• Analytical Science and Technology
• /
• v.36 no.6
• /
• pp.259-266
• /
• 2023

The demand for rare-earth elements (REEs) is increasing owing to their significance as prominent materials in electronics, high-tech industries, geological research, nuclear forensics, and environmental monitoring. In general, the utilization of REEs in various applications requires the use of chromatographic techniques to separate individual elements. However, REEs have similar physicochemical properties, which makes them difficult to separate. Recently, several studies have examined the separation of REEs using LN resin as the stationary phase and aqueous nitric acid and hydrochloric acid solutions as eluents. Using this method, light REEs have been separated using dilute acid solutions as the eluent, whereas heavy REEs are separated using solutions with high acid concentrations. To increase the separation resolution between different REEs, either the column length or resin size is changed. In addition, the suggested methods are implemented to decrease the analysis time. This review presents technical information on the chromatographic separation of REEs using the LN resin and discusses the optimal experimental conditions.

• Proceedings of the Membrane Society of Korea Conference
• /
• 2003.07a
• /
• pp.91-94
• /
• 2003

In this work, the physicochemical properties for permeant molecules and polyion complex membrane prepared by complexation between SA and chitosan were determined by using molecular modeling methods, and the permeation behaviors of water and alcohol molecules through the PIC membrane have been investigated. In the case of penetrant molecule, the experimental results showed that the prepared membrane was excellent pervaporation performance result in most solution, and the selectivity and permeability of the membrane were dependent on the molecular size, the polarity and the hydrophilic surface of permeant organics. However, the separation behavior of methanol aqueous solution exhibited other permeation tendency with other feed solutions and contradictory result. That is, the membrane were preferentially permeable to methanol over water despite water molecule has stronger polarity and small molecular size than methanol molecule. In this study, the results were discussed from the viewpoint of chemical and physical properties between permeant molecules and membrane in the diffusion state.

• Journal of the Korean Society for Aeronautical & Space Sciences
• /
• v.37 no.3
• /
• pp.232-239
• /
• 2009

The prediction of the separation trajectories of external stores carried by military aircraft is an important task in the area of aircraft design having the objective to define the operational, release envelopes. This paper presents the results obtained for safe store separation from a fighter aircraft by experimental methods in the subsonic wind tunnel. The problems associated with separation of external stores can be studied by the use of several wind-tunnel test techniques. Attention is given the two most useful techniques: 1) dynamically scaled drop-model testing, 2) grid testing. A description of each method is given and data obtained are shown to validate the similarity within acceptable limits.

• KSII Transactions on Internet and Information Systems (TIIS)
• /
• v.7 no.4
• /
• pp.613-631
• /
• 2013

Cognitive radio (CR) is proposed as a key solution to improve spectral efficiency and overcome the spectrum scarcity. Spectrum sensing is an important task in each CR system with the aim of identifying the spectrum holes and using them for secondary user's (SU) communications. Several conventional methods for spectrum sensing have been proposed such as energy detection, matched filter detection, etc. However, the main limitation of these classical methods is that the CR network is not able to communicate with its own base station during the spectrum sensing period and thus a fraction of the available primary frame cannot be exploited for data transmission. The other limitation in conventional methods is that the SU data frames should be synchronized with the primary network data frames. To overcome the above limitations, here, we propose a spectrum sensing technique based on blind source separation (BSS) that does not need time synchronization between the primary network and the CR. Moreover, by using the proposed technique, the SU can maintain its transmission with the base station even during spectrum sensing and thus higher rates are achieved by the CR network. Simulation results indicate that the proposed method outperforms the accuracy of conventional BSS-based spectrum sensing techniques.

• Journal of the Korean Geographical Society
• /
• v.43 no.1
• /
• pp.134-153
• /
• 2008

The main purpose of the research is to illustrate the value of the spatial statistical approach to residential differentiation by providing a framework for exploratory spatial data analysis (ESDA) using a local spatial separation measure. ESDA aims, by utilizing a variety of statistical and cartographic visualization techniques, at seeking to detect patterns, to formulate hypotheses, and to assess statistical models for spatial data. The research is driven by a realization that ESDA based on local statistics has a great potential for substantive research. The main results are as follows. First, a local spatial separation measure is correspondingly derived from its global counterpart. Second, a set of significance testing methods based on both total and conditional randomization assumptions is provided for the local measure. Third, two mapping techniques, a 'spatial separation scatterplot map' and a 'spatial separation anomaly map', are devised for ESDA utilizing the local measure and the related significance tests. Fourth, a case study of residential differentiation between the highly educated and the least educated in major Korean metropolitan cities shows that the proposed ESDA techniques are beneficial in identifying bivariate spatial clusters and spatial outliers.

• Proceedings of the Korean Society For Composite Materials Conference
• /
• 2005.11a
• /
• pp.111-116
• /
• 2005

In this study the compatibility of Epoxy resin with Phenolic using three different separation layer techniques was investigated; some important process variables such as pressure, flow front and deformation were monitored in order to get a better understanding of the process.

• Journal of the Korean Society of Industry Convergence
• /
• v.27 no.3
• /
• pp.601-607
• /
• 2024

The discharge of oily wastewater into water bodies and soil poses a serious hazard to the environment and public health. Various conventional techniques have been employed to treat oil-water mixtures and emulsions; Unfortunately, these approaches are frequently expensive, time-consuming, and unsatisfactory outcomes. Porous materials and adsorbents are commonly used for purification, but their use is limited by low separation efficiencies and the risk of secondary contamination. Recent advancements in nanotechnology have driven the development of innovative materials and technologies for oil-contaminated wastewater treatment. Nanomaterials can offer enhanced oil-water separation properties due to their high surface area and tunable surface chemistry. The fabrication of nanofiber membranes with precise pore sizes and surface properties can further improve separation efficiency. Notably, novel technologies have emerged utilizing nanomaterials with special surface wetting properties, such as superhydrophobicity, to selectively separate oil from oil-water mixtures or emulsions. These special wetting surfaces are promising for high-efficiency oil separation in emulsions and allow the use of materials with relatively large pores, enhancing throughput and separation efficiency. In this study, we introduce a facile and scalable method for fabrication of superhydrophobic-superoleophilic felt fabrics for oil/water mixture and emulsion separation. AlN nanopowders are hydrolyzed to create the desired microstructures, which firmly adhere to the fabric surface without the need for a binder resin, enabling specialized wetting properties. This approach is applicable regardless of the material's size and shape, enabling efficient separation of oil and water from oil-water mixtures and emulsions. The oil-water separation materials proposed in this study exhibit low cost, high scalability, and efficiency, demonstrating their potential for broad industrial applications.

• Proceedings of the Korean Society of Near Infrared Spectroscopy Conference
• /
• 2001.06a
• /
• pp.3114-3114
• /
• 2001

During the last years phytochemistry and phytopharmaceutical applications have developed rapidly and so there exists a high demand for faster and more efficient analysis techniques. Therefore we have established a near infrared transflectance spectroscopy (NIRS) method that allows a qualitative and quantitative determination of new polyphenolic pharmacological active leading compounds within a few seconds. As the NIR spectrometer has to be calibrated the compound of interest has at first to be characterized by using one or other a combination of chromatographic or electrophoretic separation techniques such as thin layer chromatography (TLC), high performance liquid chromatography (HPLC), capillary electrophoresis (CE), gas chromatography (GC) and capillary electrochromatography (CEC). Both structural elucidation and quantitative analysis of the phenolic compound is possible by direct coupling of the mentioned separation methods with a mass spectrometer (GC-MS, LC-MS/MS, CE-MS, CEC-MS) and a NMR spectrometer (LC-NMR). Furthermore the compound has to be isolated (NPLC, MPLC, prep. TLC, prep. HPLC) and its structure elucidated by spectroscopic techniques (UV, IR, HR-MS, NMR) and chemical synthesis. After that HPLC can be used to provide the reference data for the calibration step of the near infrared spectrometer. The NIRS calibration step is time consuming, which is compensated by short analysis times. After validation of the established NIRS method it is possible to determine the polyphenolic compound within seconds which allows to raise the efficiency in quality control and to reduce costs especially in the phytopharmaceutical industry.

• Journal of Satellite, Information and Communications
• /
• v.10 no.4
• /
• pp.58-63
• /
• 2015

Due to GPS signal's vulnerability of jamming attack, various enhancement techniques are needed. Among variety of techniques, we focused on GPS receiver's anti-jamming techniques. There are many anti-jamming methods at GPS receivers which include filtering methods in time domain, frequency domain and space domain. However, these methods are ineffective to signals, which include both jamming and noise. To solve the problem, this paper proposes a jamming separation scheme by using a BSS method in a jamming environment. As separated GPS signals include noise after the jamming separation method, it is difficult to receive accurate GPS signals. For this reason, this paper also proposes a wavelet de-noising method to effectively eliminate noise. Experimental results of this paper are based on a real field test data of an integrated GPS/QZSS/Wi-Fi positioning system. At the end, the simulation result demonstrates its superiority by showing improved positioning accuracy.

• Parasites, Hosts and Diseases
• /
• v.47 no.4
• /
• pp.353-357
• /
• 2009

Cryptosporidium can cause gastrointestinal diseases worldwide, consequently posing public health problems and economic burden. Effective techniques for detecting contaminated oocysts in water are important to prevent and control the contamination. Immunomagnetic separation (IMS) method has been widely employed recently due to its efficiency, but, it is costly. Sucrose floatation technique is generally used for separating organisms by using their different specific gravity. It is effective and cheap but time consuming as well as requiring highly skilled personnel. Water turbidity and parasite load in water sample are additional factors affecting to the recovery rate of those 2 methods. We compared the efficiency of IMS and sucrose floatation methods to recover the spiked Cryptosporidium oocysts in various turbidity water samples. Cryptosporidium oocysts concentration at 1, $10^1$, $10^2$, and $10^3$ per $10{\mu}l$ were spiked into 3 sets of 10 ml-water turbidity (5, 50, and 500 NTU). The recovery rate of the 2 methods was not different. Oocyst load at the concentration < $10^2$ per 10 ml yielded unreliable results. Water turbidity at 500 NTU decreased the recovery rate of both techniques. The combination of sucrose floatation and immunofluorescense assay techniques (SF-FA) showed higher recovery rate than IMS and immunofluorescense assay (IMS-FA). We used this SF-FA to detect Cryptosporidium and Giardia from the river water samples and found 9 and 19 out of 30 (30% and 63.3%) positive, respectively. Our results favored sucrose floatation technique enhanced with immunofluorescense assay for detecting contaminated protozoa in water samples in general laboratories and in the real practical setting.