 발열체의 내구성 및 물성 평가 )

  • Tae-Ung Park;Da-Eun Hyun;Ik-Soo Kim;Sung-Chul Lee;Yeon-Sook Lee;Yong-Nam Kim;Dong-Won Lee;Jong-Min Oh
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.36 no.1
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    • pp.81-87
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    • 2023
  • Heaters using the resistance heating principle are used in various industrial fields that require heat and are also essentially used in bidet among small home appliances. A planar heater and a coil-inserted heater mounted on a conventional commercially used bidet have disadvantages and limitations of complicated manufacturing process and local heating. In this study, silver-palladium (Ag-Pd) powder material was used for a screen-printing process that is more advantageous in achieving simplification than the existing process, and a rod-type heater for bidet was manufactured. The on-off cycle test under actual conditions was conducted to confirm the durability and the capability of the fabricated heater, and the fabricated heater operated more than 2,600 on-off cycles, which means it could be applied for a commercial product. In addition, through the on-off cycles under harsh conditions, the cause of failure was identified after the test that the durability limit temperature of the heater was 850℃. Through Ag-Pd rod heater in this study, it is expected to contribute to the efficient development of electrode materials for heaters and the improvement of the durability of heaters in the future.