• Title/Summary/Keyword: residual gas analysis

Search Result 211, Processing Time 0.029 seconds

Method to Reduce the Activity Loss and Pain when Injecting 18F-Florbetaben (18F-Florbetaben 주사 시 Activity 손실과 통증 감소를 위한 방법)

  • Kwon, Hyeong Jin;Choi, Jin Wook;Lee, Hyeong Jin;Woo, Jae Ryong;Kim, Yoo Kyeong
    • The Korean Journal of Nuclear Medicine Technology
    • /
    • v.20 no.2
    • /
    • pp.42-45
    • /
    • 2016
  • Purpose Neuracep is used to other diagnostic evaluations of the brain to estimate beta-amyloid neuritic plaque density in adult patients with cognitive impairment and inspected cognitive impairment. $^{18}F-Florbetaben$ specially has moderate lipophilicity and property of the added ethanol. It is the subject of interest of the patient pain and residual activity after injecting. Our study is effective injection method of the radiopharmaceutical and patient care. So it is for the highest quality image. Materials and Methods Patients were targeted 70 subjects, it was injected mean $259{\pm}74MBq$ to the patients ($^{18}F-FDG$: 20 subjects, $^{18}F-FP-CIT$: 20 subjects, $^{18}F-Florbetaben$: 30 subjects). After injection (reflusing 2 times, reflusing 3 times) using a 3-way set, it measured the residual activity. When injecting $^{18}F-Florbetaben$, we evaluated the effective injection methods(3-way set method and heparin cap method). The average residual activity after the injection was compared using a statistical analysis of SPSS 12.0(ANOVA, t-test analysis). Also, elemental analysis was performed on $^{18}F-Florbetaben$ by GC (Gas Chromatography). Results When reflusing 2 times measured residual activity as follows ($^{18}F-FDG$: 1.48 MBq, $^{18}F-FP-CIT$: 7.4 MBq, $^{18}F-Florbetaben$: 32.6 MBq). And when reflusing 3 times measured residual activity as follows ($^{18}F-FDG$: 1.85 MBq, $^{18}F-FP-CIT$: 3.7 MBq, $^{18}F-Florbetaben$: 36.3 MBq). There was a significant difference when reflusing 2 times(P < 0.05) and reflusing 3 times (P < 0.05). But when reflusing 3 times, there was no significant difference relation FDG and FP-CIT (P > 0.05). $^{18}F-Florbetaben$ Residual activity according to the injection method was a significant difference (P < 0.05). GC analysis results were measured ethanol: 207665 ppm and acceton: 377.4 ppm. Conclusion $^{18}F-Florbetaben$ was high residual activity compared to FDG and FP-CIT. Heparin cap method was effective when $^{18}F-Florbetaben$ was injected. $^{18}F-Florbetaben's$ ethanol component analysis was highly measured. So it is recommended that inject to 6 sec/ml or more in order to reduce the pain.

  • PDF

THE EFFECTS OF HEAT INPUT AND GAS FLOW RATE ON WELD INTEGRITY FOR SLEEVE REPAIR WELDING OF IN-SERVICE GAS PIPELINES

  • Kim, Young-pyo;Kim, Woo-sik;Bani, In-wan;Oh, Kyu-Hwan
    • Proceedings of the KWS Conference
    • /
    • 2002.10a
    • /
    • pp.390-395
    • /
    • 2002
  • The experimental and numerical study has been conducted on the sleeve repair welding of API 5L X65 pipeline. SMA W and GTAW were applied to weld the sleeve. The macrostructure and hardness of repair welds have been examined. The [mite element analysis of the multi-pass sleeve-fillet welding has been conducted to validate the experiment and investigate the effects of in-service welding conditions. The effect of gas flow rate on the hydrogen cracking was investigated. The effect of internal pressure on residual stresses and plastic strain was investigated. The allowable heat input was predicted considering the maximum temperature of inner surface of pipe and cooling rate at CGHAZ.

  • PDF

The Effects of Heat Input and Gas Flow Rate on Weld Integrity for Sleeve Repair Welding of In-Service Gas Pipelines

  • Kim, Y.P.;Kim, W.S.;Bang, I.W.;Oh, K.H.
    • International Journal of Korean Welding Society
    • /
    • v.2 no.2
    • /
    • pp.36-41
    • /
    • 2002
  • The experimental and numerical study has been conducted on the sleeve repair welding of API 5L X65 pipeline. SMAW and GTAW were applied to weld the sleeve. The macrostructure and hardness of repair welds have been examined. The finite element analysis of the multi-pass sleeve-fillet welding has been conducted to validate the experiment and investigate the effects of in-service welding conditions. The effect of gas flow rate on the hydrogen cracking was investigated. The effect of internal pressure on residual stresses and plastic strain was investigated. The allowable heat input was predicted considering the maximum temperature of inner surface of pipe and cooling rate at CGHAZ.

  • PDF

Analysis of Residual Nuarimol in Apples (사과 중 Nuarimol의 잔류성 분석)

  • Kim, Il Kwang;Han, Seong Soo;Kim, Youn Geun;Kim, Hea Jin
    • Analytical Science and Technology
    • /
    • v.6 no.3
    • /
    • pp.283-288
    • /
    • 1993
  • The solvent extraction and clean up processes for the gas chromatographic determination of muarimol pesticide residues in apples were investigated and examined the changes of residual concentration with the passage of time. The extracted pesticide with methanol were partitioned with dichloromethane after adding sodium chloride solution. The separated solutions were concentrated and transfered to the alumina column for clean up, and eluated with 1-chlorobutane : methanol solution. As a results their recovering for 0.200 and 1.00ppm muarimol spiked on apples have shown 79~95%. Residual amounts of nuarimol in apple was 0.0830ppm when the fungicide was treated eight times until 3 days before its harvest. It seems to be safely used when nuarimol is treated six times until 7 days before harvest of apple.

  • PDF

Prediction of Positions of Gas Defects Generated from Core (중자에서 발생한 가스 결함 위치 예측)

  • Matsushita, Makoto;Kosaka, Akira;Kanatani, Shigehiro
    • Journal of Korea Foundry Society
    • /
    • v.42 no.1
    • /
    • pp.61-66
    • /
    • 2022
  • Hydraulic units are important components of agricultural and construction machinery, and thus require high-quality castings. However, gas defects occurring inside the sand cores of the castings due to the resin used is a problem. This study therefore aimed to develop a casting simulation method that can clarify the gas defect positions. Gas defects are thought to be caused by gas generated after the molten metal fills up the mold cavity. The gas constant is the most effective factor for simulating this gas generated from sand cores. It is calculated by gas generating temperature and analysis of composition in the inert gas atmosphere modified according to the mold filling conditions of molten metal. It is assumed that gases generated from the inside of castings remain if the following formula is established. [Time of occurrence of gas generation] + [Time of occurrence of gas floating] > [Time of occurrence of casting surface solidification] The possibility of gas defects is evaluated by the time of occurrence of gas generation and gas floating calculated using the gas constant. The residual position of generated gases is decided by the closed loops indicating the final solidification location in the casting simulation. The above procedure enables us to suggest suitable casting designs with zero gas defects, without the need to repeat casting tests.

A Study on Analysis of Residual Antibiotics and Prop Acid in Honey (벌꿀중의 잔유항생물질 및 Propionic Acid 분석011 관한 조사연구)

  • 전상수
    • Journal of environmental and Sanitary engineering
    • /
    • v.5 no.2
    • /
    • pp.63-80
    • /
    • 1990
  • A sensitive and simple analytical system for the simultaneous determination of residual oxytetracycline, tetracycline, and doxycycline in honey was described, and that the analytical method for determination of residual propionic acid in honey was established. Experimental subjects were purchased four kinds of honey, native kind honey, acaccia honey, mixed floral honey, chestnut honey in Kyung Sang Nam Do. Several microbiological methods are available to determine tetracycline antibiotecs(TCs) in foods but their precision apears to be variable and the specificity is questionable. These methods are considered to be not suitable for analysis of tetracycline antibiotics in honey because honey itself has bacteriostatic action. For determination of tetracycline antibiotics in honey, therefore the High Performance Liquid Chromatography(HPLC) method was applied, and the propionic acid were determined by Gas Chromatography(5.C). Ethylacetate, as an extract solvent, was found to be suitable for seperation of TCs in honey, but methanol and acetone were not. The recoverly rate of Oxytetracycline(OTC), Tetracycline(TC), Doxycycline(DC) from honey spiked at a level of 10 $\mu $g/g were 97%, 89%, and 91%, respectively. The cailbration curve in TCs was linear expression from 2$\mu $g/ml to 10$\mu $g/ml. As the results of analysis, the residual tetracycline antibiotics were not detected in the 100 samples of honey. The recovery rate of propionic acid from honey spiked at level of 10$\mu $g/g was 98.3% , and the calibra lion curves were linear expression from 21$\mu $g/ml to 101$\mu $g/ml. As the results of analysis, the residual propionic acid was not detected in the 100 samples of honey. Retention time(min) of OTC, DC, and TC were 3.35, 4.61, and 5.30 minutes at the conditions of table 2, respectively, and retention time(min) of propionic acid was 3.50 minutes at the conditions of table 3. The residual TCs and propionic acid were not detected in the 100 samples of honey, but there is a possibility that antibiotics or propionic acid will be to remain in honey if they are used during product period in order to prevent putrefaction of honey-bee.

  • PDF

Analysis on Flexural Behavior of Spiral Steel Pipe Considering Residual Stress Developed by Pipe Manufacturing (조관에 의한 잔류 응력을 고려한 스파이럴 강관의 휨 거동 분석)

  • Kim, Kyuwon;Kim, Jeongsoo;Kang, Dongyoon;Kim, Moon Kyum
    • Journal of the Korean Institute of Gas
    • /
    • v.23 no.4
    • /
    • pp.65-73
    • /
    • 2019
  • A spiral steel pipe has been more used widely as a structural member as well as transport pipeline because the pipe can be manufactured continuously, consequently more economical than the conventional UOE pipe. As improved pipe manufacture technology makes spiral pipes to have high strength and to have larger diameters, the spiral pipes have been recently used as long distance transport pipeline with a large diameter and strain-based design is thus required to keep structural integrity and cost effectiveness of the spiral pipe. However, design codes of spiral pipe have not been completely established yet, and structural behaviors of a spiral pipe are not clearly understood for strain-based design. In this paper, the effects of residual stresses due to the spiral pipe manufacture process are investigated on the flexural behavior of the spiral pipe. Finite element analyses were conducted to estimate residual stresses due to the manufacturing process for the pipes which have different forming angle, thickness, and strength, respectively. After that, the results were used as initial conditions for flexural analysis of the pipe to numerically investigate its flexural behaviors.

Out Gassing from Plastic Substrates Affect on the Electrical Properties of TCO Films (플라스틱 기판의 Outgassing이 TCO 박막의 전기적 특성에 미치는 영향)

  • Kim, Hwa-Min;Ji, Seung-Hun
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
    • /
    • v.22 no.11
    • /
    • pp.961-968
    • /
    • 2009
  • In this work, transparent conductive oxide(TCO) films such as $In_2O_3-SnO_2$(ITO) and $In_2O_3-ZnO$(IZO) were prepared on polyethylene naphthalene(PEN) and glass substrates by using rf-magnetron sputtering system. The TCO films deposited on PEN substrate show very poor conductivity as compared to that of the TCO films deposited on glass substrates. From the results of the residual gas analysis(RGA) test, this poor stability of plastic substrate is presumed to be caused by the deteriorated adhesion between the TCO films and the plastic substrate due to outgassing from the plastic substrate during deposition of TCO films. From our experiment, it is found that the vaporization of some defects in the plastic substrates deteriorate the adhesion of the TCO films to the plastic substrate, because the most plastic substrates containing the water vapor and/or other adsorbed particles such as organic solvents. Mixing of these gases vaporized in the sputtering process will also affect the electrical property of the deposited TCO films. Inorganic thin composite $(SiO_2)_{40}(ZnO)_{60}$ film as a gas barrier layer is coated on the PEN substrate to protecting the diffusion of vapors from the substrate, so that the TCO films with an improved quality can be obtained.

Role of A-TIG process in joining of martensitic and austenitic steels for ultra-supercritical power plants -a state of the art review

  • Bhanu, Vishwa;Gupta, Ankur;Pandey, Chandan
    • Nuclear Engineering and Technology
    • /
    • v.54 no.8
    • /
    • pp.2755-2770
    • /
    • 2022
  • The need for Dissimilar Welded Joint (DWJ) in the power plant components arises in order to increase the overall efficiency of the plant and to avoid premature failure in the component welds. The Activated-Tungsten Inert Gas (A-TIG) welding process, which is a variant of Tungsten Inert Gas (TIG) welding, is focus of this review work concerning the DWJ of nuclear grade creep-strength enhanced ferritic/martensitic (CSEF/M) steels and austenitic steels. A-TIG DWJs are compared with Multipass-Tungsten Inert Gas (M-TIG) DWJ based on their mechanical and microstructural properties. The limitations of multipass welding have put A-TIG welding in focus as A-TIG provides a weld with increased depth of penetration (DOP) and enhanced mechanical properties. Hence, this review article covers the A-TIG welding principle and working parameters along with detailed analysis of role played by the flux in welding procedure. Further, weld characteristics of martensitic and austenitic steel DWJ developed with the A-TIG welding process and the M-TIG welding process are compared in this study as there are differences in mechanical, microstructural, creep-related, and residual stress obtained in both TIG variants. The mechanics involved in the welding process is deliberated which is revealed by microstructural changes and behavior of base metals and WFZ.

Analysis of Deformation and Stress Generated by Repair Welding and Its Accuracy (보수용접시 발생하는 변형 및 응력의 해석 및 정도)

  • Chang Kyong-Ho;Lee Sang-Hyong
    • Journal of the Computational Structural Engineering Institute of Korea
    • /
    • v.17 no.4
    • /
    • pp.365-374
    • /
    • 2004
  • Steel bridges, which have been damaged by load and corrosion, need repair or strengthening. That is a cause of decreasing the durability of structure. In order to solve these problems, welding repair and strengthening methods can be considered. In general, cutting and welding procedure is carried out during the repair welding. Therefore, the investigation of the behavior of residual stress and deformation generated by cutting and welding is very important for safety of structure. Residual stress and deformation produced by gas cutting and arc welding were analyzed using 2D and 3D thermal elasto-plastic FEM. According to the results, the magnitude of temperature was analyzed by 2D-FEM is smaller than that was analyzed using the 3D-FEM at the start and end edge of flange. And the magnitude and distribution of residual stress of perpendicular direction of the cutting line and welding line was analyzed by the 2D-FEM was similar to that was analyzed by 3D-FEM. Therefore, it is possible to predict cutting and welding residual stress by 2D and 3D FEM.