• Title/Summary/Keyword: resin acid

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An experimental study on durability evaluation of the concrete applied nano level inorganic polymer based coatings (나노합성 무기질 폴리머계 표면처리제를 적용한 콘크리트의 내구성능 평가에 관한 실험적 연구)

  • Baek Jong-Myeong;Kim Eun-Kyeum
    • Proceedings of the KSR Conference
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    • 2004.10a
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    • pp.1014-1020
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    • 2004
  • In this study, durability of the nano-level inorganic polymer based coatings which can provide a barrier against the ingress of moisture or aggressive ions to concrete is discussed. For the durability evaluation of the coatings, chloride penetration test, accelerating carbonation test, freezing and thawing test, and sulfate ponding test are conducted. As the result of this study, concrete applied nano-level inorganic polymer based coatings has a much higher resistance to the ingress of chloride ion, carbon dioxide, moisture and aggressive acid than plain concrete and epoxy resin based paint by means of crosslinking three-dimensional structure with concrete structure.

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Advanced Nanoimprinting Material for Liquid Crystal Alignment

  • Gwag, Jin-Seog;Oh-e, Masahito;Yoneya, Makoto;Yokoyama, Hiroshi;Satou, H.;Itami, S.
    • 한국정보디스플레이학회:학술대회논문집
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    • 2007.08a
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    • pp.534-537
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    • 2007
  • To promote liquid crystal application of nanoimprint lithography, a polymer with new concept is proposed. The material consists of a polyamic acid for good LC alignment and an epoxy resin for good imprinting. The result of sum-frequency generation (SFG) vibrational spectroscopy proves that this material is a functionally gradient material. This material shows excellent capability as a nanoimprinting material as well as an LC alignment layer.

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Studies on the Chemical composition of Zostera marina ("거머리 말"의 화학성분에 관한 연구)

  • 박명삼
    • Journal of Plant Biology
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    • v.12 no.1
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    • pp.1-6
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    • 1969
  • General components, free sugars, and free amino acids about Zostera marina which is much distributing and producing along the coastlines of Korea have been separated and identified through Ion exchange resin and Paper chromatography method. So distrigushed are sugars contained that this was quantitated by Bertrand method. 1) The result of the general component analysis of Zostera marina shows that there are much free sugars. 2) According to Bertrand method sugar containment quantitated from terrestrial stem and subterranean stem on Po-hang and Ko-hung areas is much more in terrestrial stem than subterranean stem. 3) Seven kinds of sugars are used in experiments(Table 2) among there glucose, fructose and sucrose which keep the sweetness are very much contained. 4) Shown in Fig. 3 ten kinds of free amino acids inspected from experimental liquid by Paper chromatography are separated, which are known, and one spot which in unknown is additionally separated, and in which four kinds of essential amino acid to nutrient are contained.

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A Dtudy on the Effect of Polyamines of Korean Red Ginseng on the Growth of Cultured Chichen Embryonic Muscle Cells (홍삼 Polyamine 계 성분이 배양한 계배의 근육세포 성장에 미치는 영향)

  • 구향자;김영중
    • YAKHAK HOEJI
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    • v.31 no.5
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    • pp.296-301
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    • 1987
  • Polyamines of Korean red ginseng were extracted with 5% trichloroacetic acid and purified by ion exchange chromatography using Dowex-50Wx8 resin. Four spots having R$_f$ values of 0.19, 0.28, 0.35, and 0.45 were detected. It was observed under microscopy that those polyamines stimulated the growth and differentiation of chicken embryonic muscle cell. The development of muscle cells from the stage of myoblast to that of myotube was found to be enhanced by those polyamines. It was also observed that those polyamines most likely lengthened, the life-span of the cultured chicken embryonic skeletal muscle cells.

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Development of a Measurement Method for Three Dimensional Treeing Degradation using a Computerized Tomography Method

  • Masateru-Yanagiwara;Noboru-Yoshimura
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1990.10a
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    • pp.23-25
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    • 1990
  • In this paper, a system to measure tree degradation of three dimensional phenomena in organic insulating materials using image processing system is discussed. Using a computerized tomography method, volume of tree immediately after tree initiation, as well as changes in the configuration of the tree were measured, which up to now have been difficult to measure. The specimens used an acrylic acid resin. As a result, it was possible to record the cross sections of the tree, and to describe the volume of the tree by the three dimensional measurement.

A Study on the Shrink Resist Finish of Wool Fabric(I) - Effect of Treating Condition on Mechanical Properties of Wool Fabric with Chlorination and MONAMIN BTN Resin - (양모직물의 방축가공에 관한 연구(I) - 염소화/MONAMIN BTN 방축가공 양모직물의 역학특성에 미치는 처리조건의 영향 -)

  • 황백순;이재호;김덕리
    • Textile Coloration and Finishing
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    • v.13 no.4
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    • pp.272-281
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    • 2001
  • Shrink resist finishing of wool fabric was carried out with MONAMIN BTN shrink resist agent after chlorination with D.C.C.A.(dichloro isocyanuric acid). The purpose of this study is to investigate the effect of treating conditions, such as concentrations of D.C.C.A and MONAMIN BTN, pH of treating bath, dying times, curing times and temperatures, on shrink resist finishing. Mechanical properties of the treated fabric were measured by KES-FB system. The optimum chlorination of wool corresponds to 2∼3%(o.w.f.) of D.C.C.A. without rendering the damage on surface of wool fiber. Also it seems likely that the shirink resist finishing carried out at 2 ∼3%(o.w.f.) of MONAMIN BTN and pH 7∼8 of treating bath is effective in increasing a softness of hand.

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The effect of adhesive property on microtensile bond strength of human dentin

  • Kim, Hyoun-Jin;Hur, Bock
    • Proceedings of the KACD Conference
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    • 2003.11a
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    • pp.609-609
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    • 2003
  • I. Objectives The purpose of this study was to evaluate the effect of adhesive property on microtensile bond strength and to determine the failure mode. II. Materials and Methods Flat occlusal dentin surfaces were prepared using low-speed diamond saw. The dentin was etched with 37% phosphoric acid. The following adhesives were applied to the etched dentin according to manufacturer's directions;Scotchbond Multi-Purpose in group 1, Primer&Bond NT in group 2, Scotchbond Multi-Purpose followed by Tetric-flow in group 3. After adhesive application, a cylinder of resin-based composite was built up the occlusal surface.(omitted)

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MORPHOLOGIC CHANGE OF DENTIN SURFACE ACCORDING TO THE DIFFERENCE IN CONCENTRATION AND APPLICATION TIME OF PHOSPHORIC ACID (인산용액의 농도 및 적용시간 차이에 따른 상아질 표면의 형태적 변화)

  • Kim, Myeong-Su;Ohn, Young-Seok;Lee, Kwang-Won;Son, Ho-Hyun
    • Restorative Dentistry and Endodontics
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    • v.23 no.1
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    • pp.141-161
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    • 1998
  • The depth and patterns of demineralization according to the difference in concentration and application time of phosphoric acid were observed through the transmission electron microscope, and shear bond strengths to the acid -conditioned dentin were then measured and compared with the TEM results. To investigate the influence of polymer addition into the phosphoric acid and the effect of difference in concentration and application time of the acid, the specimens were randomly divided into 9 groups. Among the specimens, the exposed dentin surfaces were acid-conditioned with 10% polymer-thickened phosphoric acid(All Bond 2, Bisco, U.S.A.) and aqueous 10%, 20%, 30%, 40% phosphoric acid for 20 seconds, The rest of the specimens were acid-conditioned with 10% phosphoric acid for 15s, 30s, 60s, 120s respectively. The specimens were immersed in 4% glutaraldehyde in 0.1M sodium cacodylate buffer and postfixed with 1 % osmium tetroxide without decalcification and then observed under a JEOL Transmission Electron Microscope(JEM 1200 EX II, Japan). After the specimens were acid-conditioned as the above, primer and adhesive resin were applied to blot-dried dentin and shear bond strengths were then measured and analysed. The results were as follows : 1. The intertubular demineralization depth of 4.0-$5.0{\mu}m$ in 10% polymer-thickened phosphoric acid gels was similar or slightly deeper than that of 4.0-$4.5{\mu}m$ in aqueous 10% phosphoric acid solution. 2. The intertubular demineralization depth of aqueous 20%, 30% and 40% phosphoric acid solution was 6.5-$7.0{\mu}m$, 6.5-$7.5{\mu}m$ and 9.0-$15.0{\mu}m$ respectively. It showed that the depth of dentin demineralization is partly related to the concentration of phosphoric acid solution. 3. The intertubular demineralization depth of aqueous 10% phosphoric acid solution in application time for 15s, 30s, 60s and 120s was 2.5-$3.0{\mu}m$, 4.0-$6.0{\mu}m$, 6.5-$7.0{\mu}m$ and 8.5-$14.0{\mu}m$ respectively. It showed that the depth of dentin demineralization is directly related to the application time of phosphoric acid solution. 4. The partially demineralized dentin layer between demineralized collagen layer and unaffected dentin was showed to a width of 0.5-$1.0{\mu}m$ in lower concentration groups treated with aqueous 10% phosphoric acid for 20s, 60s, 120s and 20% phosphoric acid for 20s. 5. The demineralization effect at the border of intertubular-peritubular junction was less evident than that in the peritubular and intertubular dentin. The collagen fibers in the intertubular dentin had a random orientation, whereas those that lined the tubules were circumferentially aligned. The cross-linkage of dentinal collagen in demineralized collagen layer was clearly seen. 6. A statistically significant difference of bond strengths according to the difference in phosphoric acid concentration did not exist among the groups treated with 10%, 20%, 30% and 40% acid solution (P>0.05). However, bond strengths to the treated dentin with 10% phosphoric acid solution for 30s were significantly higher than that for 120s (P<0.05).

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Effect of Particle Pre-Treatment on Properties of Jatropha Fruit Hulls Particleboard

  • Iswanto, Apri Heri;Febrianto, Fauzi;Hadi, Yusuf Sudo;Ruhendi, Surdiding;Hermawan, Dede;Fatriasari, Widya
    • Journal of the Korean Wood Science and Technology
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    • v.46 no.2
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    • pp.155-165
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    • 2018
  • The objective of the research was to evaluate the effect of particle pre-treatment on physical, mechanical, and durability of jatropha fruit hulls (JFH) particleboard. The pre-treatments included were immersing in cold water, hot water, and acetic acid solution. After each treatment, the particles were dried up to 3% moisture content. Urea-formaldehyde (UF) resin was used to fabricate particleboards with board size, thickness and density target of 25 cm by 25 cm, 0.80 cm, and $0.70g/cm^3$, respectively. Board pressed at $130^{\circ}C$ for 10 minutes, and $25kg/cm^2$ pressure. The evaluation of particleboard followed the JIS A 5908-2003. Whilist their resistance to subterranean termite test (mass loss, mortality, antifeedant value and feeding rate) refers to the Indonesian standard (SNI 01.7207-2006). The physical and mechanical properties of particleboards showed that all pre-treatments decreased the pH of particles. Overall, all particle immersing treatments resulted of better physical and mechanical properties of particleboard than those of untreated ones. The acetic acid treatment resulted the best physical and mechanical properties of particleboard. Based on the mass loss of JFH particleboard, hot water and acetic acid treated particleboards were classified into weak resistance to subterranean attack. The other two treatments were classified into very weak resistance. Hot water treated particleboard provided the highest mortality and antifeedant as much as 87.40% and 34.20%, respectively. Based on antifeedant classification, hot water treated particleboards were classified into moderately strong resistance, while other treatments were categorized into weak resistance. The lowest feeding rate value ($45.30{\mu}g/termite/day$) was attained by hot water treatment.

Enrichment of Lithium Isotopes by Cation Exchange Chromatography (양이온 교환 크로마토그래피에 의한 리튬 동위원소의 농축)

  • Kim, Dong Won;Kim, Chang Suck;Choi, Ki Young;Jeon, Young Shin;Jeong, Young Kyu;Park, Sung Up
    • Analytical Science and Technology
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    • v.7 no.2
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    • pp.201-204
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    • 1994
  • Cation exchange column chromatography of lithium was carried out to investigate the lithium isotope separation in aqueous ion exchange system. A Pyrex glass column of $50cm{\times}6mm$ inner radius with a water jacket was used as the separation column in experiment. Upon column chromatography using hydrochloric and succinic acid mixtures as an elunent, single separation factor, ${\alpha}$, 1.0068 was obtained. From the experiment, it was found that $^6Li$ was enriched in the resin phase and $^7Li$ in the solution phase.

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