• Title/Summary/Keyword: salt analysis

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Preparation and Chrominance of Metal Oxide Coated Titania/Mica Pearlescent Pigment (금속산화물이 코팅된 마이카 티타니아 진주광택 안료의 제조 및 색차변화)

  • Lee, Kwan-Sik;Kang, Kuk-Hyoun;Lee, Jin-Hee;Lee, Dong-Kyu
    • Journal of the Korean Applied Science and Technology
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    • v.30 no.2
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    • pp.233-243
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    • 2013
  • The inorganic pearlescent pigment have high physical and chemical stability, thus it is used in a variety field, which has better light stability, solvent resistance and thermostability. In this paper, we were synthesized the pearlescent pigment for cosmetics which was coated cobalt chloride for base of blue color metal oxide on mica titania substrate using hydrothermal synthesis method. To complement the color of the pigment by cobalt, pearl pigment were coated by different metal salt and cobalt ratio, to implement a variety of color value, depending on the kind of metal salts were synthesized. Synthesized pearlescent pigments appear various color as kind of added metal salt precursor and molar ration of cobalt and other metals. We controlled coating and color by composition of metal salt and type of metal salts, and that confirm the pigment characteristics of color changes through the analysis of color difference meter. Synthesized pigment was characterized by SPM, SEM, XRD, and EDS.

Fabrication and Characterization of PCL/TiO2 Nanoparticle 3D Scaffold (PCL/TiO2 Nanoparticle 3차원 지지체 제조 및 특성 평가)

  • Kim, Jung-Ho;Lee, Ok Joo;Sheikh, Faheem A.;Ju, Hyung Woo;Moon, Bo Mi;Park, Hyun Jung;Park, Chan Hum
    • Polymer(Korea)
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    • v.38 no.2
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    • pp.150-155
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    • 2014
  • Polycaprolactone (PCL) is a synthetic biodegradable polymer with excellent mechanical properties. $TiO_2$ (titanium dioxide) has a hydrophilic, high density and excellent biocompatibility. In this work, we produced three-dimensional porous scaffolds with PCL and $TiO_2$ nanoparticles using a salt-leaching method. Physical properties of the scaffolds were analyzed by FE-SEM, FTIR, TGA and compressive strength. Interestingly, the addition of $TiO_2$ nanoparticles decreased the water absorption and swelling ratio of the porous scaffolds. However, the compressive strength was increased by $TiO_2$. CCK-8 assay, which is generally used for the analysis of cell growth, shows that $TiO_2$ nanoparticles have no cytotoxicity. Taken together, we suggest that the PLC/$TiO_2$-scaffold can be used for biomedical applications.

Permeate Flux Analysis of Direct Contact Membrane Distillation (DCMD) and Sweep Gas Membrane Distillation (SGMD) (직접접촉식과 동반기체식 막증류 공정의 투과수 변화에 따른 비교해석)

  • Eum, Su-Hwan;Kim, Albert S.;Lee, Yong-Taek
    • Membrane Journal
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    • v.21 no.3
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    • pp.236-246
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    • 2011
  • In this study, we used prepared a cylindrical module consisting 100 hollow fibers of commercialized (hydrophobic) polyethylene membrane of $0.4{\mu}m$ pore size and systematically studied performance of direct contact membrane distillation (DCMD) and sweep gas membrane distillation (SGMD) in terms of variation of permeate flux and salt rejection with respect to temperature drop across the membrane, salt concentrations in feed, and flow rates of cooling water and sweep gas. SGMD was regarded as DCMD with a sweep gas layer between permeate-side membrane surface and cooling water. Sweep gas flow decreases the permeate flux from that of DCMD by providing an additional gas-layer resistance. We compared DCMD and SGMD performance by using mass balance with a fitting parameter (${\omega}$), indicating fraction of permeate flow rate.

Development of 3-D Hydrodynamical Model for Understanding Numerical Analysis of Density Current due to Salinity and Temperature and its Verification (염분과 온도차에 의한 밀도류 해석을 위한 3차원 동수역학적 수치모델의 개발 및 검증)

  • Lee, Woo-Dong;Hur, Dong-Soo
    • KSCE Journal of Civil and Environmental Engineering Research
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    • v.34 no.3
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    • pp.859-871
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    • 2014
  • In order to analyze the density current due to salt and temperature difference, this study develops new numerical model (LES-WASS-3D ver. 2.0) by introducing state equation for salt and temperature and 3D advection-diffusion equation to existing 3D numerical wave tank (LES-WASS-3D ver. 1.0). To verify the applicability, the newly-developed numerical model is analyzed comparing to the experimental result of existing numerical model. In the result, it well implement the behavior and vertical salt concentration of advected and diffused seawater as well as flow velocity and temperature of the discharged warm water. This confirms the validity and effectiveness of the developed numerical model.

Subsurface Water Storage Using Coastal Aquifers Filled With Saline Water (염수로 포화된 해안지역 대수층을 활용한 수자원확보 방안)

  • Jung, Eun Tae;Park, Namsik;Kim, In Chul;Lee, Seoung Hwi
    • Journal of Korean Society of Coastal and Ocean Engineers
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    • v.27 no.5
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    • pp.353-357
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    • 2015
  • A new method is proposed for water resources using aquifers in coastal areas. These aquifers are generally filled with saline water due to seawater intrusion and consequently being left unutilized. Surface water can be injected into these aquifers and recovered for water quality enhancement and stored water. Injection and pumping wells are used. For this technique to be successful protection of pumping well from seawater intrusion is an essential issue. Salt water pumping can be used to prevent saline water upconing. Numerical analysis demonstrated that a properly designed and executed salt water pumping well can protect a freshwater pumping well from salt water intrusion.

A rapid determination of chloride in saturated paste extracts of salt-affected soils using EC change upon AgCl precipitation (AgCl 침전 전후 전기전도도 변화를 이용한 염해지 포화침출액의 염소 이온 신속 정량)

  • Lee, Yehun;Kim, Jeeyoon;Lee, Jeongsu;Pros, Khok;Park, Jee Won;Han, Gwang Hyun
    • Journal of Applied Biological Chemistry
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    • v.60 no.3
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    • pp.279-282
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    • 2017
  • Chloride is known as the most important anion in salt-affected soils. We observed the degree of EC change upon AgCl precipitation was quantitatively related with the chloride concentration. Method validation and intercomparison with ion chromatography revealed the proposed method can provide rapid and moderately precise chloride concentrations in salt-affected soils.

Effect of Zeolite Application on Growth and Yield of Chinese Cabbage and Chemical Properties of Soil Under Greenhouse Cultivation

  • Kim, Lee-Yul;Kim, Ki-In;Kang, Seong Soo;Kim, Jung-Ho;Jung, Kang-Ho;Hong, Soon-Dal;Lee, Won-Hee
    • Korean Journal of Soil Science and Fertilizer
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    • v.48 no.3
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    • pp.218-224
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    • 2015
  • Zeolite may help crop growth, yield increase, and salt removal. Field experiment under greenhouse cultivation was conducted to study the effect of zeolite application on growth and yield of Chinese cabbage (Brassica campestris L.) and soil. Soil was classified as Gyuam series (coarse silty, mixed, nonacid, mesic family of Aquic Fluvaquentic Eutrudepts). Six zeolite rates were 0, 3, 5, 10, 20 and $40Mg\;ha^{-1}$. Experimental design was a completely randomized design. Chinese cabbage was grown three times consecutively. Established plant number of plant and yield as fresh weight (F.W.) were measured and soil samples were taken before and after harvesting. Chinese cabbage yield was $76.9Mg\;ha^{-1}$ at a rate of $20Mg\;zeolite\;ha^{-1}$, $54.3Mg\;ha^{-1}$ at a rate of $5Mg\;zeolite\;ha^{-1}$, and $51.3Mg\;ha^{-1}$ at control (no zeolite), respectively. Second order regression analysis using zeolite rate and yield showed that optimum zeolite application rate was between 24 and $26Mg\;ha^{-1}$. The regression equation explained about 88% of the yield variability. The electrical conductivity (EC) decreased from 3.2 to $1.0dS\;m^{-1}$ for all treatments so that salt accumulation was not a concern. Based on the results, we recommend that optimum zeolite application rate is between 20 and $24Mg\;ha^{-1}$ for Chinese cabbage under greenhouse cultivation.

Theoretical Study of Boric Acid Determination In Nickel Plating Solution (니켈 도금액의 붕산분석에 관한 연구)

  • 염희택
    • Journal of Surface Science and Engineering
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    • v.4 no.1
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    • pp.5-15
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    • 1971
  • "Rapid Determination of Boric Acid in Nickel Plating Solution" by the addition of Na$_2$C$_2$O$_4$ and thus preventing the precipitation of i(OH)$_2$ during titiration , has previously been reported. In this paper, the exact amount of glycerine and the complexing possibility of oxalate with nickel has been determined by measn of conductivity titrations. This experimental work has been supported by the mathematical application of the Debye-Huckel and mass action equitions as well as statistical analysis. The results were ; (1) Fro determining boric acid in nickel plating solution, 20 ml of 400ml/ι glycerine was sufficient, since 97% of the H$_3$BO$_3$ was dissoicated by this addition. (2) In the absence of Na$_2$C$_2$O$_4$ the continious precipitation of Ni(OH)$_2$ during titration with NaOH even past end -point for boric acid determination resulted in considerable anlaytical error. (3) In the presence of Na$_2$C$_2$O$_4$ during titration , Ni++ combined with C$_2$O$_4$-to form NiC$_2$O$_4$. The solution with this precititate of very fine, colloidal , trantsparent particles, remained quite clear for approximately 2 hours. Therefore it was shown that the presence of Na$_2$C$_2$O$_4$ prevents the formation of gross Ni(OH)$_2$ precititation by forming NiC$_2$O$_4$ instead of a complex salt with Ni++ , which did not interfere with the visible determination of the end point for boric acid with NaOH titation. This observous may be interpreted in the light of the previously published solubility ratio for NiC$_2$O$_4$ and Ni(OH)$_2$, 0.3mg/100g H$_2$O(25$^{\circ}C$), respectively. Precipitation of the less soluble , albeit transparent salt, NiC$_2$O$_4$ precluded therefore the precipitation of the Ni(OH)$_2$ salt.

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Construction of a Network Model to Reveal Genes Related to Salt Tolerance in Chinese Cabbage (배추 염 저항성 관련 유전자의 네트워크 모델 구축)

  • Lee, Gi-Ho;Yu, Jae-Gyeong;Park, Ji-Hyun;Park, Young-Doo
    • Horticultural Science & Technology
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    • v.32 no.5
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    • pp.684-693
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    • 2014
  • Abiotic stress conditions such as cold, drought, and salinity trigger physiological and morphological changes and yield loss in plants. Hence, plants adapt to adverse environments by developing tolerance through complex regulation of genes related to various metabolic processes. This study was conducted to construct a coexpression network for multidirectional analysis of salt-stress response genes in Brassica rapa (Chinese cabbage). To construct the coexpression network, we collected KBGP-24K microarray data from the B. rapa EST and microarray database (BrEMD) and performed time-based expression analyses of B. rapa plants. The constructed coexpression network model showed 1,853 nodes, 5,740 edges, and 142 connected components (correlation coefficient > 0.85). On the basis of the significantly expressed genes in the network, we concluded that the development of salt tolerance is closely related to the activation of $Na^+$ transport by reactive oxygen species signaling and the accumulation of proline in Chinese cabbage.

Prokaryotic Communities of Halophilic Methylotrophs Enriched from a Solar Saltern (염전으로부터 농화배양된 호염 메틸영양미생물 군집의 특성)

  • Kim, Jong-Geol;Park, Soo-Je;Rhee, Sung-Keun
    • Korean Journal of Microbiology
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    • v.46 no.3
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    • pp.286-290
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    • 2010
  • C-1 compounds are observed in anaerobic sediment of high salt environments. Thus, surface sediments and waters from these environments are therefore potential habitats for aerobic methylotrophic microorganisms. The soil samples collected from saltern and tidal flat as inoculums and methanol as carbon and energy source was supplied. After subculture depending on the salt concentration, methanol oxidizing bacteria growth condition investigated, the results of methanol oxidizing bacteria can grow in salt conditions, and the maximum concentration was 20%. Analysis based on denaturing gradient gel electrophoresis of 16S rRNA genes indicates that Methelyophaga-like bacteria were dominants of methylotrophs in the enrichment culture. Quantitative PCR showed that archaeal cells were about 1-10% of bacterial cells. Additionally archaea were assumed not to be involved in methanol oxidation since bacterial antibiotics completely blocked the methanol oxidation. Our results suggest that Methelyophaga-like bacteria could be involved in C-1 compounds oxidation in hypersaline environments although those activities are sensitive to salinity above 20%.