• 제목/요약/키워드: secondary materials

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선택적 레이저 용융법으로 제조된 Ti-6Al-4V 합금의 고 주기 피로 특성에 미치는 건식 전해 연마의 영향 (Effect of Dry-Electropolishing on the High Cycle Fatigue Properties of Ti-6Al-4V Alloy Manufactured by Selective Laser Melting)

  • 양동훈;김영균;황유진;김명세;이기안
    • 한국분말재료학회지
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    • 제26권6호
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    • pp.471-476
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    • 2019
  • Additively manufactured metallic components contain high surface roughness values, which lead to unsatisfactory high cycle fatigue resistance. In this study, high cycle fatigue properties of selective laser melted Ti-6Al-4V alloy are investigated and the effect of dry-electropolishing, which does not cause weight loss, on the fatigue resistance is also examined. To reduce the internal defect in the as-built Ti-6Al-4V, first, hot isostatic pressing (HIP) is conducted. Then, to improve the mechanical properties, solution treatment and aging are also implemented. Selective laser melting (SLM)-built Ti64 shows a primary α and secondary α+β lamellar structure. The sizes of secondary α and β are approximately 2 ㎛ and 100 nm, respectively. On the other hand, surface roughness Ra values of before and after dry-electropolishing are 6.21 ㎛ and 3.15 ㎛, respectively. This means that dry-electropolishing is effective in decreasing the surface roughness of selective laser melted Ti-6Al-4V alloy. The comparison of high cycle fatigue properties between before and after dry-electropolished samples shows that reduced surface roughness improves the fatigue limit from 150 MPa to 170 MPa. Correlations between surface roughness and high cycle fatigue properties are also discussed based on these findings.

교과서의 노인에 관한 내용 분석 및 교사용 노인교육 자료 개발 (Content Analysis of Aging in the Textbook & the Development of Instructional Materials about Aging)

  • 윤인경;조병은;한정란;김영환;장명희;김명자;박윤명;박길자;박선영
    • 한국가정과교육학회지
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    • 제17권1호
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    • pp.85-111
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    • 2005
  • 본 연구는 현행 초$\cdot$$\cdot$고등학교 교과서와 교사용 지도서에 수록된 노인관련 내용을 분석하고, 학교에서의 노인 교육에 반드시 포함되어야 하는 내용 요소를 추출, 체계화하며, 이를 바탕으로 노인 관련 내용의 교수 학습을 도울 수 있는 교육 자료를 개발하는데 목적이 있다. 연구는 3단계의 과정을 거쳐 수행되었다. 첫째, 외국의 관련 교과서 분석과 국내외의 노인교육프로그램에 대한 문헌 분석. 둘째 내용요소 추출과 체계화를 한 전문가 협의단계, 셋째 개발한 교육자료를 현장에서 실험 적용하고 적용전후의 설문조사를 한 현장 적용 단계로 이루어졌다. 개발된 교수 ·학습자료에 대한 교사와 학생들의 반응은 개발된 노인교육 자료가 노인에 대한 인식과 이해에 기여 할 수 있음을 보여주고 있다.

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Thermal Expansion and Dielectric Properties of CaO-ZnO-B2O3-SiO2 Glass-Added Al2O3 Composites for LTCC Applications

  • Byeon, Tae-Hun;Park, Hyo-Sung;Shin, Hyun-Ho;Yoon, Sang-Ok;Oh, Chang-Yong
    • 한국세라믹학회지
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    • 제47권4호
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    • pp.325-328
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    • 2010
  • Varying quantities of a high-thermal-expansion glass, 50CaO-20ZnO-$20B_2O_3-10SiO_2$ (CZBS), were added to alumina and sintered at $875^{\circ}C$ for 2 h for low temperature co-firing ceramic (LTCC) applications. As the amount of glass addition increased from 40 wt% to 70 wt%, the apparent density of the sintered product increased from 88.8% to 91.5%, which was also qualitatively confirmed by microstructural observation. When the glass addition was very high, e.g., 70 wt%, an apparent formation of secondary phases such as $CaZn_2AlZnSiAlO_7$, $Ca_2Al(AlSi)O_7$, $Ca_2Al_2SiO_7$, $Ca_2ZnSi_2O_7$ and ZnO, was observed. Both the dielectric constant and the coefficient of thermal expansion increased with the glass addition, which was qualitatively consistent with the analytical models, while the experimental values were lower than the predicted ones due to the presence of pores and secondary phases.

고 에너지 (1.5 MeV) Boron 이온 주입과 초기 산소농도 조건이 깊은 준위에 미치는 영향에 관한 연구 (The Effects of high Energy(1.5MeV) B+ ion Implantation and Initial Oxygen Concentration Upon Deep Level in CZ Silicon Wafer)

  • 송영민;문영희;김종오
    • 한국재료학회지
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    • 제11권1호
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    • pp.55-60
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    • 2001
  • 고 에너지 (1.5 MeV) 이온 주입된 Boron의 농도와 silicon 기판의 초기 산소 농도의 변화에 따라 silicon기판에 형성된 결정 결함 및 금속 불순물의 Gettering 효율에 대하여 DLTS(Deep Level Transient Spectroscopy), SIMS(Secondary ion Mass Spectroscopy), BMD(Bulk Micro-Defect) analysis 및 TEM (Transmission Electron Microscopy)을 이용하여 연구하였다. 이온 주입 전후의 DLTS 결과를 확산로 및 RTA를 이용한 열처리 전후의 DLTS 결과와 비교할 때 이온 주입 전 시편에서 볼 수 있는 공공에 의한 깊은 준위는 열처리 온도의 증가에 따라 금속 불순물과 관련된 깊은 준위로 천이함을 알 수 있다. 또한 고온 열처리의 경우, 초기 산소 농도가 높을수록 깊은 준위의 농도가 감소함을 볼 때 초기 산소 농도가 높을 수록 gettering 효율 측면에서 유리한 것으로 사료된다

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PDP용 유전체 보호막 재료 개발을 위한 연구 (I) (두께 최적화된 $Al_2O_3/MgO$의 열처리 특성 ) (A study for development of a dielectric protection layer in PDP (I) (The annealing characteristics of thickness-optimized $Al_2O_3/MgO$))

  • 정진만;임기주;신경;이현용;정흥배
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 1998년도 춘계학술대회 논문집
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    • pp.117-120
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    • 1998
  • In this study, $Al_2O_3/MgO$ bilayer was prepared with Electron-beam evaporation and the properties of the film was investigated in order to improve the property of MgO film, which is used for the protection layer in PDP(P1asma Display Panel). The thickness of $Al_2O_3/MgO$ bilayer was optimized by the Matrix Theory for the fabrication of antireflection structure for 5350A wavelength. The secondary electron emission yields of as-deposited film and annealed film were measured and compared, the bilayer was considered for the applicability as PDP. XRD showed the strong (200) primary peak of MgO. The intensity of (200) peak in the film annealed at 300C was decreased. As the result of SEM analysis for MgO films and Alz03 films, it is considered that the morphology of the films were improved of roughness and it were condensed by annealing.

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산업용 니켈-카드뮴 폐 이차전지 습식 재활용을 위한 전처리 및 산 침출에 대한 연구 (A Study on Pretreatment and Acid Leaching for Wet Recycling of Waste Industrial Ni-Cd Secondary Battery)

  • 정수훈;김대원;박일정;최중엽;양대훈;최희락
    • 자원리싸이클링
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    • 제26권5호
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    • pp.67-76
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    • 2017
  • 산업용 폐 니켈-카드뮴 전지를 효율적으로 재활용하기 위하여 케이스에서 분리된 양극 및 음극 스크랩을 cut mill로 분쇄하여 분급하였으며, 철 성분 제거를 위하여 습식 자력선별법을 이용하였다. 또한 얻어진 양극 및 음극 분말을 습식법을 이용하기 위하여 다양한 조건에서의 산 침출 실험을 실시하였다. 최적 침출조건으로 2.0 M $H_2SO_4$, 반응온도 $90^{\circ}C$, 15 wt% $H_2O_2$, L/S=20의 조건에서 3시간 침출을 하여 유가금속인 니켈 및 카드뮴의 침출율을 99% 이상 얻을 수 있었다.

이온치환 반응을 이용한 니켈-카드뮴 폐이차전지에서 카드뮴의 분리에 대한 연구 (A Study on the Separation of Cadmium from Waste Ni-Cd Secondary Batteries by Ion Substitution Reaction)

  • 김대원;박일정;안낙균;정항철;정수훈;최중엽;양대훈
    • 자원리싸이클링
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    • 제27권4호
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    • pp.36-43
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    • 2018
  • 폐 니켈-카드뮴 전지의 재활용을 위하여 효율적으로 카드뮴과 니켈을 분리할 수 있도록 이온치환 반응을 이용하여 선택적으로 카드뮴을 분리하였다. 폐 니켈-카드뮴 전지 내의 전극을 분쇄하여 얻은 전극 분말을 황산에 침출시킨 니켈-카드뮴 용액에 황화나트륨을 첨가하여 CdS로 침전시켰다. 다양한 조건에서 이온치환실험을 실시하였으며, 최적조건으로는 상온에서 용액의 pH = -0.1, $Na_2S/Cd=2.3$일 때 용액 내 잔존하는 Cd은 약 100 ppm으로 대부분 CdS로 침전된 결과를 얻을 수 있었다.

다이캐스팅으로 제조한 AXE710 Mg 합금의 미세조직 및 크리프 특성 (Microstructure and Creep Property of Die-Cast AXE710 Mg Alloy)

  • 강문구;소태일;정화철;신광선
    • 대한금속재료학회지
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    • 제49권9호
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    • pp.686-691
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    • 2011
  • To develop creep resistant die-cast Mg alloys, various alloying elements, including Ca, Ce, and Sr, were added to a Mg-Al alloy. The AXE710 alloy was produced on a 320 ton high-pressure die casting machine. The microstructure and creep properties of the alloy were examined. The creep behavior was investigated at $150^{\circ}C$ for stresses ranging from 50 to 100 MPa. The stress exponent was derived from the relationship between normalized secondary creep rates and compensated effective stresses. It was found to be 4.9, indicating that the dislocation climb is a dominant creep mechanism.

복합재 보강패널의 분리파손 및 좌굴 후 강도 특성 (Debonding and Postbuckling Failure Characteristics of Composite Stiffened Panels)

  • 김광수;유재석;안재모;장영순;이영무
    • 한국복합재료학회:학술대회논문집
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    • 한국복합재료학회 2005년도 춘계학술발표대회 논문집
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    • pp.59-63
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    • 2005
  • Compression tests were performed for six types of hat stiffened composite panels with different bonding methods and stiffener section shapes. Six panels showed similar behaviors in buckling and post-buckling region before a skin-stiffener separation failure occurred. The skin-stiffener separation failures occurred in the panels with closed type stiffeners regardless of bonding methods, but not in the panels with open type stiffeners. The separation failures not only reduced the postbuckling strength but also changed buckling mode and postbuckling stiffness. All the separation failures were initiated at the stiffener flange edges closest to skin buckling crests. The co-cured or secondary bonded panels with open type stiffeners had the largest structural performance. Because the post-buckling strength and performance of the composite stiffened panels are reduced by the separation failure, it is important to find bonding methods, stiffener types and manufacturing parameters for preventing of the separation failure.

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Mulching Methods and Removing Dates of Mulch Affects Growth and Post Harvest Quality of Garlic (Allium sativum L.) cv. Uiseong

  • Kwon, Kwon-Seok;Azad, Md. Obyedul Kalam;Hwang, Jae-Moon
    • 원예과학기술지
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    • 제29권4호
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    • pp.293-297
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    • 2011
  • This experiment was conducted to elucidate the effects of mulching materials and removing time of the transparent polyethylene (PE) film on the growth of garlic at Uiseong experimental field, Korea. The experimental mulching materials comprised of transparent polyethylene film (0.025 mm) and net polyethylene (NPE). Plant height and leaf number of garlic were highest at PE treatment when the PE removing date was March 18 and this treatment also promoted the no. of cloves. Length of leaf sheath and bolting rate were highest and bulb weight loss rate was lowest at PE + NPE treatment when the PE removing date was March 18. But clove number was the lowest in this treatment compared to conventional PE film treatment. Conventional mulching method accelerated secondary growth rate but bulb weight loss was vice versa. There were statistically no differences in bulb diameter among treatments but conventional treatment positively focused on bulb diameter. Whenever PE film remove can suppress weeds compared to no mulching treatment but the dry weight of weeds were increasing trends as the removal dates of PE film were delayed. Transparent PE or PE + NPE treatments can be recommended to grow best quality garlic when PE film removing date is March 18.