• 한국재료학회:학술대회논문집
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• 한국재료학회 1992년도 추계학술발표강연 및 논문개요집
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• pp.77-77
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• 1992

• 한국재료학회:학술대회논문집
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• 한국재료학회 1993년도 춘계학술발표회
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• pp.16-16
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• 1993

• 한국결정성장학회지
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• 제31권5호
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• pp.218-227
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• 2021

저온 동시 소성용 후막 NTC 서미스터를 Mn_1.5Ni_0.4Co_0.9Cu_0.4O₄ 조성의 NTC 분말과 lead free frit 및 RuO₂를 이용하여 제조한 페이스트를 96 % 알루미나 기판 위에 인쇄와 소결을 통해 제조한 후, 이 후막 NTC의 전기적 특성에 미치는 프릿트 및 RuO₂의 영향을 연구하였다. 후막 NTC 서미스터의 저항은 동일한 온도에서 소결한 벌크 상에 비해 높게 나타났으나 저항-온도 특성에서 부 저항 온도 특성은 더 명확하게 직선적으로 나타남을 알 수 있었다. 한편, 소결온도 증가에 따라 면적저항은 감소하였고 프릿트 첨가량이 많을수록 면적저항은 높게 나타났다. 후막 NTC 서미스터의 B 정수는 3000 K 이상의 값 나타냈는데 그 중 프릿트를 5 wt% 첨가한 페이스트로 만든 후막 NTC를 900℃에서 소결한 시편의 B 정수가 가장 높게 나타남을 알 수 있었다. 또한, RuO₂ 첨가에 따라 면적저항의 감소가 나타남을 알 수 있었으며 RuO₂를 5 wt% 첨가한 페이스트를 900℃에서 소결한 후막 NTC 서미스터의 면적저항 감소의 변화가 가장 뚜렷이 나타남을 알 수 있었다.

• 한국분말재료학회지
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• 제4권4호
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• pp.243-251
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• 1997

Engine valve-shaped TiAl-Mn intermetallics containing 43.5 to 47.5at%Al (Mn/Al=0.036) are successively fabricated by reactive sintering the elemental powder mixtures near-net shaped by extrusion and die forging. A duplex structure consisted of lamellar grains and equiaxed $\gamma$ grains is developed for all compositions, and the areal fraction of the lamellar grains(or equiaxed $\gamma$ grains) decreases (or increases) with increasing Al content. As Al content increased, the elongation increases with accompanying decrease in yield strength and ultimate tensile strength at both room temperature and 80$0^{\circ}C$. This indicates that the suitable composition is Ti-45at%Al-1.6at%Mn in considering the balance of ambient and elevated tensile properties. The reactive-sintered Ti-45Al-1.6Mn alloy shows superior oxidation resistance not only to the plasma arc melted one but also to the heat resistance steel STR35(representative exhaust valve head material for automotive engine). The reactive-sintered Ti-45Al-1.6Mn alloy coated with an oxidizing scale exhibits a better wear resistance than induction hardened martensitic steel STR11(representative exhaust valve tip material for automotive engine).

• The Journal of Advanced Prosthodontics
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• 제12권3호
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• pp.114-123
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• 2020

PURPOSE. The aim of this study was to evaluate the corrosion resistance of the specimens produced by five different commercial metal laser sintering (MLS) systems with their recommended Co-Cr alloy powders. MATERIALS AND METHODS. The MLS machines and the alloy powders used were, ProX 100-ST2724G (St-Pro), Mysint 100-EOS SP2 (SP2-Mys), EOSINT 270-EOS SP2 (SP2-EOS), SLM 100-Starbond CoS (SB-SLM), and MLab Cusing-Remanium^® Star (RS-MLab), respectively. Eight specimens from each group were prepared. Open circuit potential (E_ocp) and electrochemical impedance spectroscopy (EIS) measurements of polished surfaces of the specimens were conducted in a three-electrode cell using a potentiostat-galvanostat in Fusayama-Meyer artificial saliva (AS). Specimens from each group were immersed in AS and de-ionized water for seven days. E_ocp, charge transfer resistance (R_ct) values, and released ions (㎍/㎠ × 7d) in different solutions were determined. The specimen surfaces were observed with SEM/EDS. Results were analyzed statistically. RESULTS. E_ocp values have shifted to potentials that are more positive over time. Steady-state E_ocp values were from high to low as follows, SB-SLM, SP2-Mys, SP2-EOS, RS-MLab, and ST-Pro, respectively. After 60 mins, RS-MLab specimens had the highest R_ct value, followed by SP2-Mys, SB-SLM, SP2-EOS, and ST-Pro. In all groups, ion release was higher in AS than that in de-ionized water. CONCLUSION. There were small differences among the corrosion resistances of the Co-Cr alloy specimens produced with MLS systems; meanwhile, the corrosion resistances were quite high for all specimens.

• 한국건축시공학회지
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• 제20권5호
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• pp.425-432
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• 2020

전통한식 점토기와는 외관이 미려하고, 내수성 및 내화성, 내구성이 우수하나 높은 소성온도를 요구하여 경제성과 중량문제 등으로 인하여 전통양식의 기와를 사용하기 보다 기존의 공법을 사용하고 있는 것이 현 추세이다. 이에 본 연구에서는 우리나라의 산청에서 생산되는 고령토와 점토의 기와 소재에 나노알루미나실리케이트를 첨가하여 1,000℃ 이하의 저온소성하면서 전통한식 점토기와로서의 요구되는 물성을 만족하는 최적배합과 재료의 공정을 설계하고 이를 통해 나노코팅 전통한식 점토기와 소재개발에 관한 특성은 연구하고자 한다.

• 대한금속재료학회지
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• 제47권8호
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• pp.508-515
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• 2009

Ti-6Al-4V biomaterial is widely used as a bone alternative. However, Ti-6Al-4V ELI alloy suffers from numerous problems such as a high elastic modulus and high toxicity. Therefore, non-toxic biomaterials with low elastic moduli need to be developed. Ti-HA(hydroxyapatite) composites were fabricated in the present work by pulsed current activated sintering (PCAS) at $1000^{\circ}C$ under 60 MPa using mixed Ti and HA powders. The effects of HA content on the physical and mechanical properties of the sintered Ti-HA composites have been investigated. X-ray diffraction(XRD) analysis of the Ti-HA composites, including Ti-40 wt%HA in particular, revealed new phases, $Ti_{2}O$, CaO, $CaTiO_3$, and TixPy, formed by chemical reactions between Ti and HA during sintering. The hardness of the Ti-HA composites decreased with an increase in HA content. The corrosion resistance of these composites was observed to be an excellent candidate as a commercial Ti-6Al-4 V ELI alloy. A Ti-5 wt%HA composite fabricated by PCAS is recommended as a new biomaterial, because it offers good corrosion resistance, compressive strength, wear resistance, and biocompatibility, and a low Young's modulus.

• Nuclear Engineering and Technology
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• 제54권3호
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• pp.975-983
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• 2022

A four-layered W/Cu functionally graded material (FGM) (W90% + Cu10%/W80% + Cu20%/W70% + Cu30%/W60% + Cu40%, wt.% fraction) and a four-layered diamond/W-Cu FGM (W90% + Cu10%/W80% + Cu20%/W70% + Cu30%/W55% + Cu40% + diamond5%, wt.% fraction) were fabricated by microwave sintering. The thermal conductivity and thermal shock resistance of diamond/W-Cu FGM and W-Cu FGM were investigated. The morphologies of the diamond particles and different FGMs were analyzed using AFM, SEM, EDS, and TEM. The results show that a 200 nm rough tungsten coating was formed on the surface of the diamond. The density of the tungsten-coated diamond/W-Cu FGM, obtained by microwave sintering at 1200 ℃ for 30 min, was 94.66%. The thermal conductivity of the fourlayered diamond/W-Cu FGM was 220 W·m^-1·K^-1, which is higher than that of the four-layered W/Cu FGM (209 W m^-1 K^-1). This indicates that adding an appropriate amount of tungsten-coated diamond to the high Cu layer W/Cu FGM improves the thermal conductivity of the composite. The diamond/W-Cu FGM sintered at 1200 ℃ for 10 min exhibited better thermal shock resistance than diamond/W-Cu FGM sintered at 1100 ℃ for 10 min.

• 한국결정성장학회지
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• 제28권1호
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• pp.28-37
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• 2018

저온에서 소성이 가능한 NTC 서미스터의 제조를 위해 $Mn_{1.85}Ni_{0.25}Co_{0.9}O_4$ 기본 조성의 NTC 서미스터의 전기적 특성에 미치는 무연계 프릿트(frit)와 $RuO_2$ 첨가의 영향에 대하여 연구하였다. 기본 NTC 조성에 프릿트를 10 wt% 첨가하여 $1000^{\circ}C$에서 소결한 시편의 소결특성이 프릿트를 첨가하지 않고 $1200^{\circ}C$에서 소결한 시편과 유사하였다. 그러나 프릿트의 첨가량이 증가할수록 전기저항과 B 정수는 높게 나타났다. 저항을 낮추기 위해 프릿트를 10 wt% 첨가한 조성에 $RuO_2$를 0, 2, 5 wt% 첨가하여 $1000{\sim}1200^{\circ}C$에서 소결하여 NTC 서미스터를 제조 한 후 소결 및 전기적 특성을 측정하였다. $RuO_2$ 첨가량이 많을수록 전기저항과 B 정수는 감소하는 경향을 나타내었으나, $RuO_2$를 5 wt% 첨가하여 $1000^{\circ}C$의 소결온도에서 소결한 소결체가 저항이 가장 낮았고 이후 소결온도 증가에 따라 저항은 오히려 증가하는 경향을 나타내었다. 기본 NTC 조성에 10 wt%의 프릿트와 5 wt%의 $RuO_2$를 첨가하여 $1000^{\circ}C$에서 소결한 NTC 서미스터가 프릿트를 첨가하지 않은 기본 조성의 NTC를 $1200^{\circ}C$에서 소결한 경우와 소결특성과 전기적 특성이 유사하였다.

• 대한전기학회:학술대회논문집
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• 대한전기학회 1989년도 추계학술대회 논문집 학회본부
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• pp.119-121
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• 1989

The properties of Pb-doped Bi-Sr-Ca-Cu-O Super-conductors prepared by solidstate reaction have been studied. Zero resistance was attained at l03K for the sample sintered 845[$^{\circ}C$]for 264hours and it was depended upon sintering conditions. From XRD data low Tc phase and high Tc phase were observed and the volume fraction of high Tc phase increased with increase in sintering period. The grain size increased with increase in sintering temperature and time.