• Korean Journal of Veterinary Service
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• v.29 no.3
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• pp.339-346
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• 2006

Semi-micro-HPLC using a column-switching technique was developed for simultaneous determination of vitamin A and E contents in infant formula. Vitamin A and E were extracted by PDA - HPLC with reversed phase column using organic solvent and their contents in Certified Reference Material (CRM) and infant formula were determined and compared with hydrolysis method and rapid extraction. Developed method has many advantages of simple and rapid sample preparation and simultaneous determination of vitamin A and E by micro-HPLC using reversed phase column.

• Earthquakes and Structures
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• v.11 no.5
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• pp.873-885
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• 2016

Determination of earthquake-safety of existing buildings requires a rather long and challenging process both in terms of time and expertise. In order to prevent such a tedious process, rather rapid methods for evaluating buildings were developed. The purpose of these rapid methods is to determine the buildings that have priority in terms of risk and accordingly to minimize the number of buildings to be inspected. In these rapid evaluation methods detailed information and inspection are not required. Among these methods the Canadian Seismic scanning method and the first stage evaluation method included in the principles concerning the determination of risk-bearing buildings promulgated by the Ministry of Environment and Urbanization in Turkey are used in the present study. Within the scope of this study, six reinforced concrete buildings damaged in Van earthquakes in Turkey are selected. The performance scores of these buildings are calculated separately with the mentioned two methods, and then compared. The purpose of the study is to provide information on these two methods and to set forth the relation they have between them in order to manifest the international validity.

• Korean Journal of Food Science and Technology
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• v.36 no.2
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• pp.189-195
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• 2004

Rapid and simple method was developed for simultaneous determination of vitamins A and E contents in infant formula. Vitamins A and E were extracted by PDA-HPLC with reversed phase column using organic solvent, and their contents in Certified Reference Material (CRM) and infant formula were determined and compared with results of Food Standards Codex and AOAC method for evaluation of developed method, Vitamins A and E contents in CRM determined by developed method were within certified range of standard values. Developed method has great advantages of simple and rapid sample preparation and simultaneous determination of vitamins A and E by PDA-HPLC using reversed phase column.

• Journal of Astronomy and Space Sciences
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• v.18 no.2
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• pp.129-136
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• 2001

The accuracy of GPS applications is heavily dependent on the satellite ephemeris and earth orientation parameter. Specially applications like as the real time monitoring of troposphere and ionosphere require real time or predicted ephemeris arid earth orientation parameter with very high quality. IGS is producing IGS ultra rapid product called IGU for real time applications which includes the information of ephemeris and earth orientation. IGU is being made available twice everyday at 3:00 and 15:00 UTC arid covers 48 hours. The first 24 hours of it are based on actual GPS observations and the second 24 hours extrapolated. We will construct the processing strategy for yielding ultra rapid product and demonstrate the propriety through producing it using 48 hours data of 32 stations.

• Proceedings of the Korean Society of Near Infrared Spectroscopy Conference
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• 2001.06a
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• pp.1072-1072
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• 2001

The purpose of this research is to evaluate rapid determination of phosphorus in soils using NIR spectroscopy. The soil samples from the fields subject to different crops and land-use in Kyeongbook province, Korea were used to make the calibration and validation of the calibration set estimating phosphorus in soil. The NIR reflectance was scanned at 2nm intervals from 1100 to 2500nm with an InfraAlyzer 500 (Bran+Luebbe Co.). Various regression analyses were used to evaluate a NIRS method for determination of phosphorus in the soil. NIR absorption approach requires many soil samples to obtain optimal prediction. Applicability of NIR spectra technique may allow for the analysis of available soil phosphorus rapidly as well as total component within a few seconds.

• Journal of the Korean Chemical Society
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• v.5 no.1
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• pp.84-87
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• 1961

A polarographic method for rapid determination of Uranium in the presence of foreign ions was proposed. The method is based on the measurement of polarogram in the sulfuric acid as supporting electrolyte. In this medium Uranyl ions give well defined reduction waves, and half-wave potentials are -0.19V vs. S.C.E. as first wave, and uncertain volt. vs. S.C.E. as second wave in $2.4 N-H_2SO_4.$ The first wave has a linear relationship between the concentration of Uranyl ion and wave height. The author also studied a method for rapid determination of Uranium in Korean monazite sand without eliminating the foreign ions. The Korean monazite sands were analyzed by this method and satisfactory result were obtained.

• Journal of the Korean Society for Precision Engineering
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• v.22 no.10 s.175
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• pp.31-38
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• 2005

• Near Infrared Analysis
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• v.1 no.1
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• pp.31-35
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• 2000

Near-infrared reflectance spectroscopy(NIRS) was used to determine the humic acids in soil samples from the fields of different crops and land-use over Youngnam and Honam regions in Korea. An InfraAlyzer 500 scanning spectrophotometer was obtained near infrared relectance spectra of soil at 2-nm intervals from 1100 to 2500nm. Multiple linear regression(MLR) or partial least square regression (PLSR) was used to evaluate a NIRS method for the rapid and nondestructive determination of humic acid, fulvic acid and its total contents in soils. The raw spectral data(log 1/R) can be used for estimating humic acid, fulvic acid and its total contents in soil by MLR procedure between the content of a given constituent and the spectral response of several bands. In which the predicted results for fulvic acid is the best in the constituents. The new spectral data are converted from the raw spectra by PLSR method such as the first derivative of each spectrum can also be used to predict humic acid and fulvic acid of the soil samples. A low SEC, SEP and a high coefficient of correlation in the calibration and validation stages enable selection of the best manipulation. But a simple calibration and prediction method for determining humic acid and fulvic acid should be selected under similar accuracy and precision of prediction. NIRS technique may be an effective method for rapid and nondestructive determination for humic acid, fulvic acid and its total contents in soils.

• Journal of the Korean Ceramic Society
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• v.13 no.4
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• pp.15-19
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• 1976

Mutual interferences of alkali and alkali-earth metals in atomic absorption were examined. For determination of Na or K interfering elements increase the absorbancy, and for Ca or Mg decrease. Since influences of coexisting elements become nearly constant by addition of large amount of same coexisting element, could be use mixed standard solution for alkali or alkali-earth metal determination in the presence of other alkali and alkali-earth metals. The metals can be readily incorporated into scheme of rapid silicate analysis. Precision and accuracy are good.

• Analytical Science and Technology
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• v.31 no.3
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• pp.134-142
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• 2018

The uranium isotopic ratio in environmental samples around nuclear facilities is important because it reveals information regarding illegal activities or anthropogenic pollution. Determination of uranium isotopes, however, is a challenging task requiring much labor and time because of the complex separation procedures and lengthy process. In this study, a rapid determination method for uranium isotopes in environmental samples was developed using. The sample was completely decomposed using the alkali fusion method. The separation procedure using extraction chromatography (UTEVA) was simplified in a single step without any further removal process for Si and major matrix elements. The established method can be completed within 3 h from sample dissolution to ICP-MS measurement. Most matrix elements and uranium isotopes in the soil samples were well separated and purified. Five types of were used to assess the method's accuracy and precision for a rapid uranium analysis method. The analytical accuracy for all CRM samples ranged from 95.1 % to 97.8 %, and the relative standard deviation was below 3.9 %. From the analytical results, one may draw conclusions that the evaluated method for uranium isotopes using alkali-fusion, the extraction chromatography process, and ICP-MS measurements is fast and fairly reliable owing to its recovering efficiencies. Thus, it is expected that the evaluated method can contribute to the improvement of environmental monitoring ability.