• 분석과학
• /
• 제21권6호
• /
• pp.518-525
• /
• 2008

포도, 고추, 배추, 토마토 및 감자 등 5종 농산물에 대하여 mandelamide계 신규 살균제인 mandipropamid의 잔류분석법을 확립하였다. 각 농산물을 세절한 시료에 methanol을 가하고 고속마쇄하여 잔류분을 추출하였다. 추출액을 포화식염수와 증류수로 희석하고 dichloromethane으로 분배하여 극성분순물을 제거하였으며, Florisil 흡착크로마토그래피법으로 추가 정제하였다. Mandipropamid의 HPLC/UV 검출기상 최소검출량은 2 ng (S/N>10, 0.01 AUFS)이었고 시료추출물 중 불순물에 의한 간섭은 관찰되지 않았다. 무처리 포도, 토마토, 고추, 배추 및 감자에 대하여 2수준 3반복으로 회수율을 산출한 결과 각각 $99.8{\pm}1.7$ (n=6), $89.3{\pm}5.3$(n=6), $98.7{\pm}2.2$ (n=6), $99.7{\pm}6.8$ (n=6) 및 $91.1{\pm}3.1$ (n=6)이었으며, 분석법의 정량한계는 0.02~0.04 mg/kg이었다. 아울러 검출된 잔류분은 재확인을 위하여 selected-ion monitoring (SIM)을 이용한 LC/MS법을 추가로 확립하였다. 본 연구에서 확립된 mandipropamid의 잔류분석법은 검출감도 및 재현성을 고려할 때 공정분석법으로 사용이 가능하였다.

• 한국철도학회:학술대회논문집
• /
• 한국철도학회 2010년도 춘계학술대회 논문집
• /
• pp.282-291
• /
• 2010

In line with current speed-up of railroad, a slab track has been increasingly adopted in a bid to secure the safety of track structure as well as to reduce the maintenance cost, and furthermore, the need for commercialization of domestically-developed swing-nose crossing turnout on slab track has been on the rise. For commercialization of swing-nose crossing turnout on slab which was developed in Korea, a technical and systematic performance evaluation system, considering local environment, shall be established and then the performance evaluation shall be accordingly implemented. This paper was intended to summarize the performance evaluation system, referring to the data available at home and abroad and the results of performance evaluation for domestically-developed swing-nose crossing turnout on slab track carried out to date based on that system. A performance evaluation system comprises the technical requirement appropriateness evaluation(component performance evaluation and design verification), laboratory test and on-site test. For domestically-developed swing-nose crossing turnout on slab track, appropriateness evaluation and laboratory test have been completed and the on-site test of those installed on the 2nd phase of Kyung-Bu HSR is underway now.

• Food Science and Biotechnology
• /
• 제16권6호
• /
• pp.868-872
• /
• 2007

The microbiological and chemical identification of antibiotic residues was attempted for livestock and seafood products including pork (n=34), beef (n=34), chicken (n=32), flatfish (n=37), armorclad rockfish (n=36), and sea bream (n=27). The meat (n=100) and seafood (n=100) samples were collected from 9 markets in 5 major Korean cities. Antibiotic substances were identified from the classes of tetracyclines, macrolides, penicillins, aminoglycosides, polyethers, peptides, sulfonamides, quinolones, chlorampenicols, and novobiocins using a microbiological assay, the Charm II test and high performance liquid chromatography (HPLC) with ultra violet (UV) and fluorescence detectors. The results showed that 2 tetracyclines (oxytetracycline and tetracycline) and 3 quinolones (ciprofloxacin, norfloxacin, and enrofloxacin) were detected in 4 samples of flatfish among all 100 seafood samples tested. No antibiotic residues were detected in the 100 livestock product samples tested. The amounts (min-max, mg/kg) of the residual antibiotics were as follows; tetracycline 0.78-0.85, oxytetracycline 0.49-0.74, ciprofloxacin 0.09-0.83, norfloxacin 0.01-0.21, enrofloxacin 0.12-2.98. These data indicate that the total detection rate of antibiotics in livestock and seafood products was approximately 2%.

• 분석과학
• /
• 제34권4호
• /
• pp.160-171
• /
• 2021

Synthetic azo dyes are used extensively in herbal medicines to render the medicines more visually attractive to consumers. This study developed and validated a rapid high-performance liquid chromatography (HPLC) method to determine whether synthetic colorants such as Tartrazine, Auramine O, Metanil yellow, Sunset yellow, and Orange II are used extensively in Typha orientalis. To increase the recovery of the synthetic dyes, this method employed containing 50 mM ammonium acetate in 70 % methanol at first extraction and 100 mM HCl in 70 % methanol at second extraction. Five synthetic pigments in Typha orientalis were separated by gradient elution with a mobile phase consisting of acetonitrile and 50 mM ammonium acetate in distilled water at ultra-violet (UV) detection 428 nm or 500 nm. Additionally, this study established the liquid chromatography tandem mass spectrometry (LC-MS/MS) method to confirm positive samples suspected by HPLC results. The HPLC-UV method had good linearity, indicating r²> 0.999. The recoveries of the samples spiked with three different concentration ranged from 73.8~91.5 %, and relative standard deviation values indicated 0.2~5.2 %. The established LC-MS/MS could successfully identify the synthetic pigments in herbal medicine samples. The study demonstrates that Typha orientalis adulterated by yellowish synthetic dyes can be successfully distinguished when using the HPLC-UV method.

• 한국유체기계학회 논문집
• /
• 제17권1호
• /
• pp.5-11
• /
• 2014

The purpose of this paper is to investigate an analytical approach for opening performance evaluation of the nuclear pressure safety valve based on standard codes such as ASME or KEPIC. It is well-known that safety valve is considered as one of pressure relief valves for protecting a boiler or pressure vessel from exceeding the maximum allowable working pressure. When pressure in a container reaches its set pressure, the safety valve commences discharging the internal fluid by a sudden opening called as popping. Safety valve is usually evaluated by set pressure, full open, blow-down, leakage and flow capacity. The test procedure and technical requirement for performance evaluation is described in international code of ASME code such as BPVC. The opening characteristics of steam safety valve can be analyzed by computational fluid dynamics (CFD) and steam shaft dynamics. First, the flow analysis along opening process is simulated by running the CFD models of the ten types of opening steps from 0 to 100%. As a analysis result, the various CFD outputs of flow pattern, pressure, forces on the disc and mass flow at each simulation step is demonstrated. The lift force is calculated by using the forces applied on disc from static pressure and secondary flow. And, the effect of huddle chamber or control chamber is studied by dynamic analysis based on CFD simulation results such as lift force. As a result, dynamics analysis shows opening features according to the sizes of control chamber.

• 해양환경안전학회:학술대회논문집
• /
• 해양환경안전학회 2003년도 춘계학술발표회
• /
• pp.31-40
• /
• 2003

There are winds and waves in the sea, and they are changed frequently in accordance with the weather. By analyzing them which have the closest relation to the ship's safe voyage. evaluating the seakeeping performance and then taking a proper action, navigators should carry out safe navigation on the sea. A ship in seaways suffers continuous disturbances by irregular waves, and ship motions with irregular waves cannot be easily described as a system model which is adequate to a control system. But, in general, for seakeeping analysis, ship motions in irregular seas can be estimated by the superposition of the motion responses in regular wave components of the sea spectrum. After comparing and analyzing the winds and waves in major sea areas, this paper evaluates the navigational safety of ships on the Korean coast with potential dangerous seakeeping performance using the weather information provided by land. The conclusion is as follows : (1) It is possible that the safety of ships could be secured more accurately by evaluating the seakeeping performance of ships. (2) When the weather is bad, the departure of ships could be controlled by evaluating the navigational safety of ships. (3) When a ship is placed in commission in any area, this evaluation could be used to decide the type and size of ship in use.

• Journal of Korean Biological Nursing Science
• /
• 제26권2호
• /
• pp.154-162
• /
• 2024

Purpose: This study investigated the performance of patient safety activities among hospital nurses and aimed to identify the factors influencing their performance of these activities. Methods: It employed a descriptive survey design, targeting 131 nurses currently working in hospitals. The data collection involved posting a guide to the study on an online social network for nurses (NURSECAPE) and recruiting nurses who understood the content and agreed to participate in the survey. The survey was conducted through a self-reporting method via a URL provided to research participants, and the data collection period was from August 11 to September 11, 2019. Results: The results revealed that 46.6% of the participants had experienced patient safety incidents, with falls being the most common. The factors influencing the performance of patient safety nursing activities among the participants were found to be the type of medical institution, community orientation, and environmental suitability in organizational health. These factors explained 38.5% of the variance. Conclusion: Based on these findings, it appears crucial to explore strategies for improving organizational health tailored to the characteristics of each hospital to facilitate better performance of patient safety activities among hospital nurses. Furthermore, subsequent studies are needed to objectively evaluate the adequacy of patient safety activity performance according to the size of the hospital.

• 한국정밀공학회지
• /
• 제32권7호
• /
• pp.591-595
• /
• 2015

The roller rig tester for safety performance evaluation of wheel derailment is a test facility which can give the test load condition to the test wheel, similar to the actual dynamic condition in actual running condition. This study describes the evaluation result on the durability of the resilient wheel equipped with the ring damper and the damping material, and installed in the half part of a full scaled bogie in combination with the primary spring when it rotates under the dynamic condition. The evaluation result on durability of resilient wheel after load test of 2 million cycles shows that the safety of wheel is not affected by the applied load in visual inspection and nondestructive test, however, in the bolt used for fastening the ring damper to the wheel the loosening was found. Accordingly the use of self-locking nut and washer is recommended.

• 대한전기학회:학술대회논문집
• /
• 대한전기학회 2004년도 춘계학술대회 논문집 전기기기 및 에너지변환시스템부문
• /
• pp.272-274
• /
• 2004

Test evaluation field of railroad system that safety and reliability are important is to verify basic performances of unit products and system that were producted according to the specifications. Also, it is important works that verify finally in respect to commercialize verifying reliability and safety. As one part of system technology, this field is to construct database based on know-how of accumulated technology till now than high technical idea and, is to construct test evaluation system of railroad system that can utilize the constructed database. According to the necessity, our researchers investigated good measuring system of foreign country and performed research on performance test and evaluation technology of high-speed tilting vehicle that suits to domestic state.

• 한국도로학회논문집
• /
• 제14권5호
• /
• pp.145-155
• /
• 2012

PURPOSES: This study proposes a novel method based on microscopic simulation models to evaluate bicycle passing ways in mixed traffic flow conditions at signalized intersections. METHODS: Both operational efficiency and safety are taken into consideration in the evaluation. A widely used performance measure, delay, is used for evaluating the operational efficiency. Regarding the safety evaluation, surrogate safety measures (SSM) to represent traffic conflicts and the level of crash severity, DeltaS and Max.DeltaV, are applied in the proposed method. RESULTS: Extensive simulations and statistical tests show that an integrated bike-box way is identified as the best in terms of operational efficiency and safety. CONCLUSIONS: The proposed method and outcomes of this study will be valuable for bicycle traffic operations and facility design.