• Title/Summary/Keyword: residual time

Search Result 2,098, Processing Time 0.03 seconds

Sensing of the Insecticide Carbofuran Residues by Surface Plasmon Resonance and Immunoassay (표면플라즈몬공명과 효소면역분석법을 이용한 살충제 카보후란 잔류물 검출)

  • Yang G. M.;Cho N. H.
    • Journal of Biosystems Engineering
    • /
    • v.30 no.6 s.113
    • /
    • pp.333-339
    • /
    • 2005
  • The pesticide is raising public interest in the world, because it causes damage to an environmental pollution and the human health remaining agricultural products and an ecosystem, in spite of the advantages. Particularly, each country restricts the residual pesticide and induces observance about the safety and usage standard so that they can control the amount of pesticide used and defend the safety of agricultural products. The habitual practice for the analysis of the residual pesticide depends on GC (gas chromatography), HPLC (high performance liquid chromatography) and GC/MS (gas chromatography/mass spectroscopy), which triturate the fixed quantity of samples, abstract and purify as a suitable organic solvent. These methods have the highly efficient in aspects of sensitivity and accuracy. On the other hand, they need the high cost, time consuming, much effort, expensive equipment and the skillful management. Carbofuran is highly toxic by inhalation and ingestion and moderately toxic by dermal absorption. As with other carbamate compounds, it is metabolized in the liver and eventually excreted in the urine. The half-life of carbofuran on crops is about 4 days when applied to roots, and longer than 4 days if applied to the leaves. This research was conducted to develop immunoassay for detecting carbofuran residue quickly on the basis of surface plasmon resonance and to evaluate the measurement sensitivity. Gold chip used was CM5 spreaded dextran on the surface. An applied antibody to Immunoassay was GST (glutathione-s-transferase). The association and the dissociation time were 176 second and 215 second between GST and carbofuran. The total analysis time using surface plasmon resonance was 13 minutes including regeneration time, on the other hand HPLC and GC/MS was 2 hours usually. The minimum detection limit of a permissible amount for carbofuran in the country is 0.1 ppm. The immunoassay method using surface plasmon resonance was 0.002 ppm.

The Difference of Fish Toxicity by Preparation Methods of Test Solution (시험용액의 조제방법에 따른 어독성 차이)

  • Bae, Chul-Han;Kim, Yeon-Sik;Park, Yeon-Ki;Park, Eun-Hee;Park, Hynn-Ju;Shin, Dong-Chan;Lee, Seung-Yeol;Lee, Suk-Hee;Chung, Chang-Kook
    • The Korean Journal of Pesticide Science
    • /
    • v.14 no.3
    • /
    • pp.219-225
    • /
    • 2010
  • The solubility in water of granular pesticides is not equal because the difference of methods of producing a granular pesticide. This study was conducted to investigate fish acute toxicity of butachlor 5% GR, fipronil 0.4% GR by impregnation and carbosulfan 3% GR, diazinon 0.4% GR by coating, using carp (C. carpio), medaka (O. tatipes) and loach (M. anguillicaudatus). The test solution of each pesticide was prepared by direct addition of granular pesticide and add after grinding granular pesticide to powder in test water, We also investigated $LC_{50}$ and residual concentration until 96 hours. Test results were appeared that the treatment of powder was 1.2~4 time higher than granular and toxicity increased clearly according to elapsed time, And the residual amounts by time were detected much at early time in the powder treatment of butachlor GR and diazinon GR. Conclusively, fish acute toxicity and residual concentration in test solution appeared higher in the powder treatment than treat granular form directly in water. Also, 96 hours toxicity values were stable comparatively and the error is less than 48 hours.

Preparation and Characteristics of Kimchi Tablet (김치 타블렛의 제조와 품질특성)

  • 박석란;최유원;윤광섭;김순동
    • Food Science and Preservation
    • /
    • v.8 no.3
    • /
    • pp.302-307
    • /
    • 2001
  • In order to prepare kimchi tablet(K7), the kimchi was fermented with crushed materials and lactic acid bacterial starter. The effect of raying methods (hot air-drying : HAD, freeze drying: FD), moulding pressure (100, 150 and 200 kg/cm2) and moulding time (0, 1, 2, 3 and 4 min) of kimchi tablet on residual solid, characteristics of filtrate, color, textual properties, hygroscopicity and sensory quality were investigated. No great difference showed in residual solid of the tablet prepared with freeze dried kimchi (FD-KT), but the tablet prepared with hot air-dried kimchi (HAD-KT) decreased markedly with an increase in moulding pressure. Residual solid of FD-KT was lower than that of HAD-KT. The pH and redness for HAD-KT and FD-KT were similar. Total sugar. acidity and lightness of FD-KT as compared with HAD-KT were higher, while higher max, yield, strength and hardness were found for HAD-KT. Color, tactile, flavor, chewing taste, acceptability and hygroscopicity of FD-KT were generally higher than those of HAD-KT. Hygroscopicity of HAD-KT decreased with an increase in moulding pressure in md time, but that of FD-KT increased. Overall qualities of FD-KT and HAD-KT showed best in 200 kg/㎠ of moulding pressure, 3min of moulding time.

  • PDF

The Measurement Errors of Elastic Modulus and Hardness due to the Different Indentation Speed (압입속도의 변화에 따른 탄성계수와 경도의 오차 연구)

  • Lee, Kyu-Young;Lee, Chan-Bin;Kim, Soo-In;Lee, Chang-Woo
    • Journal of the Korean Vacuum Society
    • /
    • v.19 no.5
    • /
    • pp.360-364
    • /
    • 2010
  • Most research groups used two analysis methods (spectroscopy and nanotribology) to measure the mechanical properties of nano-materials: NMR (Nuclear Magnetic Resonance), IR (Infrared Spectroscopy), Raman Spectroscopy as the spectroscopy method and AFM (Atomic Force MicroScope), EFM (Electrostatic Force Microscope), KFM (Kelvin Force Microscope), Nanoindenter as the nanotribological one. Among these, the nano-indentation technique particularly has been recognized as a powerful method to measure the elastic modulus and the hardness. However, this technique are prone to considerable measurement errors with pressure conditions during measurement. In this paper, we measured the change of elastic modulus and hardness of an Al single crystal with the change of load, hold, and unload time, respectively. We found that elastic modulus and hardness significantly depend on load, hold, and unload time, etc. As the indent time was shortened, the elastic modulus value decreased while the hardness value increased. In addition, we found that elastic modulus value was more sensitive to indent load, hold, and unload time than the hardness value. We speculate that measurement errors of the elastic modulus and the hardness originate from the residual stress during indenting test. From our results, the elastic modulus was more susceptible to the residual stress than the hardness. Thus, we find that the residual stress should be controlled for the minimum measurement errors during the indenting test.

Gas Chromatographic Analysis on Residual Concentration and Half-life Time of Cyfluthrin in Potato and Soil (감자와 토양 중에서 Cyfluthrin의 잔류농도와 반감기에 대한 기체 크로마토그래피 분석)

  • Han, Seong Soo;Jeong, Seung Il;Chun, Hyun Ja;Hoang, Geun Chang;Kim, Il Kwang
    • Analytical Science and Technology
    • /
    • v.13 no.6
    • /
    • pp.722-730
    • /
    • 2000
  • The residual concentration and half-life time of synthetic pyrethroid insecticide cyfluthrin in potato and soil were investigated by gas chromatography (GC). The pesticide in potato was extracted with n-hexane, filtered and concentrated. The concentrated phase was transferred to the Sep-Pak silica gel column and purified with acetonitrile and acetone for the analysis by gas chromatography equipped with electron capture detector (GC-ECD). From the standard additional experiments with 0.01 and $0.1{\mu}g$, the recoveries were 85-87% and the detection limit was 0.005 ng. The soil sample was extracted with acetone and dichloromethane. The organic phase was concentrated and redissolved with n-hexane and analyzed with GC-ECD after cleaned with Sep-Pak column. From the standard additional experiments with 0.01 and 0.1 ng, the recoveries were 84-88% and the detection limit was 0.005ng. The half-life time of cyfluthrin in the silty clay was 25 days in the room laboratory and 0.6 days in the fieJd test whereas it was 38 days and 0.5 days for each in case of silty loam.

  • PDF

Highly accurate family of time integration method

  • Rezaiee-Pajand, Mohammad;Esfehani, S.A.H.;Karimi-Rad, Mahdi
    • Structural Engineering and Mechanics
    • /
    • v.67 no.6
    • /
    • pp.603-616
    • /
    • 2018
  • In this study, the acceleration vector in each time step is assumed to be a mth order time polynomial. By using the initial conditions, satisfying the equation of motion at both ends of the time step and minimizing the square of the residual vector, the m+3 unknown coefficients are determined. The order of accuracy for this approach is m+1, and it has a very low dispersion error. Moreover, the period error of the new technique is almost zero, and it is considerably smaller than the members of the Newmark method. The proposed scheme has an appropriate domain of stability, which is greater than that of the central difference and linear acceleration techniques. The numerical tests highlight the improved performance of the new algorithm over the fourth-order Runge-Kutta, central difference, linear and average acceleration methods.

Development of the Roundwood Demand Prediction Model

  • Kim, Dong-Jun
    • Journal of Korean Society of Forest Science
    • /
    • v.95 no.2
    • /
    • pp.203-208
    • /
    • 2006
  • This study compared the roundwood demand prediction accuracy of econometric and time-series models using Korean data. The roundwood was divided into softwood and hardwood by species. The econometric model of roundwood demand was specified with four explanatory variables; own price, substitute price, gross domestic product, dummy. The time-series model was specified with lagged endogenous variable. The dummy variable reflected the abrupt decrease in roundwood demand in the late 1990's in the case of softwood roundwood, and the boom of plywood export in the late 1970's in the case of hardwood roundwood. On the other hand, the prediction accuracy was estimated on the basis of Residual Mean Square Errors(RMSE). The results showed that the softwood roundwood demand prediction can be performed more accurately by econometric model than by time-series model. However, the hardwood roundwood demand prediction accuracy was similar in the case of using econometric and time-series model.

The Characteristics of ElectroKinetic Remediation on Unsaturated Soil with Treatment Time (정화기간에 따른 불포화 자연토의 동전기 정화 특성)

  • Kim, Byung-Il;Kim, Jong-Yun;Lee, Jung-Chul;Kim, Soo-Sam
    • Proceedings of the Korean Geotechical Society Conference
    • /
    • 2004.03b
    • /
    • pp.890-896
    • /
    • 2004
  • This study is intended as an investigation of the EK remediation characteristics of natural soil with treatment time under unsaturated conditions. EK tests are performed under the voltage gradient of 1V/cm, the degree of saturation of 82.8%, and the installing of cation exchange membrane. It was found from the results that the acid front is initially transported at 0.75cm/day and then continuously degreased until the transport velocity of the acid front is balanced to the velocity of the base front. The residual lead concentration indicated the maximum value at the treatment time of lOdays, then the increasing of treatment time largely decreases the concentration within the sample though electromigration than electroosmosis.

  • PDF

The effects of short persistent CCFL in Blinking Back Light Unit to reduce blur on TFT-LCD

  • Han, J.M.;Bae, K.W.;Kim, S.Y.;Kim, Y.H.;Lim, Y.J.
    • 한국정보디스플레이학회:학술대회논문집
    • /
    • 2003.07a
    • /
    • pp.694-697
    • /
    • 2003
  • In applying LCD to TV application, one of the most significant factors to be improved is image sticking on the moving picture. LCD is different from CRT in the sense that it's continuous passive device, which holds images in entire frame period, while impulse type device generate image in very short time. To reduce image sticking problem related to hold type display mode, we made an experiment to drive LCD like CRT. We made articulate images by turn on-off backlight, and we realized the ratio of Back Light on-off time by adjusting between on time and off time for video signal input during 1 frame (16.7ms). Conventional CCFL (cold cathode fluorescent lamp) cannot follow fast on-off speed, so we evaluated new fluorescent substances of light source to improve residual light characteristic of CCFL. We realized articulate image generation similar to CRT by blinking drive. As a result, reduced image sticking phenomenon was validated by naked eye and response time measurement.

  • PDF

ALC(Autoclaved Lightweight Concrete) Hardness Prediction Research By Multiple Regression Analysis (다중회귀분석을 이용한 ALC 경도예측에 관한 연구)

  • Kim, Gwang-Su;Baek, Seung-Hun
    • Proceedings of the Safety Management and Science Conference
    • /
    • 2012.04a
    • /
    • pp.117-137
    • /
    • 2012
  • In the ALC(Autoclaved lightweight concrete) manufacturing process, if the pre-cured semi-cake is removed after proper time is passed, it will be hard to retain the moisture and be easily cracked. Therefore, in this research, we took the research by multiple regression analysis to find relationship between variables for the prediction the hardness that is the control standard of the removal time. We study the relationship between Independent variables such as the V/T(Vibration Time), V/T movement, expansion height, curing time, placing temperature, Rising and C/S ratio and the Dependent variables, the hardness by multiple regression analysis. In this study, first, we calculated regression equation by the regression analysis, then we tried phased regression analysis, best subset regression analysis and residual analysis. At last, we could verify curing time, placing temperature, Rising and C/S ratio influence to the hardness by the estimated regression equation.

  • PDF