• 제목/요약/키워드: scanning measurements

검색결과 741건 처리시간 0.034초

Activated Physical Properties at Air-Polymer Interface

  • Kajiyama, Tisato
    • Macromolecular Research
    • /
    • 제15권2호
    • /
    • pp.109-113
    • /
    • 2007
  • The surface molecular motion of monodisperse polystyrene (PS) films was examined using scanning vis-coelasticity microscopy (SVM) in conjunction with lateral force microscopy (LFM). The dynamic storage modulus, E', and loss tangent, $tan\delta$, at a PS film surface with number-average molecular weights, $M_n$, smaller than 30 k were found to be smaller and larger than those for the bulk sample, even at room temperature, meaning that the PS surface is in a glass-rubber transition or fully rubbery sate at this temperature when the $M_n$ is small. In order to quantitatively elucidate the dynamics of the molecular motion at the PS surface, SVM and LFM measurements were performed at various temperatures. The glass transition temperature, $T_g$, at the surface was found to be markedly lower than the bulk $T_g$, and this discrepancy between the surface and bulk became larger with decreasing $M_n$. Such an intensive activation of the thermal molecular motion at the PS surfaces can be explained in terms of an excess free volume in the vicinity of the film surface induced by the preferential segregation of the chain end groups.

The Formation Technique of Thin Film Heaters for Heat Transfer Components (열교환 부품용 발열체 형성기술)

  • 조남인;김민철
    • Journal of the Semiconductor & Display Technology
    • /
    • 제2권4호
    • /
    • pp.31-35
    • /
    • 2003
  • We present a formation technique of thin film heater for heat transfer components. Thin film structures of Cr-Si have been prepared on top of alumina substrates by magnetron sputtering. More samples of Mo thin films were prepared on silicon oxide and silicon nitride substrates by electron beam evaporation technology. The electrical properties of the thin film structures were measured up to the temperature of $500^{\circ}C$. The thickness of the thin films was ranged to about 1 um, and a post annealing up to $900^{\circ}C$ was carried out to achieve more reliable film structures. In measurements of temperature coefficient of resistance (TCR), chrome-rich films show the metallic properties; whereas silicon-rich films do the semiconductor properties. Optimal composition between Cr and Si was obtained as 1 : 2, and there is 20% change or less of surface resistance from room temperature to $500^{\circ}C$. Scanning electron microscopy (SEM) and Auger electron spectroscopy (AES) were used for the material analysis of the thin films.

  • PDF

Facile Hydrothermal Synthesis and Characterization of the $CeO_2$ Nanorings

  • Arul, N. Sabari;Kim, Tae Whan;Mangalaraj, Devanesan
    • Proceedings of the Korean Vacuum Society Conference
    • /
    • 한국진공학회 2013년도 제44회 동계 정기학술대회 초록집
    • /
    • pp.455-455
    • /
    • 2013
  • $CeO_2$ nanorings were synthesized by using a surfactant free hydrothermal method. The surface morphology, structural and optical properties of the synthesized $CeO_2$ was investigated by using scanning electron microscopy (SEM), X-ray diffraction (XRD), and ultraviolet-visible (UV) spectroscopy measurements. SEM images showed that the surface morphology of the formed $CeO_2$ appeared as nanorings. The XRD pattern of $CeO_2$ nanorings showed the presence of the polycrystalline $CeO_2$ phase readily indexed to the cubic fluorite structure of the $CeO_2$. The mean crystallite size of the $CeO_2$ was calculated using the Scherrer equation from the XRD line broadening of the (111) planes of the cubic $CeO_2$. The UV-Visible spectroscopy spectrum of the $CeO_2$ nanorings exhibited a strong UV absorption band around 350 nm.

  • PDF

Incoherent Optical Signal Processor Using an Acousto-Optic Modulator and a Scanner (어쿠스토옵틱 광변조기와 스캐너를 사용한 인코히런트 광신호 처리기)

  • Park, Jin-Woo
    • Journal of the Korean Institute of Telematics and Electronics
    • /
    • 제26권12호
    • /
    • pp.2016-2024
    • /
    • 1989
  • A versatile incoherent optical processing system is developed and analyzed in detail, in which an acousto-optic modulator is used to generate the temporal offset frequency for heterodyning and an optical scanner to process the input object in scanning mode. The operational characteristics of the systems are studied with respect to spatial filtering in terms of the spectral width change of the light source, the temporal offset frequency, and a scanning rate. To enhance the system's capability, two schemes for tuning the system's OTF, structural tuning and defocused object tuning, are also developed and verified with the MTF measurements and computer calculations.

  • PDF

Tropospheric Ozone Retrieval Algorithm Based on the TOMS Scanning Geometry

  • Kim, Jae-Hwan;Na, Sun-Mi;Newchurch, M.J.
    • Korean Journal of Remote Sensing
    • /
    • 제19권1호
    • /
    • pp.11-19
    • /
    • 2003
  • This paper applies the Scan-Angle Method (SAM) to the Total Ozone Mapping Spectrometer (TOMS) aboard Earth Probe (EP) satellite for determining tropospheric ozone based on TOMS scan geometry. In the northern tropical Africa burning season, the distribution of the SAM-derived tropospheric ozone presents a tropospheric ozone enhancement related to biomass burning. This distribution is consistent with that of fire counts observed from Along Track Scanning Radiometer (ATSR) and that of carbon monoxide, the tropospheric ozone precursor, observed from Measurements of Pollution In The Troposphere (MOPITI). However, this feature is not shown in the distribution of tropospheric ozone derived from other TOMS-based algorithms for the northern burning season. In the high latitudes, the influence of pollution in the SAM results is seen over the northern continents in agreement with carbon monoxide for northern summer when the dynamical activity is weak in the northern hemisphere.

A STUDY OF GEL STRUCTURE IN THE NONIONIC SURFACTANT / CETOSTEARYL ALCOHO L/ WATER TERNARY SYSTEMS BY DIFFERENTIAL SCANNING CALORIMETER

  • Yoon, Moung-Seok;Chung, Youn-Bok;Kun Han
    • Journal of the Society of Cosmetic Scientists of Korea
    • /
    • 제26권1호
    • /
    • pp.213-232
    • /
    • 2000
  • Cetostearyl alcohol has been incorporated into cosmetic or pharmaceutial emulsions to give them an appropriate consistency and a long term stability. It is well known that cetostearyl alcohol forms a gel phase with a nonionic surfactant in an aqueous system, and the properties of the gel phase depend on several factors such as the ratio of fatty alcohols. The aim of the present Paper is to investigate the effect of the structural difference of the lipophilic part of surfactants on the stability of the gel phase in the nonionic surfactant / cetostearyl alcohol / water ternary systems using differential scanning calorimeter. It is concluded that the gel phase formed by the surfactant having the bended alkyl chain is more unstable than that formed by the case of the straight alkyl chain, and we discussed the reason why the former is more unstable after long term storage by means of the measurements of the ${\Delta}$H.

  • PDF

Genetic Analysis of Ultrasound and Carcass Measurement Traits in a Regional Hanwoo Steer Population

  • Hwang, Jeong Mi;Cheong, Jae Kyoung;Kim, Sam Su;Jung, Bong Hwan;Koh, Myung Jae;Kim, Hyeong Cheol;Choy, Yun Ho
    • Asian-Australasian Journal of Animal Sciences
    • /
    • 제27권4호
    • /
    • pp.457-463
    • /
    • 2014
  • Ultrasound measurements of backfat thickness (UBF), longissimus muscle area (ULMA) and marbling score (UMS) and carcass measurements of carcass weight (CW), backfat thickness (BF), longissimus muscle area (LMA), and marbling score (MS) on 7,044 Hanwoo steers were analyzed to estimate genetic parameters. Data from Hanwoo steers that were raised, finished in Hoengseong-gun, Gangwon-do (province) and shipped to slaughter houses during the period from October 2010 to April 2013 were evaluated. Ultrasound measurements were taken at approximately three months before slaughter by an experienced operator using a B-mode real-time ultrasound device (HS-2000, FHK Co. Ltd., Tokyo, Japan) with a 3.5 MHz linear probe. Ultrasound scanning was on the left side between 13th rib and the first lumbar vertebrae. All slaughtering processes and carcass evaluations were performed in accordance with the guidelines of beef grading system of Korea. To estimate genetic parameters, multiple trait animal models were applied. Fixed effects included in the models were: the effects of farm, contemporary group effects (year-season at the time of ultrasound scanning in the models for UBF, ULMA, and UMS, and year-season at slaughter in the models for CW, BF, LMA, and MS), the effects of ultrasound technicians as class variables and the effects of the age in days at ultrasound scanning or at slaughtering as linear covariates, respectively for ultrasound and carcass measures. Heritability estimates obtained from our analyses were 0.37 for UBF, 0.13 for ULMA, 0.27 for UMS, 0.44 for CW, 0.33 for BF, 0.36 for LMA and 0.54 MS, respectively. Genetic correlations were strongly positive between corresponding traits of ultrasound and carcass measures. Genetic correlation coefficient between UBF and BF estimate was 0.938, between ULMA and LMA was 0.767 and between UMS and MS was 0.925. These results suggest that ultrasound measurement traits are genetically similar to carcass measurement traits.

Clinical usefulness of facial soft tissues thickness measurement using 3D computed tomographic images (3차원 전산화단층촬영 영상을 이용한 안면 연조직 두께 계측의 임상적 유용성)

  • Jeong Ho-Gul;Kim Kee-Deog;Han Seung-Ho;Hu Kyung-Seok;Lee Jae-Bum;Park Hyok;Choi Seong-Ho;Kim Chong-Kwan;Park Chang-Seo
    • Imaging Science in Dentistry
    • /
    • 제36권2호
    • /
    • pp.89-94
    • /
    • 2006
  • Purpose : To evaluate clinical usefulness of facial soft tissue thickness measurement using 3D computed tomographic images. Materials and Methods : One cadaver that had sound facial soft tissues was chosen for the study. The cadaver was scanned with a Helical CT under following scanning protocols about slice thickness and table speed; 3 mm and 3 mm/sec, 5 mm and 5 mm/sec, 7 mm and 7 mm/sec. The acquired data were reconstructed 1.5, 2.5, 3.5 mm reconstruction interval respectively and the images were transferred to a personal computer. Using a program developed to measure facial soft tissue thickness in 3D image, the facial soft tissue thickness was measured. After the ten-time repeation of the measurement for ten times, repeated measure analysis of variance (ANOVA) was adopted to compare and analyze the measurements using the three scanning protocols. Comparison according to the areas was analyzed by Mann-Whitney test. Results : There were no statistically significant intraobserver differences in the measurements of the facial soft tissue thickness using the three scanning protocols (p>0.05). There were no statistically significant differences between measurements in the 3 mm slice thickness and those in the 5 mm, 7 mm slice thickness (p>0.05). There were statistical differences in the 14 of the total 30 measured points in the 5 mm slice thickness and 22 in the 7 mm slice thickness. Conclusion : The facial soft tissue thickness measurement using 3D images of 7 mm slice thickness is acceptable clinically, but those of 5 mm slice thickness is recommended for the more accurate measurement.

  • PDF

Development of MRI Scanning Technique that is Comfortable for Patients with Anxiety Disorder

  • Cho, Moo-Seong;Cho, Jae-Hwan;Chang, Yong-Min;Cho, Yong-Ho;Zeon, Seok-Kil;Dong, Kyung-Rae;Chung, Woon-Kwan;Lee, Hae-Kag;Kim, Hyun-Ju;Bae, Jae-Young;Ahn, Jae-Ouk;Lee, Sang-Jeong
    • Journal of Magnetics
    • /
    • 제16권4호
    • /
    • pp.350-362
    • /
    • 2011
  • The principal objective of this study was to develop a scanning technique that helps patients reduce their anxiety and relax their physical tension in the MRI system. The study targeted 10 healthy persons with no medical history of anxiety disorder in the past and with no current clinically diagnosed anxiety disorder, as well as 10 patients who were currently experiencing an anxiety disorder during the MRI scanning. The focusing board assembly was self-manufactured to conduct a clinical experiment via MRI scans. As a method to confirm the efficacy of the experiment, the bio meter was used to measure brainwaves from the study targets that were divided into the normal person group (A), who felt no anxiety in the MRI system and the experimental group, (B) who did experience anxiety in the MRI system. The two groups were compared between the cases in which the focusing board assembly was used and not used after measurements were conducted using the model MRI system and the bio meter. According to the comparison and analysis results, low measurements of the ${\alpha}$ wave indicate highly effective relaxation of tension. In the normal person group, the ${\alpha}$ wave measurement showed almost no difference between cases in which the focusing board assembly was used and cases in which it was not used. In the experimental group, the $\acute{a}$ wave measurements were lower in cases in which the focusing board assembly was used than in cases in which the focusing board assembly was not used; this was indicative of a profound relaxation effect.

Corrosion Inhibition of Aluminium using 3-Hydroxy flavone in the Presence of Quarternary Ammonium Salts in NaOH Medium

  • Princey, J. Morris;Nagarajan, Prabavathi
    • Journal of the Korean Chemical Society
    • /
    • 제56권2호
    • /
    • pp.201-206
    • /
    • 2012
  • The anticorrosive effect of 3-Hydroxyflavone (3HF) in combination with quarternary ammonium bromide and iodide salts (QAB and QAI) for aluminium corrosion in NaOH medium was studied at the temperature range of 303K-323K using weight loss study, potentiodynamic polarization study and impedance spectroscopic measurements. The results revealed that the inhibition efficiency increases with the inhibitor concentration and it further increases on the addition of quarternary ammonium bromide and iodide salts. The enhanced inhibition efficiency of the inhibitor in the presence of quarternary ammonium salts may be due to synergistic effect. The adsorption process of 3HF on the aluminium surface obeys Langmuir's adsorption isotherm. The mechanism of adsorption is further supported by Scanning Electron Microscopic study (SEM).