• Title/Summary/Keyword: safety and performance evaluation

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Determination of 11 Illicit Compounds in Dietary Supplements Using High-Performance Liquid Chromatography and Liquid Chromatography-Tandem Mass Spectrometry

  • Shin, Dasom;Kang, Hui-Seung;Kim, Hyung-soo;Moon, Guiim
    • Journal of Food Hygiene and Safety
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    • v.35 no.4
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    • pp.326-333
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    • 2020
  • In this work, we developed an analytical method for determining 11 illicit compounds in dietary supplements using high-performance liquid chromatography and liquid chromatography-tandem mass spectrometry. Eleven target compounds, including those meant for weight loss (7-keto-dihydroepiandrosterone, buformin, metformin, phenformin, salbutamol, and tolbutamide), sexual enhancement (dihydroepiandrosterone), and relaxation (asarone, kavain, magnoflorine, and picamilon) were screened and confirmed in dietary supplements. Method validation was performed by evaluating the selectivity, linearity, limit of quantification (LOQ), accuracy, and precision according to the Association of Official Analytical Chemists guidelines. The linearity was > 0.993 for all analytes. The LOQs were ranged in 2.1-9.9 ㎍/mL (HPLC-DAD) and 0.002-0.008 ㎍/mL (LC-MS/MS). The accuracies (expressed as recovery) were 90.0-106% (HPLC-DAD) and 83.0-114% (LC-MS/MS). The precision (expressed as the relative standard deviation) was below 10% using HPLC and LC-MS/MS. The proposed method can be used for the surveillance of illicit compounds in dietary supplements.

A Study on Anti-Islanding Evaluation of Grid-Connected Power Conditioning System for Fuel Cell System in Parallel Operation (병렬 연결된 계통연계형 연료전지 전력변환장치의 단독운전방지 평가 연구)

  • Choi, Young-Joo;Oh, Gun-Woo;Kim, Min-Woo;Lee, Seung-Kuk;Park, Ga-Woo
    • Journal of the Korean Institute of Gas
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    • v.22 no.5
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    • pp.124-132
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    • 2018
  • The supply of renewable energy has become more vigorous due to Paris Agreement. In Korea, supply policies of renewable energy is being promoted with priority given to public buildings, so, the supply of fuel cell system that are relatively easy to install in buildings is expected to expand, so it is important that study on anti-islanding evaluation of grid-connected power conditioning system(PCS) for fuel cell. In this study, we consider that KGS AB934 PC53 in domestic certification standard of PCS for fuel cell correspond with abroad standard and analyze anti-islanding evaluation that important safety performance when connected grid. Additionally, we constructed a prototype for anti-islanding evaluation of PCS for fuel cell connected in parallel and carried out the demonstration evaluation, so, we have conducted ways that ensure safety performance in accordance with the circumstances where several fuel cell systems are installed.

A Study on the Development of Evaluation System on the Construction Project Manager's Safety Capability (건설사업관리자의 안전역량 평가체계 개발에 대한 연구)

  • Shin, Dong Hyuk;Seong, Joo Hyun;Yook, In Soo;Lee, Myeong-Gu;Oh, Tae Keun
    • Journal of the Korean Society of Safety
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    • v.32 no.4
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    • pp.40-45
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    • 2017
  • Among various methods to build the construction safety, the consecutive improvement by the measuring and evaluating safety management capabilities for the construction participants such as an owner, a contractor, and a supervisor (construction project manager) can be the effective one. Thus, an effective evaluation and grading criteria to provide performance index for the implementation of safety management activities should be necessary. In this regards, the purpose of this study is to verify the adequacy by offering a competency evaluation system for the supervisor's safety capability and by applying the system to some construction sites. The proposed evaluation system was developed on the basis of the principles of safety management & accident prevention, basic elements of safety and health management system, and safety evaluation cases at home and abroad. The trial evaluation showed that the safety management of the construction site is mainly carried out by the contractor and the supervisor's awareness for the safety management is low on the whole. Especially, it is urgent to improve the support system from the supervisor headquarter and to place the dedicated safety management person in the field.

Evaluation of Quality Management of Domestic Asbestos Survey and Monitoring Service Providers (국내 석면조사기관의 품질관리 수준에 대한 평가)

  • Kwon, Jiwoon
    • Journal of Korean Society of Occupational and Environmental Hygiene
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    • v.29 no.2
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    • pp.217-225
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    • 2019
  • Objectives: The aim of this study is to evaluate the quality management systems of domestic asbestos survey and monitoring service providers and the relationships with the number of licenses or designations and sales performances. Methods: Data on quality management systems were collected by assessors who were assigned by the Korea Occupational Safety and Health Agency(KOSHA) during a pilot evaluation program for designated asbestos survey and monitoring service providers in 2016 using evaluation criteria developed by KOSHA. Basic characteristics, evaluated scores, and sales performance were gathered and statistically analyzed. Results: The median and arithmetic mean of the total scores were 0.64 and 0.66. Evaluation fields that scored highly with the highest percentages were sales performance, installation and availability of equipment, compliance with the mandatory minimum number of airborne samples, laboratory independence, and results of proficiency analytical testing, in that order. Evaluation fields that received low marks with the highest percentages were the training of personnel, blank field samples, calibration of flow rates, preliminary check and visual inspection of the work area prior to the clearance test, and review and approval of final reports, in that order. Comparison of normalized scores between service providers registered for asbestos and other tasks and those designated for only asbestos showed significant differences in their evaluated scores. Sales performance did not show a positive correlation with evaluated scores. Conclusions: The quality management systems of domestic asbestos survey and monitoring service providers were poor. High scores were recorded mostly in evaluation fields related to regulatory requirements. Low scores were recorded mostly in evaluation fields related to documentation and recordkeeping. Considering the low influence of quality on sales performance, the government needs to evaluate the quality management of asbestos survey and monitoring service providers and provide the results to public in order to address their low levels of quality management.

Development of Design Technology for Safety Enhancement of Damaged Ship (손상 선박의 안전성 향상 설계 기술 개발)

  • Lee, Soon-Sup;Lee, Dong-Kon;Kim, Ki-Sup
    • Journal of the Society of Naval Architects of Korea
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    • v.46 no.1
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    • pp.69-77
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    • 2009
  • Loss of human lives and properties including environmental damage due to large scale accidents requires change of our perception to marine safety. IMO is trying to re-establish overall marine safety system through long term plan such as GBS. Along this line, current regulation based safety evaluation is in process of changing into performance based methods, and for this transition, simulation based safety evaluation during design stage considering damage is highly necessary. In this paper, first, damage scenario is developed from IMO regulations and accident case studies. Then an integrated and simulation based safety evaluation prototype system considering both damage stability and structural safety is developed for the use during ship design process.

Numerical Study on Earthquake Performance of Gravity Dam Considering Earthquake Frequencies (지진진동수에 따른 콘크리트 중력댐의 내진성능에 대한 해석적 사례연구)

  • Chai, Young-Suk;Min, In-Ki
    • Journal of the Korean Society of Safety
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    • v.31 no.4
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    • pp.64-74
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    • 2016
  • Recently, the seismic stability evaluation of concrete gravity dams is raised due to the failure of dams occurred by the Izmit, Turkey and JiJi, Taiwan earthquake in 1999. Dams failure may incur loss of life and properties around the dam as well as damage to dam structure itself. Recently, there has been growing much concerns about "earthquake - resistance" or "seismic safety" of existing concrete gravity dams designed before current seismic design provisions were implemented. This research develops three evaluation levels for seismic stability of concrete gravity dams on the basis of the evaluation method of seismic stability of concrete gravity dams in U.S.A., Japan, Canada, and etc. Level 1 is a preliminary evaluation which is for purpose of screening. Level 2 is a pseudo-static evaluation on the basis of the seismic intensity method. And level 3 is a detail evaluation by the dynamic analysis. Evaluation results on existing concrete gravity dams on operation showed good seismic performance under designed artificial earthquake(KHC earthquake).

Some Thoughts on the Seismic Performance Evaluation Procedure of Urban Railway Infrastructures (도시철도 시설물의 내진성능평가체계에 대한 소고)

  • Hur, Jin-Ho;Kim, Jin-Ho
    • Proceedings of the KSR Conference
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    • 2011.05a
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    • pp.1539-1543
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    • 2011
  • Due to recent large earthquakes around the world, there are increasing social needs for seismic safety of urban railway infrastructures. Urban railway infrastructures are applied different seismic performance evaluation procedure each of overground structures, underground structures and bridge structures, and the characteristics of urban railway infrastructures are not properly considered in the procedure. This study presents problems in the existing seismic performance evaluation procedure of urban railway infrastructures and proposes necessities of unified evaluation procedure.

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A study on the improvement plan for precision safety diagnosis and seismic repair and reinforcement measures according to seismic performance evaluation (내진성능평가에 따른 정밀안전진단 및 내진 보수보강 조치의 개선방안 연구)

  • Kim, Jang-Ook
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2022.04a
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    • pp.87-88
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    • 2022
  • For an earthquake-safe urban environment, the Republic of Korea conducts seismic performance evaluation in accordance with laws and guidelines to assign safety ratings and implement necessary management measures such as repairs and reinforcements. In the seismic performance evaluation result, structures lacking in preparation for earthquakes are prioritized and classified into measures such as repair, reinforcement, or careful observation to respond to physical risks such as earthquakes. Such repair and reinforcement work is not a one-time thing, but it is necessary to further enhance the effect through continuous follow-up observation. In this study, the location of the vertical and horizontal displacement measuring part of the construction part is displayed so that the post-construction status of the reinforcement construction part can be visually checked by identifying the problems in the process of post-monitoring in 2022 for the maintenance and reinforcement work of local governments' public facilities carried out in 2021. We propose a plan to institutionalize the installation of, inspection tools, and crack gauges at certain locations in the construction department, and to have facility managers periodically inspect and manage them with a smartphone program or the 'Facility Autonomous Safety Inspection' app.

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The Corelation Analysis between Condition Evaluation Factors and Defect Index on the Concrete Retaining Wall (콘크리트 옹벽에 대한 상태평가 항목과 결함지수와의 상관관계 분석)

  • Seong, Joo Hyun;Byun, Yoseph;Lee, Dong Yul;Oh, Tae Keun
    • Journal of the Korean Society of Safety
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    • v.30 no.5
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    • pp.52-58
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    • 2015
  • Although lots of safety inspection and precision safety diagnosis have been conducted on concrete retaining wall, there is no comprehensive analysis on the basis of the accumulated data associated with the statistic. Especially, the concentrated management is necessary on the evaluation items that cause critical damages for the efficient performance. In this regard, this study conducted a correlation analysis between the 18 condition evaluation items and defect index for the concrete retaining wall as well as how each item affects the final defect index as much as in the manual. As a result, correlation coefficient between sliding and overturning was 0.601, which means that they have a strong correlation, and the most influential item on defect index is the condition of drainage that scored the 0.750 correlation coefficient. In addition, as a result of regression analysis, the condition of drainage with the 0.683 correlation coefficient has a strong correlation with the defect index. If the condition evaluation items are integrated or readjusted based on the results of the statistical analysis in this study, the more efficient and accurate maintenance will be possible.

A Study on the Protective Function Performance Evaluation of Grid-Connected Power Conditioning System for Residential Fuel Cell System (가정용 연료전지시스템 계통연계형 전력변환장치의 보호기능 성능평가에 관한 연구)

  • Lee, Jung-Woon;Seo, Won-Seok;Kim, Young-Gyu
    • 한국신재생에너지학회:학술대회논문집
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    • 2009.06a
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    • pp.341-344
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    • 2009
  • In this paper, protective function evaluation was conducted to determine the performance and safety of a power conditioning system(PCS) for 1kW residential fuel cell system. It is essential to have a power quality, grid-connection and safety of PCS. Even though it is under 500ms by KGS-A410 standard, it is shown a rapid response time of 25ms from input under-voltage test. In terms of output over/under-voltage test, it is shown 29.15 and 79.4ms. Especially using anti-islanding test, it is shown all times under 100ms for combination cases of real and reactive power. We confirmed a rapid response characteristics and safety of PCS. The results of this evaluation are being used to develop a new test protocols of PCS.

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