• Title/Summary/Keyword: sample compositions

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Punch Properties of Some Vegetables (몇가지 채소류의 펀치특성)

  • Min, Young-Kyoo;Jeong, Heon-Sang
    • Korean Journal of Food Science and Technology
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    • v.29 no.2
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    • pp.273-278
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    • 1997
  • In order to investigate the punch properties of some vegetables-cucumber, radish, garlic, ginger and potato-force, distance, and time were measured with a texturometer, and the correlations between compositions and cell characteristics of samples were characterized. Many reflection and rupture points on the force-distance and distance-time curve were observed, and these points appeared when the cells of sample were resisted and yielded against the applied force. They were big and clear at the slow crosshead speed. The regression analysis for force-time and distance-time to the rupture point showed $R^{2}>0.95$. The rupture time and rupure force were 5.63 sec, 4.88 N in ginger and 4.15 sec, 2.00 N in cucumber. The rupture forces become large values at the fast crosshead speed. As cell sizes were increased, the moisture content and rupture distance were increased, while the viscosity of juice, density, regularity of cell, and slope of force-time were decreased. Rupture force, time and distance were decreased at the large specific gravity of samples. The slopes of distance-time curve were inversely proportional to slope of force-time curve.

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Fatty Acid Compositions of Cultured Oyster (Crassostrea gigas) from Korean and Japanese Spats

  • Jeong Bo-Young;Moon Soo-Kyung;Jeong Woo-Geon
    • Fisheries and Aquatic Sciences
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    • v.2 no.2
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    • pp.113-121
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    • 1999
  • Changes in lipid content, lipid class and fatty acid compositions of the cultured oysters in shallow-water, Bukman bay (Tongyeong, Korea), using both Korean and Japanese spats were investigated. The content of non-polar lipid (NL) comprised approximately $60- 80\%$ of total lipid (TL) in the cultured oysters. There was a positive correlation between NL content and meat weight, y=0.287lx-15.309 (r=0.834l, p<0.001). The prominent fatty acids of the oysters were 16:0, 20:5n-3 (eicosapentaenoic acid, EPA), 22:6n-3 (docosahexaenoic acid, DHA), 18:0, l8:1n-7, l8:1n-9, l6:1n-7, 14:0 and l6:4n-3. During the growth of the oysters, l6:4n-3 showed the highest coefficient of variation, accounting for $41.8\%$ for the Korean oyster and $32.3\%$ for the Japanese one, respectively. Both oysters showed low level of n-3 fatty acids such as DHA and EPA and high level of n-6 fatty acid, 20:4n-6, in the spawning period (August). During growth of the oysters, both EPA and DHA were the richest fatty acids in the harvest period (December, 314 mg/100g sample) and in the pre-spawning period (July, 237-247 mg/100g sample), respectively. Consequently, the cultured oyster with Japanese spat contained approximately two times more n-3 fatty acids per oyster individual than those with Korean one in the harvest season.

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백두산 화산군 환경과 동굴 암석의 년대측정 및 성분분석

  • 김경훈
    • Journal of the Speleological Society of Korea
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    • v.34 no.35
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    • pp.32-42
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    • 1993
  • The Paektu-san mountains are geographically situated in the Korea strait to the north of the main peninsula, coordinated between the longitudes of W(127$^{\circ}$15'~128$^{\circ}$00')and E(128$^{\circ}$15'~129$^{\circ}$00'), and between the latitudes of S(41$^{\circ}$15'~42$^{\circ}$00') and N(42$^{\circ}$10'~42$^{\circ}$40'). The volcanic group of the Paektu-san mountains can be devided into 2 main kinds of volcanos by the method investigation, The ashes are mainly made of tremolite, trachte, basalt and pumice, or, a little quartz, labradorite and volcanic glass. These sorts, ratios and forms of the rocks are respectively similar. The Haeven lake is surrounded by 19 peaks. The central volcanic cone is a secant cone in shape, with an altitude of the 1800m to 2749,2m (Chang-kun-bong), an average diameter of 10km, and a shape of an ellipse seen high from the plane. They say there were several eruptions in 1668, 1700 and 1702 A. D. The crystal structure of the rock sample collected at the cave of Mt. Paektu-san is monoclinic. The quantitative analysis of the rock samples in the cave is done by using XRF this time. The chemical compositions by XRF fundamamental parameter analysis is : SiO$_2$: 50.72Wt%, TiO = 2.422Wt%, $Al_2$O$_3$= 17.65Wt%, Fe$_2$O$_3$= 9.371Wt%, CaO = 8.711Wt%, MgO = 4.l19Wt%, MnO = 0.l15Wt%, $K_2$O = 1.369Wt%, Na$_2$O : 3.028Wt% and P$_2$O$_{5}$ = 0.365Wt%. The K-Ar age of the rock sample is also determined to be 0.16Ma. This paper describes some problems experienced in dating young volcanic rocks, and then discusses chemical compositions, X-ray fluorescence analyses and the age of the formation of a lava tunnel such as in Mt. Paektu-san.n.

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Preparations and Magnetic Properties of Aluminum Anodic Oxidized Films Electrodeposited Cobalt-Iron Alloys (코발트-철을 전해석출한 양극산화피막의 제작과 자기특성)

  • 강희우
    • Journal of the Korean Magnetics Society
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    • v.4 no.1
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    • pp.25-31
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    • 1994
  • The magnetic properties of aluminum anodized film in which Co-Fe alloy electrodeposited are investigated with regard to the alloy composition of magnetic films. The electrodeposited Co-Fe particles are confirmed to be single phase Co-Fe alloys by X-ray diffractions. At 34 at% Co, the sample with small pore diameter(particle diameter $150\;{\AA}$) has a large magnetic energy product($B_{max}$) of about 1.44 MGOe due to the large saturation magnetization, the high coercive force and good squareness of the M-H curve. However, for the samples with particle diameter larger than $450\;{\AA}$, the bottom of each particle forms abnormal particle claaed branch-shaped unlike the sample of the particle diameter $150\;{\AA}$. In this case, the magnetic anisotropy energy was about zero at the compositions of 45 and 75 at% Co. Moreover, at the compositions from 50 to 70 at% Co, the anisotropy became negative value. This means that an easy axis of magnetization of the film is in plane in plane in spite of the perpendicular shape anisotropy of the particle. It was found that the bottom extremity of the particle contains FeC from the X-ray diffraction. Thus the effect of the bottom extremity, that is, an unusal magnetic property was removed by electrodepositing Cu at the bottom extremity of the particle. Itis clear that the magnetic properties of the ilms are influenced by he branch-shaped bottom extremity filled with FeC.

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Characteristic of Electrical Conductivity in the $\textrm{CuO}-\textrm{Bi}_{2}\textrm{O}_3-\textrm{V}_2\textrm{O}_5$ Glass System with Various Compositions ($\textrm{CuO}-\textrm{Bi}_{2}\textrm{O}_3-\textrm{V}_2\textrm{O}_5$계 글라스에서 조성 변화에 따른 전기 전도도의 특성)

  • Park, S.S.;Jeong, D.J.;Lee, H.;Park, C.Y.;Min, S.K.;Park, H.C.
    • Korean Journal of Materials Research
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    • v.8 no.12
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    • pp.1110-1114
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    • 1998
  • The crystallization behaviors and electrical conductivities of the glasses heat-treated at various times and temperatures in the CuO-Bi$_2$O$_3$-V$_2$O$_{5}$ glass system were investigated. Among glass samples with various compositions, the highest conductivity obtained in the 31CuO-14Bi$_2$O$_3$-55V$_2$O$_{5}$ (mol%) glass sample. The 31CuO-14Bi$_2$O$_3$-55V$_2$O$_{5}$ (mol%) glass sample crystallized by heat treatment at 358$^{\circ}C$ for 8h had 2.67$\times$10$^{-2}$ $\Omega$$^{-1}$ $cm^{-1}$ /, which was much high value as a solid electrolyte. Compared to the glass sample, the heat- treated glass sample was increased in conductivity by an order of 10$^3$-10$^4$due to the formation and growth of BiVO$_4$ and CuVO$_3$crystals.

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Comparative Study on the Effects of Combined Treatments of Lactic Acid Bacteria and Cellulases on the Cell Wall Compositions and the Digestibility of Rhodesgrass (Chloris gayana Kunth.) and Italian Ryegrass (Lolium multiflorum Lam.) Silages

  • Ridla, M.;Uchida, S.
    • Asian-Australasian Journal of Animal Sciences
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    • v.12 no.4
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    • pp.531-536
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    • 1999
  • This study was conducted to compare the effects of lactic acid bacteria (LAB) or LAB+cellulases on the cell wall compositions and the in vitro dry matter digestibility (IVDMD) of Rhodesgrass (RG) and Italian ryegrass (IRG) silages. LAB (Lactobacillus cassei) at a concentration of $10{\times}10^5\;cfu.g^{-1}$ fresh forage was added to all ensiling samples (except the untreated control) of RG and IRG. The cellulases used were Acremoniumcellulase (A), Meicelase (M) or a mixture of both (AM). Each cellulase was applied at levels of 0.005, 0.01 and 0.02 % fresh sample. The samples were incubated at 20, 30 and $40^{\circ}C$ for about 2 months of storage. LAB inoculation did not affect cell wall components or IVDMD of both the RG and IRG silages, but LAB+cellulase treatments did. Increasing the amount of cellulase addition resulted in further decreases of cell wall concentrations. This reduction more markedly occurred with cellulases A and AM than it did with cellulase M. Cell wall components losses were higher in the IRG silages than in the RG silages. LAB+cellulase treatments decreased IVDMD of the RG silages, but had no effect on the IRG silages. The different effect of LAB+cellulase treatments on cell wall degradation and IVDMD of the RG and IRG silages suggested that RG contains more structural carbohydrates, which were difficult to degrade with cellulase, than did IRG.

Characterization of Molecular Composition of Bacterial Melanin Isolated from Streptomyces glaucescens Using Ultra-High-Resolution FT-ICR Mass Spectrometry

  • Choi, Mira;Choi, A Young;Ahn, Soo-Yeon;Choi, Kwon-Young;Jang, Kyoung-Soon
    • Mass Spectrometry Letters
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    • v.9 no.3
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    • pp.81-85
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    • 2018
  • In this study, the chemical composition of bacterial melanin isolated from the Streptomyces glaucescens strain was elucidated by ultra-high-resolution Fourier transform ion cyclotron resonance (FT-ICR) mass spectrometry. Ultra-high-resolution mass profiles of the microbial melanin product were acquired using a 15 Tesla FT-ICR mass spectrometer in positive and negative ion modes via electrospray ionization to obtain more complete descriptions of the molecular compositions of melanin-derived organic constituents. A mass resolving power of 500,000 (at m/z 400) was achieved for all spectra while collecting 400 scans per sample with a 4 M transient. The results of this analysis revealed that the melanin pigment isolated from S. glaucescens predominantly exhibits CHON and CHO species, which belong to the proteins class of compounds, with the mean C/O and C/N ratios of 4.3 and 13.1, thus suggesting that the melanin could be eumelanin. This analytical approach could be utilized to investigate the molecular compositions of a variety of natural or synthetic melanins. The compositional features of melanins are important for understanding their formation mechanisms and physico-chemical properties.

TSSG growth, morphology and properties of potassium lithium niobate (KLN) crystals

  • Chong, Tow-Chong;Xu, Xue-Wu;Lian Li;Zhang, Guang-Yu;H. Kumagai;M. Hirano
    • Proceedings of the Korea Association of Crystal Growth Conference
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    • 1999.06a
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    • pp.167-185
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    • 1999
  • In the present paper, KLN crystals have been grown along <001>, <100> and <110> directions by the top seeded solution growth (TSSG) method from Li-richer melts with different compositions. The morphologies of KLN crystals grown along different directions have been studied, and the well-developed facets have been unambiguously indexed using X-ray goniometer and stereographic projection analysis. The growth mechanism and defects such as cracks and inclusions were discussed on the basis of observations of facets on the crystal-melt interfaces. The crystal compositions were determined by chemical analysis method. The structure and lattice constants of KLN crystals were determined and calculated on the basis of XRD data by using TREOR90 and PIRUM programs. The Curie temperature and optical absorption were determined by dielectric constant peak and spectrum measurements, respectively. The blue SHG characteristics of a KLN sample were also investigated using a pulsed dye laser. PACS: 42.70.M;81.10;81.10A;42.65.K.

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TSSG growth, morphology and properties of potassium lithium niobate (KLN) crystals

  • Chong, Tow-Chong;Xu, Xue-Wu;Li, Lian;Zhang, Guang-Yu;Kumagai, H.;Hirano, M.
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.9 no.4
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    • pp.396-401
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    • 1999
  • In the present paper, potassium lithium niobate(KLN) crystals have been grown along <001>, <100> and <110> directions by the top seeded solution growth (TSSG) method from Li-richer melts with different compositions. The morphologies of KLN crystals grown along different directions have been studied, and the well-developed facets have been unambiguously indexed using X-ray goniometer and stereographic projection analysis. The growth mechanism and defects such as cracks and inclusions were discussed on the basis of observations of facets on the crystal-solution interfaces. The crystal compositions were determined by a chemical analysis method. The structure and lattice constants of KLN crystals were determined and calculated on the basis of XRD data by using TREOR90 and PIRUM programs. The Curie temperature and optical absorption were determined by dielectric constant peak and spectrum measurements. respectively. The blue second harmonic generation (SHG) characteristics of KLN sample were also investigated using a pulsed dye laser.

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Modification of Retention Factor of Mononucleotides by Compositions of Buffers and Methanol in RP-HPLC (RP-HPLC에서 Buffer와 메탄올의 조성에 의한 Mononucleotides 체류인자의 조절)

  • 강덕희;이주원;노경호
    • KSBB Journal
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    • v.15 no.5
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    • pp.452-457
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    • 2000
  • Due to the advantage of RP-HPLC with a variety of compositions of mobile phases, experiments on water-soluble charged species were examined. The samples were mononucleotides (5-CMP, 5-UMP, 5-GMP, 5-IMP, 5-AMP), and the buffers used were sodium phosphate monobasic and acetic acid. The concentrations of buffers ranged from 0.01 to 10 mM, while that of the methanol, an additive to the mobile phase was 5 to 20 vol.%. To predict the retention factor of a sample in terms of its methanol composition (M, vol.%) and buffer(C(sub)B, mM), the following nonlinear equation is suggested, k= $\frac{a+b C_B}{(1+c C_B) M^d}($ where a, b, c, and d were experimentally determined constants. The regression coefficients were above 0.96, and the agreement between experimental and calculated retention factors were relatively good.

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