• Title/Summary/Keyword: recrystallization behavior

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Rapid Thermal Annealing of Silicon on Insulator (SOI) with a W-Halogen Lamp (텅스텐 할로겐 램프에 의한 절연층 상의 실리콘)

  • 김춘근;김용태;민석기
    • Journal of the Korean Institute of Telematics and Electronics
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    • v.25 no.8
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    • pp.950-958
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    • 1988
  • We have implemented a RTA system using W-halogen lamps and tried to recrystallize the phosphorus ion implanted amorphous silicon on insultor (SOI) taking advantages of seeding window. The purpose of this study is to investigate the possibility of a typical crystalline orientation occurred during the solidifying process of molten amorphous silicon layer. Experimental results show that several twin boundaries are found on the seeding window region after annealing for 15 sec at 1040\ulcorner. These twin boundaries represent that the recrystallization is partialy possible and when the annealing is done at 1150\ulcorner, (100) etch pits with <110> facets are found on the solidified amorphous silicon layer. Consequently, Hall mobility of recrystallized silicon film is measured and the thermal behavior of grain boundary is also observed by SEM.

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Creep Mechanisms of Calcium-Silicate-Hydrate: An Overview of Recent Advances and Challenges

  • Ye, Hailong
    • International Journal of Concrete Structures and Materials
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    • v.9 no.4
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    • pp.453-462
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    • 2015
  • A critical review on existing creep theories in calcium-silicate-hydrate (C-S-H) is presented with an emphasis on several fundamental questions (e.g. the roles of water, relative humidity, temperature, atomic ordering of C-S-H). A consensus on the rearrangement of nanostructures of C-S-H as a main consequence of creep, has almost been achieved. However, main disagreement still exists on two basic aspects regarding creep mechanisms: (1) at which site the creep occurs, like at interlayer, intergranular, or regions where C-S-H has a relatively higher solubility; (2) how the structural rearrangement evolutes, like in a manner of interlayer sliding, intra-transfer of water at various scales, recrystallization of gelled-like particles, or dissolution-diffusion-reprecipitation at inter-particle boundary. The further understanding of creep behavior of C-S-H relies heavily on the appropriate characterization of its nanostructure.

Prediction on Flow Stress Curves and Microstructures of 304 Stainless Steel (304 스테인레스강의 고온 유동응력곡선과 미세조직의 예측)

  • 조범호
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 1999.03b
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    • pp.171-175
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    • 1999
  • the high temperature deformation behavior of 304 stainless steel was characterized by the hot torsion test. Continuous deformation was carried out at the temperature ranges 900-110$0^{\circ}C$ and the strain rate ranges 5x10-2~5/sec. The formulation of the flow stress curves was developed as subtraction form which was based on dynamic softening mechanisms The volume fraction of dynamic recrystallization and the mean grain size could be expressed as a function of deformation variables temperature (T) strain ($\varepsilon$) strain rate ($\varepsilon$) The calculated values of flow stress and mean grain size could be well matched with experimental values.

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Effect of SiC Particle Size on Hot Workability of AA2024/$SiC_P$ Composites (AA2024/$SiC_P$ 복합재료의 열간 가공성에 미치는 강화상 크기의 영향)

  • 고병철;홍흥기;유연철
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 1997.03a
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    • pp.81-84
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    • 1997
  • The hot deformation behavior of SiCp/AA2024 composites reinforced with different sizes of SiCp reinforcements (1, 8, 15, 36, and 44${\mu}{\textrm}{m}$) was investigated by hot torsion tests. The hot restoration of the composites depending on the SiCp reinforcements particle size was studied from the effective stress - strain curves. Dynamic recrystallization (DRX) was occurred in the SiCp/AA2024 composites during the hot deformation at 320 - 43$0^{\circ}C$ under a strain rate of 1.0/sec. Also, the critical strain for DRX decreased with decreasing the reinforcement size of SiCp from 44 to 8${\mu}{\textrm}{m}$. The composite reinforced with SiCp of 8${\mu}{\textrm}{m}$ showed the highest flow stress (265 MPa) and the work hardening rate at 32$0^{\circ}C$ under a strain rate of 1.0/sec.

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Thermal Pro0perties and High Temperature Deformation Behaviors of Al-Ni-Y Amprphous Alloy (Al-Ni-Y 비정질 합금의 열적특성 및 고온변형특성에 관한 연구)

  • 고병철;김종현;유연철
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 1998.03a
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    • pp.72-75
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    • 1998
  • High temperature deformation behavior of Al85Ni10Y5 alloy extrudates fabricated with amorphous ribbons was investigated at temperature range form 300 to 550$^{\circ}C$ by torsion tests. Thermal properties of amorphous ribbons as a function of aging temperature was studied by Differential Scanning Calorimetry(DSC). The Al phase crystallite firstly formed in the amorphous ribbons and its crystallization temperature(Tx) was ∼210$^{\circ}C$. During the processings of consolidation and extrusion, nano-grained structure was formed in the Al85Ni10Y5 alloy extrudates. The as-extrudated Al85Ni10Y5 alloy and the Al85Ni10Y5 alloy annealed at 250$^{\circ}C$ for 1 hour showed the flow curve of DRV(dynamic recovery) during hot deformation at 400-550$^{\circ}C$. On the other hand, the Al85Ni10Y5 alloy annealed at 400$^{\circ}C$ for 1 hour showed the flow curve of DRX(dynamic recrystallization) during hot deformation at 450-500$^{\circ}C$.

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An Experimental Study and the Design of the Rubber Laminated Lead Damper (탄성체 적층 납삽입 제진장치의 설계 및 특성시험)

  • Lee, Wan-Ha;Park, Jin-Young;Park, Jung-Woo;Kim, Ki-Man;Park, Kun-Nok
    • Proceedings of the Korean Society for Noise and Vibration Engineering Conference
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    • 2011.04a
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    • pp.165-170
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    • 2011
  • A large number of seismic isolation systems have been developed since the early 1970s. They are basically a combination of elastomeric bearing and energy dissipators. The investigation described in this paper analyzes shear property and the frequency dependence of Lead Rubber Damper(LRD). Lead Rubber Damper is similar in shape and performance property to Lead Rubber Bearing. Experimental condition ranges from 20 to 200% in share strain and from 0.1 to 1.0Hz in frequency. When the shear strain is increased, effective stiffness and damping ratio are decreased. When the frequency is increased, change of the behavior characteristic is subtle.

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Secondary Recrystallization Behavior in Mechanically Alloyed ODS NiAI (기계적 합금화한 ODS NiAI의 이차 재결정화 거동)

  • Eo, Sun-Cheol
    • Korean Journal of Materials Research
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    • v.6 no.12
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    • pp.1248-1256
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    • 1996
  • Ni 및 AI단원소 분말을 혼합하여 attrition mill을 사용하여 분위기 속에서 기계적 합금화 NiAI 기 산화물 분산강화 금속간화합물을 제조하였다. 제조된 분말은 여러 가지 다른 미세조직을 얻기 위하여 각기 다른 공정으로 열간성형을 하였으며, 연이어 이차 재결정 조직을 얻기 위한 가공열처리(thermomechanical treatment)를 실시하였다. 이차 재결정이 일어날 수 있는 선수조건으로서의초기 미세조직과 가공열처리와의 상관관계를 조사하였다. 정상 결정립 성장의억제와 접합조직의 존재가 이차 재결정을 일으키기 위한 필요조건으로 판명되었다. 이 재료에 있어서, 잔류 변형에너지를 공급할 수 있고 결정립을 미세화 할 수 있는 특정 공정하에서 항온 열처리 후 이차 재결정이 생성됨을 알 수 있었다.

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Hot Workability Characterization of Ti Alloys Using Dynamic Material Model (동적재료모델을 활용한 티타늄합금의 고온성형성 고찰)

  • Yeom J. T.;Hyun Y. T.;Na Y. S.;Park N. K.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2001.10a
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    • pp.301-304
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    • 2001
  • Hot-compression tests were carried out to investigate the hot workability of Ti64 and Ti6246 alloys at different temperatures and strain rates. Processing maps were developed on the basis of the dynamic material model unifying the relationship among constitutive behavior, hot workability and microstructure development. Stable regions, defined on the basis of four stability criteria 0${\delta}log(m)/\frac{\bot}{\varepsilon})<0$, s<1 and ${\delta}log(s)/\frac{\bot}{\varepsilon})<0$, were found to be associated with dynamic recovery and recrystallization.

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Internal Friction Behavior in AZ31 Magnesium Alloy after Annealing Treatment (AZ31 마그네슘 합금의 어닐링 이후 내부마찰 거동)

  • Kwak, Juho;Kang, Changyong;Kim, Kwonhoo
    • Journal of Power System Engineering
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    • v.22 no.1
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    • pp.87-93
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    • 2018
  • Specimens were machined out from hot-rolled AZ31 magnesium alloy, and deformed at 623K with rolling reduction of 30%. After hot rolling, specimens were annealed at various range of temperature and time. In this study, static recrystallization was occurred during heat treatment, however, variation of main component and intensity of texture was not revealed. The results of microstructure observation, damping capacity test and dislocation mechanism indicated that increasing of damping capacity was caused by grain growth. It means that grain size is effective factor to damping capacity.

Mechanical Properties of Ultrafine Grained 5052 Al Alloy Produced by Cryogenic Rolling Process (극저온 압연으로 제조된 5052 Al 합금의 기계적 성질)

  • Nam W. J
    • Transactions of Materials Processing
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    • v.13 no.8
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    • pp.704-709
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    • 2004
  • The effect of annealing temperature on microstructures and mechanical properties of the 5052 Al sheets rolled 88% reduction at cryogenic temperature was investigated for the annealing temperature of 150 ~ $300^{\circ}C$, in comparison with those rolled at room temperature. The presence of equiaxed grains, whose size is about 200nm in a diameter, was observed in the alloy deformed 88% and annealed $200^{\circ}C$ for an hour. When compared with the deformation at room temperature, the deformation at cryogenic temperature showed the higher strengths and equivalent elongation after annealing at the annealing temperature below $200^{\circ}C$. However, for annealing above $250^{\circ}C$ materials deformed at cryogenic temperature showed the lower strength than those deformed at room temperature. This behavior might be attributed to the higher rate of recrystallization and growth in materials deformed at cryogenic temperature during annealing, due to the lager density of dislocations accumulated during the deformation.