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Effect of surface sealant on surface roughness of dental composite with different surface roughness (서로 다른 거칠기의 복합레진에 표면 강화제 도포시 표면 거칠기의 변화)

  • Dong-Ah Shin;Seon-Ju Jin;Kkot-Byeol Bae;In-Nam Hwang
    • Journal of Dental Rehabilitation and Applied Science
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    • v.39 no.4
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    • pp.195-203
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    • 2023
  • Purpose: This study aimed to evaluate the influence of surface sealants on the surface roughness of composite resins. Materials and Methods: The study used microfilled composite resin (Metafil CX, Sun Medical Co.) and hybrid composite resin (AeliteTM LS posterior, Bisco). Sixty specimens (8 mm in diameter and 4 mm in height) of each composite resin type were prepared and divided into 3 groups. Each specimen was ground with 600, 1000, and 2000-grit sandpaper. The Surface roughness (Ra) values were measured using a surface roughness tester (SJ-301, Mytutoyo) before and after surface sealant application. Surface sealants, BisCoverTM LV (Bisco), Optiguard® (Kerr), and Seal-n-ShineTM (Pulpdent), were applied to the specimens, as instructed and observed by scanning electron microscope (JSM-7500, JEOL) and atomic force microscope (MultiMode IV, Veeco Instruments). Results: Specimens ground with 600-grit sandpaper coated with surface sealants exhibited significantly lower Ra values than the untreated group (P < 0.05). Specimens ground with 1000 and 2000-grit sandpaper showed statistically no difference. There was no significant difference in surface roughness among BisCoverTM LV, Optiguard®, and Seal-n-ShineTM. SEM and AFM revealed remarkably decreased microdefects on the surfaces of composite resins after surface sealant application. Conclusion: Surface sealants can influence surface roughness when applied on the rough surface of composite resins but not on highly polished composite resins.

SHEAR BOND STRENGTH OF ORTHODONTIC BONDING RESINS TO PORCELAIN; AN IN VITRO STUDY (도재에 대한 교정용 브라켓 접착 레진의 전단접착강도에 관한 연구)

  • Ko, Jin-Hwan;Lee, Ki-Soo
    • The korean journal of orthodontics
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    • v.22 no.1
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    • pp.43-65
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    • 1992
  • Bonding orthodontic adhesive resins to glazed porcelain surface is not attainable. The aim of this investigation was to examine, in vitro, the effect of three methods of porcelain surface pretreatment on the shear bond strength of orthodontic adhesives, and to compare the shear strength of orthodontic bracket bonding to porcelain surface by the best results that to human enamel. Porcelain disks ($Ceramco^{(TM)}$ and $Vita^{(TM)}$) baked in the laboratory were roughened by sandpapers, #320, #600, #800, #1000 and #1200, and were pretreated with silane and dried at the various temperatures, room temperature, $50^{\circ}C$, $70^{\circ}C$ and $90^{\circ}C$, and were etched by 3% hydrofluoric acid solution for 1, 3, 5, 7, and 9 minutes, orthodontic adhesives (System $1+^{(TM)}$ and $Unite^{(TM)}$) were applied on them, and shear bond strengths were measured by Instron. The best results of pretreatment of each method were determined by the shear bond strengths. Again, porcelain disks were pretreated by the determined best results and human enamel were etched by 37% hydrofluoric acid solution, orthodontic brackets were bonded on them by the orthodontic adhesives, and the shear bond strengths were measured and compared between them. 1. Roughening porcelain surfaces with coarse sandpaper (#300) showed higher shear bond strength than that with finer sandpapers, but it $(22.44Kgf/cm^2)$ was distinguishably low compared to that from etched human enamel $(144.11Kgf/cm^2)$. 2. There were disparities in shear bond strengths upon the orthodontic resins, which was presumably related to the contents of fillers in orthodontic adhesive resins. Also there were disparities in shear bond strength upon the porcelains which had different composition. 3. Silane enhanced the shear bond strength of orthodontic resins to porcelain surfaces ($25.20Kgf/cm^2$ at $50^{\circ}C$), which was markedly low compared to that from etched human enamel. 4. Etched porcelain surface with 3% hydrofluoric acid solution for 1 to 9 minutes showed no difference in shear bonding strength of orthodontic adhesive resins. Shear bond strength from etched porcelain $(97.43-120.72Kgf/cm^2)$ were as high as clinically available, but low compared to that from etched human enamel. 5. Roughening with #300 sandpaper and etching by 3% hydrofluoric acid followed silane application on porcelain surface showed lower shear bond strength than etched human enamel, but were as high as clinically useful. 6. The results suggest that etching porcelain surface by 3% hydrofluoric acid solution might provide comparatively high shear bond strength as much as clinically favorable.

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Effects of Pre-Sintering Surface Treatment and Liner Application on the Shear Bond Strength of Zirconia and Pressable Ceramic (소결 전 지르코니아 표면처리와 라이너 사용에 따른 지르코니아와 열가압성형도재의 전단결합강도)

  • Lee, Gwang-Young;Cho, Mi-Hyang;Choi, Sung-Min
    • Journal of Technologic Dentistry
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    • v.37 no.3
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    • pp.121-127
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    • 2015
  • Purpose: This study was intended to investigate the effect of applying liner for chemical bonding and physical surface roughness created on zirconia by using a sandpaper before sintering on the bond strength between the two materials. Methods: Zirconia blocks were cut using a low-speed cutter. Plate-shaped specimen($6mm{\times}6mm{\times}3mm$) was fabricated by sintering after giving surface roughness according to four kinds of sandpapers. Depending on whether or not to use liner, 60 specimens were divided into two groups ZN(non-liner), ZL(liner), and the two groups were subdivided into four groups respectively in accordance with sandpaper used, totaling eight groups (n=10). The surface roughness (Ra) values and shapes before sintering were observed, and shear bond strength after pressing ceramic plasticity was measured with a universal testing machine. For a test of the significance, a one-way ANOVA was performed, and Tukey's multiple comparison test was conducted. Results: The observation of the surface roughness was SB04($2.22{\pm}1.16{\mu}m$), SB08($2.98{\pm}0.33{\mu}m$), SB12($2.44{\pm}1.32{\mu}m$), SB20($2.34{\pm}0.59{\mu}m$) and SA04($2.34{\pm}0.67{\mu}m$), SA08($1.28{\pm}0.90{\mu}m$), SA12($2.03{\pm}1.60{\mu}m$), SA20($2.19{\pm}1.73{\mu}m$). In the case of ZN Group, the shear bond strength was ZN04($23.26{\pm}3.83MPa$), ZN08($21.76{\pm}2.33MPa$), ZN12($20.49{\pm}3.01MPa$), ZN20($24.98{\pm}4.22MPa$)(p<0.05). As for ZL Group, the shear bond strength was ZL04($25.09{\pm}5.67MPa$), ZL08($22.98{\pm}2.26MPa$), ZL12($21.54{\pm}5.70MPa$), ZL20($23.98{\pm}3.23MPa$)(p<0.05). Conclusion: The research results showed that the bond strength of Zirconia core and Pressing ceramic was further improved by physical surface treatment before sintering, rather than by chemical bonding through liner surface treatment.

A Study on the Changes in Surface Properties According to Post-treatment of SLA 3D Printing Materials (SLA 3D 프린팅 소재의 후처리에 따른 표면특성 변화 연구)

  • Bae, Seo Jun;Im, Do Jin
    • Korean Chemical Engineering Research
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    • v.60 no.1
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    • pp.132-138
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    • 2022
  • In this study, a basic study was performed to systematically compare the changes in surface properties according to the post-processing method of the stereolithography (SLA) printing method, which is a photocuring 3D printing method, and to provide information on the post-processing method suitable for the application. Although it was possible to improve some of the transparency of the SLA-type output by regularly changing the irregular microstructure of the surface through polishing, it was difficult to secure sufficient transparency like glass. The change in contact angle characteristics due to grinding showed a tendency to slightly increase as the grinding time increased and the particle size of the sandpaper used was small, but the variation between samples was large and the average contact angle was 77~90°, showing no statistically significant difference. Surface treatment methods other than polishing were tried, and it was confirmed that it was possible to easily and simply improve the transparency by applying a commercially available vehicle scratch remover or silicone oil. In addition, a method for securing high transparency such as glass by using a scratch remover after sequential grinding while reducing the particle size of the sandpaper was proposed. Finally, even after surface treatment through polishing and various methods, it was difficult to secure a contact angle of 90° or more.

A Study on the Improvement of Light-Extraction Efficiency of Organic Light-Emitting Diodes with a Use of Random-Textured Film (랜덤 택스쳐 필름을 이용한 유기 발광 소자의 광추출 효율 향상에 관한 연구)

  • Kim, Hye Sook;Hwang, Deok Hyeon;Jang, Kyeong Uk;Kim, Tae Wan
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.28 no.7
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    • pp.446-449
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    • 2015
  • An improvement of light-extraction efficiency of organic light-emitting diodes was studied by using random-textured films (RTF). Device was made in a structure of RTF/glass/ITO/TPD/$Alq_3$/LiF/Al. RTF mold was made by spreading PDMS solution on a sandpaper. By pressing this mold on the glass substrate pre-coated with ZPU material, the RTF was obtained. From this study, there was an improvement of external quantum efficiency by about 30% in the device with the random-textured film (RTF 40) compared to that of the reference one.

Experiments on Single-Disk Pumps for the Transportation of Micro-scale Water Life (미소 수중 생물체 이송용 단판 디스크 펌프의 성능 실험)

  • Zhang, Z.Q.;Chang, S.M.;Jeong, Y.H.;Yang, J.S.
    • The KSFM Journal of Fluid Machinery
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    • v.14 no.6
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    • pp.18-25
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    • 2011
  • A boundary-layer pump with a single disk has been experimented to obtain its characteristic curve by changing the impeller of a centrifugal pump to a single disk. The primary objective to use of these types of pumps is to avoid hurting water life during transportation unnecessarily. The change of impeller should degrade the performance of pump, so we used the method to increase the roughness on the disk with sandpaper and mesh. The enhancement of shear force from the rotation of disk to the internal flow brought an augmentation of momentum transport, and the characteristics were far improved from the original single-disk pump without decreasing the survival rate of water life in the case of Pseudobagrus fulvidraco (bullhead fish). However, in the case of Artemia cyst (zooplankton), the survival rate was very degraded due to the micro scale smaller than turbulent eddy size. The result of this study could be used for the design of transportation and bio-filtering of water lying on a specific bandwidth of its scale of size.

박피방법에 따른 근채류(도라지 및 우엉)의 이화학적 품질특성(II)

  • 정진웅;정승원;박기재;김동진
    • Proceedings of the Korean Society of Postharvest Science and Technology of Agricultural Products Conference
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    • 2003.10a
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    • pp.145.2-146
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    • 2003
  • 일반 근채류와는 달리 기계적, 화학적 박피방법이 불가능한 도라지는 수작업에 의한 박피만이 가능하여 다양한 수작업에 의한 박피 처리후의 품질을 비교한 결과, 감모율에 있어 박피 도구를 사용한 수작업시 15.93%로 박피 도중 제거되는 측근의 수가 많아 높게 나타났다. 박피 처리후의 수분함량 변화는 칼을 이용한 수작업 처리구에서 초기치 88.26%에서 3시간후 71,55%로 16.71%의 감소율을 보였으며, 박피 도구를 사용한 수작업 처리구에서는 14.38%, sandpaper에 의한 수작업 처리구는 16%의 수분함량 감소율을 보였다. 한편, 우엉의 박피 감모율은 다른 품목과는 달리 칼을 이용한 수작업 박피에서 18.20%로 가장 크게 나타났으며, brushing에 의한 박피가 8.05%로 가장 적은 감모율을 나타내었다. 박피 처리후의 수분함량 변화는 박피 도구를 이용한 수작업 처리구가 80.50~71.30% 범위로,7$0^{\circ}C$, 12%-NaOH 에서 30초간 처리한 우엉의 80.56~69.54% 보다 다소 높게 유지되었다. pH 변화도 6.58~5.67 수준으로 다른 근채류와 마찬가지로 큰 변화가 없는 것으로 나타났다. 또한, brushing에 의한 방법은 박피 직후에 갈변도가 0.85로 다소 높게 나타났으나 시간이 경과함에 따라서는 갈변정도가 더디게 진행되는 특징을 보여 주었다.

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Turbine Performance Degradation Due to Blade Surface Roughness (블레이드 표면거칠기에 따른 터빈 성능저하)

  • Park, Il-Young;Yun, Yong-Il;Song, Seung-Jin
    • 유체기계공업학회:학술대회논문집
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    • 2003.12a
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    • pp.92-98
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    • 2003
  • Turbine blades experience significant surface degradation with service. This paper presents experimental evidence of blade surface roughness reducing turbine efficiency. Performance tests were conducted in a low speed, single-stage axial flow turbine rig with roughened blade surfaces. Sheets of sandpaper with equivalent sandgrain roughnesses of 106 and $400{\mu}m$ were used to roughen the blades. In these tests, effects of roughened stator vanes and rotor blades were separately evaluated. In the fully rough regime ($k_{s}=400{\mu}m$), the experimental results show an 11 percent decrease in normalized efficiency with roughness only on stator vanes ; an 8 percent decrease with roughness only on rotor blades ; and a 19 percent decrease with roughness on both the stator and rotor blades. In the transitionally rough regime ($k_{s}=106{\mu}m$), the trends are similar approximately 4 percent decrease with either roughened stator or roughened rotor and an 8 percent decrease with roughness on both stator and rotor blades. Thus, roughened stator vanes incur more performance penalty than roughened rotor blades.

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EVALUATION OF THE ACCURACY OF THE ELECTRONIC APEX LOCATOR USING THE POLARIZING MICROSCOPE (편광현미경을 이용한 전자적근관장측정기의 정확성에 관한 연구)

  • Park, Han-Soo;Yoon, Soo-Han
    • Restorative Dentistry and Endodontics
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    • v.17 no.1
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    • pp.235-243
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    • 1992
  • The purpose of this study was to evaluate the accuracy of an electronic apex locator, the Neosono - M, in determining the location of the cementodentinal junction. A total of 26 teeth with 46 canals were evaluated. The apex locator was used to locate the file and the teeth extracted. The specimen were prepared with highspeed burs and sandpaper discs to a thickness of $250{\sim}300{\mu}m$. Distances were measured from the cementodentinal junction with the use of polarizing microscope. Measurements made by the apex locator were also compared with those by the X - ray. The results were as follows. 1. The apex locator and X - ray were to measure a mean value of 0.17, 0.45mm coronal to the CDJ respectively. There was no significant difference between the accuracy of the apex locator and that of X - ray. 2. There was no significant difference between the accuracy of apex locator in vital and in nonvital teeth, and between in narrow and in wide canals. 3. The files in nonvital and narrow group were apical to the CDJ significantly than those of vital and narrow, vital and wide, and non vital and wide groups.

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The Effect of Mo Addition on Oxygen Vacancies in the Oxide Scale of Ferritic Stainless Steel for SOFC Interconnects

  • Dae Won Yun;Hi Won Jeong;Seong Moon Seo;Hyung Soo Lee;Young Soo Yoo
    • Corrosion Science and Technology
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    • v.23 no.1
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    • pp.33-40
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    • 2024
  • The concentration and diffusion coefficient of oxide ion vacancies in the oxide scale formed on Fe-22Cr-0.5Mn ferritic stainless steel with and without molybdenum (Mo) was measured at 800℃ by the electrochemical polarization method. After pre-oxidation for 100 h in ambient air at 800 ℃, the oxide scale on one side was completely removed with sandpaper. A YSZ plate was placed on the side where the oxide scale remained. Platinum (Pt) meshes were attached on the top of the YSZ plate and the side where the oxide scale was removed. Changes in electrical current were measured after applying an electrical potential through Pt wires welded to the Pt meshes. The results were interpreted by solving the diffusion equation. The diffusion coefficient and concentration of oxide ion vacancy decreased by 30% and 70% in the specimen with Mo, respectively, compared to the specimen without Mo. The oxide ion vacancy concentration of chromia decreased due to the addition of Mo.