• KSBB Journal
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• v.16 no.3
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• pp.233-236
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• 2001

Because of casehardenign effect of amorphous paclitaxel, residual solvents, methylene chloride and emthanol could not be reduced to the maximum value allowed, 600 ppm and 3,000 ppm, in accord with the guidelines issued by the International Conference on Harmonization (ICH, 1997), using rotary evaporation and successive drying in a vacuum oven. However, methylene chloride and methanol were reduced to 486 ppm and 403 ppm, respectively using supercritical $CO_2$ on purified paclitaxel. The optimum pressure and operating time were 80 bar and 30 min at fixed operating temperature ($40^{circ}C$). This approach serves as a novel application of supercritical fluid extraction to remove residual solvents from active pharmaceutical ingredients.

• Journal of Welding and Joining
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• v.28 no.4
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• pp.33-40
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• 2010

The purpose of this study is to establish a predictive equation of transverse residual stress at the thick FCA butt weldment of large container vessel. The variables used were restraint degree, yield strength of base material, thickness of weldment and welding heat input. Restraint degree at the thick weldment of container ship having the various welding sequence was calculated using FEA. From the result, the H-type specimen was designed to reproduce the level of restraint degree at the actual weldment of containership. Based on the results, the predictive equations of the mean value and the distribution of transverse residual stress at each location of the weldment were established using dimensional analysis and multiple-regression method. The predictive equations were verified by comparing with those measured by XRD in the actual weldment of the ship.

• Journal of information and communication convergence engineering
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• v.9 no.1
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• pp.32-37
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• 2011

In dispersion management (DM) and optical phase conjugation applied into optical transmission links with multi fiber spans for minimizing the impact of nonlinearity and group velocity (GVD), implementation possibility of DM using only one fiber span for pre- or postcompensation was assessed as a function of duty cycle of RZ pulse and residual dispersion per span (RDPS). It is confirmed that DM with optimal net residual dispersion (NRD) controlled by only one fiber span could be sufficiently applied into optical transmission links, though optimal NRD is more increased than that in transmission links with the general DM scheme of pre- and postcompensation. Thus, it is expected that optical transmission system is simply designed and implemented by applying the proposed DM scheme into real optical transmission links. Also, it is confirmed that the advantageous duty cycle of RZ is 0.5 and RDPS is setting to be small value for the effective transmitting wide signal wavelength range in optical links with optimal NRD controlled by only one fiber span.

• The Journal of Korean Institute of Communications and Information Sciences
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• v.31 no.6A
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• pp.586-592
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• 2006

In this paper, a novel detection method called the joint multiple frequency cell (JMFC) detection is addressed for spread spectrum code acquisition in the presence of residual Doppler frequency offset (RDFO). When the RDFO exists, the correlation peak used for detection during the acquisition process is split into several lower neighboring peaks, resulting in severe degradation in the detection performance, and consequently, in the overall acquisition performance. In the JMFC detection, a decision variable for detection is formed by combining several consecutive correlator outputs, so that the reduction in the correlation value due to the RDFO can be alleviated. Numerical results show that the proposed scheme can offer better detection performance over the conventional scheme based on the cell-by-cell detection.

• KSTLE International Journal
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• v.6 no.2
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• pp.45-50
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• 2005

Plasma ceramic spray that is applied on a machine part under severe work conditions has been investigated for tribological behavior. The application of ceramic coatings by plasma spray has become essential in tribosystems to produce wear resistance and long life in severe conditions. The purpose of this study was to investigate the wear characteristics of $8\%Y_{2}O_3-ZrO_2$ coating, in view of the effect of post-spay heat treatment. The plasma-sprayed $8\%Y_{2}O_3-ZrO_2$ coating was studied to know the relationship between phase transformations and wear behavior related to post-spray heat treatment. Wear test was carried out with ball on disk type on normal loads of 50N,70N and 90N under room temperature. The phase transformation of phase and the value of residual stress were measured by X-ray diffraction method(XRD). Tribological characteristics and wear mechanisms of coatings were observed by SEM. The tribological wear performance was discussed in the focusing of residual stress. Consequently, post-spray heat treatment plays an important role in decreasing residual stress. Residual stress in the coating system has a significant influence on the wear mechanism of coating.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 2005.10a
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• pp.790-793
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• 2005

In these days, the piezoresistive material has been applied to various sensors in order to measure the change of physical quantities. But the relationship between the sensitivity of a sensor and the position and size of piezoresistor has rarely been studied. Therefore, this paper was focused on the effect of residual stress induced in piezoresistor on the distribution of resistance change ratio and supposed the feasible position of piezoresistor. The resulting are following; The tensile residual stress in the vicinity of piezoresistor decreased the value of resistance change ratio and could not effect on all the area of diaphragm but local area around the piezoresistor. Also, the piezoresistor in the diaphragm type pressure sensor with boss should fabricate in the edge of boss in order to increase the sensitivity of pressure sensor.

• The Transactions of The Korean Institute of Electrical Engineers
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• v.68 no.1
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• pp.102-107
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• 2019

This paper proposes a method to improve the mass spectral detection performance of the residual gas analyzer. By improving the mode estimation method for setting the threshold value and improving the additive noise elimination method, it is possible to detect mass spectrums having low peak values of the threshold level difficult to distinguish from noise. Ion signal blocks for each mass index with noise removed by the improved method are effective for eliminating invalid ion signals based on the linear and quadratic fittings. The mass spectrum can be obtained from the quadratic fitted curves for the reconstructed ion signal block using only the valid ion signals. In addition, the resolution of the mass spectrum can be improved by correcting the error caused by the shift of the spectral peak position. To verify the performance of the proposed method, computer simulations were performed using real ion signals obtained from the residual gas analysis system under development. The simulation results show that the proposed method is valid.

• Journal of the Korean Society for Heat Treatment
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• v.37 no.3
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• pp.128-137
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• 2024

In this study, the carburizing heat treatment process used in aircraft gear manufacturing was compared with the general carburizing heat treatment process using AISI 9310 steel. The process of carburizing followed by slow cooling, and then quenching after austenitizing(Process A) showed less compressive residual stress and less retained austenite in the surface layer compared to the process of quenching directly after carburizing(Process B). In prpcess B, there was a large amount of retained austenite when quenched immediately after carburization, and when treated with subzero, martensite rapidly increased and the compressive residual stress increased significantly, but at the same time, there is a risk of cracking due to severe expansion in volume. Therefore, in the case of aviation parts, it is believed that a step-by-step heat treatment cycle was adopted to ensure stability against heat treatment cracks. As a result of the final tempering after sub-zero treatment, the A process specimen showed a deeper effective case depth and HV700 depth and a higher hardness value above HV700 than the B process specimen.

• Journal of the Institute of Convergence Signal Processing
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• v.14 no.2
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• pp.136-146
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• 2013

In this paper, the residual delay compensation algorithm is proposed for FX-type KJJVC. In case of initial version as that design algorithm of KJJVC, the integer calculation and the cos/sin table for the phase compensation coefficient were introduced in order to speed up of calculation. The mismatch between data timing and residual delay phase and also between bit-jump and residual delay phase were found and fixed. In final design of KJJVC residual delay compensation algorithm, the initialization problem on the rotation memory of residual delay compensation was found when the residual delay compensated value was applied to FFT-segment, and this problem is also fixed by modifying the FPGA code. Using the proposed residual delay compensation algorithm, the band shape of cross power spectrum becomes flat, which means there is no significant loss over the whole bandwidth. To verify the effectiveness of proposed residual delay compensation algorithm, we conducted the correlation experiments for real observation data using the simulator and KJJVC. We confirmed that the designed residual delay compensation algorithm is well applied in KJJVC, and the signal to noise ratio increases by about 8%.

• Proceedings of the KWS Conference
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• 2010.05a
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• pp.57-57
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• 2010

For thin panel welded structure, the various welding distortions were found due to the low resistance against welding deformation. Especially, buckling distortion induced in the thin panel welded structure produce severe problems related to cost in production stage and safety in service life. So, many researches including mechanical and thermal tensioning method for preventing the occurrence of buckling distortion in the production stage have been performed. The purpose of this study is to identify the behavior of longitudinal residual stress at the SA butt weldment with thin plate of 6mm thickness under tension load by 3 dimensional FEA. For it, mesh design for 3D FEA was constructed with 20 nodes brick element for butt weldment and 8 nodes shell element for base metal. According to FEA results, the longitudinal compressive strain inducing tensile residual stress at the butt weldment decreased. It was because the compressive thermal strain in way of weldment was reduced by tension load. The control effect of residual stress increased with an increase in tension load. So, if the amount of tension load applied to the weldment exceeds 1.5 times of longitudinal shrinkage force, the amount of longitudinal residual stress decreased below the critical value inducing the buckling distortion at the SA butt weldment. Its validity was verified by experiment.