• 제목/요약/키워드: purity

검색결과 2,383건 처리시간 0.039초

진단용 방사성 의약품의 정도관리 (Quality Control of Radiopharmaceutical)

  • 안성민;홍태기;함준철;김성철
    • 한국콘텐츠학회논문지
    • /
    • 제9권11호
    • /
    • pp.240-246
    • /
    • 2009
  • 본 연구의 목적은 방사성 의약품의 정도관리 실험 중 방사선 및 의약품측면에서의 방사핵종 순도, 화학적 순도, 방사화학적 순도의 세 가지로 진행하였다. 또한 방사성 의약품을 표지 후 시간에 따른 표지 효율을 관찰함으로써 실제 임상에서 표지 후 어느 정도의 시간이 경과해도 사용이 가능한지 실험해 보았다. 그 결과 현재 임상에서 사용되고 있는 방사성의약품의 방사성핵종 순도와 화학적 순도는 양호한 편이었으나, 방사화학적 순도는 표지방법과 표지 시간에 따라 약간의 차이를 띄고 있었다. 방사성 의약품은 시술자의 손을 거쳐 표지되기 때문에 표지과정에 주의를 하여 정도관리에 임한다면 보다 효율적인 검사가 가능할 것으로 보여 진다.

순도를 달리한 알루미나 세라믹스의 마멸과정 및 이의 기구에 관한 연구 (A Study on The Wear Process and Wear Mechanism of the Alumina Ceramics with Different Alumina Purity)

  • 전태옥;진동규
    • 대한기계학회논문집
    • /
    • 제18권12호
    • /
    • pp.3404-3412
    • /
    • 1994
  • The present study was undertaken to investigate the dry wear process and wear mechanism of the alumina ceramics in the purity variation which are used for the mechanical seal, roll, liner and dies. The wear test was carried out under different experimental condition using the wear testing device and in which the annular surface rubbed on dry sliding condition various sliding speed, contact pressure and sliding distance. In case of alumina purity 95%, there was speed range which wear loss increased rapidly owing to enlargement of heat impact force and temperature rise of wear surface. According as the alumina purity increased, wear loss decreased but alumina purity 85% with much void and defect had the most wear loss than any other alumina purity. The friction coefficient of sliding initial stage of wear curves has a large value but according to increase of sliding distance, it decreased owing to drop of the shear strength of wear surfaces.

Purities of Ordered Ideals of Ordered Semirings

  • Ayutthaya, Pakorn Palakawong na;Pibaljommee, Bundit
    • Kyungpook Mathematical Journal
    • /
    • 제60권3호
    • /
    • pp.455-465
    • /
    • 2020
  • We introduce the concepts of the left purity, right purity, quasi-purity, bipurity, left weak purity and right weak purity of ordered ideals of ordered semirings and use them to characterize regular ordered semirings, left weakly regular ordered semirings, right weakly regular ordered semirings and fully idempotent ordered semirings.

GC-FID/Methanizer를 이용한 고순도 질소의 순도분석법 개발 (Development of analysis method for high purity nitrogen using GC-FID/Methanizer)

  • 유제이;이진복;김진석;김운중;홍기룡
    • 분석과학
    • /
    • 제35권6호
    • /
    • pp.249-255
    • /
    • 2022
  • 본 연구에서는 기체 크로마토그래피-불꽃이온화검출기(GC-FID)를 이용한 고순도 질소의 새로운 순도분석법을 개발하였다. 고순도 질소에 존재할 수 있는 불순물인 일산화탄소(CO), 이산화탄소(CO2), 및 메탄(CH4)에 대한 3 µmol/mol 수준의 인증표준물질(Certified reference material, CRM)을 중량법을 이용하여 제조하였고, 이를 순도분석에 활용하였다. 개발된 순도분석법에서는 운반가스로 초고순도 질소와 순도분석 대상 질소를 사용하여, 제조된 인증표준물질의 기체 크로마토그래피에서 얻어지는 크로마토그램의 면적 값 차이를 비교함으로써 순도분석 대상 질소의 불순물을 정량 분석하였다. 순도분석 대상 질소로는 액체질소 및 제조사가 각기 다른 3곳의 고순도 질소를 사용하였다. 또한, 개발된 순도분석법의 유효성을 평가하기 위하여 순도분석 대상 질소 내 불순물의 물질량 분율을 기존 순도분석법과 비교하였다. 두 가지 순도분석법을 이용하였을 때 대상 질소 내 불순물의 물질량 분율이 불확도 (k = 2) 내에서 서로 일치함을 확인함으로써, 개발된 순도분석법이 유효함을 확인하였다.

마이크로파를 응용한 Rubber Compound의 가황 - (I) 마이크로파에 의한 White Carbon의 가열특성 - (Microwave Application to the Vulcanization of Rubber Compound -(I) The Heating Characteristics of While Carbon by Microwave-)

  • 박찬영;김정곤;민성기
    • Elastomers and Composites
    • /
    • 제32권5호
    • /
    • pp.318-324
    • /
    • 1997
  • Since the rigid and continuous networks of high-purity silica(white carbon) were relatively transparent to microwaves, high purity silica coupled with microwaves using a zirconia susceptor at room temperature and it was then heated to its melting temperature. The low-purity silica, contained small amount of impurities, yielded greater microwave absorption owing to easy motion of the interstitial alkali ions and it was then heated to its melting temperature. X-ray diffraction patterns of the low-purity silica were broader than those of the high-purity silica due to higher concentration of non-bridging bond and more deformed random network structure. In the vulcanization process of whitened or coloured rubber compound which is employing low-purity silica(white carbon) as a reinforcing filler, vulcanizate could be obtained effectively by microwave heating energy.

  • PDF

PURE THIN FILMS FROM Ba/Ti ALKOXIDES

  • K. Musabekov;N. Korobova;Wha, Soh-Dea
    • E2M - 전기 전자와 첨단 소재
    • /
    • 제11권11호
    • /
    • pp.46-52
    • /
    • 1998
  • Barium titanate owes its great importance to the fact that its dielectric constant is about 100 times higher than that of conventional dielectric materials provided its compositional and structural purity is extremely high. The value of crystalline BaTiO3 bodies as used, for instance, in computer elements, magnetic amplifiers, memory device, ets., depend on boththe compositional and the structural purity of the BaTiO3 crystals. This purity will, in turn, depend on the purity of the raw materials used in manufacturing the BaTiO3 compound and on the particularmethods of manufacture which determine the size, homogeneity, and the structural purity of the crystals. This paper reviews the important theoretical considerations, processing techniques and applications related to sol-gel derived thin films.

  • PDF

공기정화 살균기 개발 및 성능검증 연구 (A Study on Development and Performance Test of an Air Purify-sterilizer)

  • 정재윤;장조원
    • 한국항공운항학회지
    • /
    • 제14권3호
    • /
    • pp.51-59
    • /
    • 2006
  • The air purity-sterilizer was developed and the CFD and experimental studies were carried out in order to investigate the performance of a air purity-sterilizer. Overhaul and exchange efficiency were increased by the modularization of the air purity-sterilizer. The good performance was validated by the hot-wire measurements and flow simulations in the room. Mean velocities at the exit of the air purity-sterilizer were 0.91, 1.62, 1.99, and 6.14 m/sec according to the fan mode. And the flow visualization of pured air was shown by using CFD flow simulation in the room of 24, 50 pyeong. The results show that the air purity-sterilizer has a high performance enough to produce air purity-sterilizer on a commercial scale.

  • PDF

고순도 나이오븀과 탄탈륨 희유금속의 물리적 특성평가 (Physical Property Evaluation for High Purity Niobium and Tantalum Rare Metals)

  • 김일호;박종범;유신욱;조경원;최국선;서창열;김병규;김준수
    • 한국재료학회지
    • /
    • 제15권4호
    • /
    • pp.217-223
    • /
    • 2005
  • Thermal, electrical and mechanical properties of high purity niobium and tantalum refractory rare metals were investigated tn evaluate the physical purity. Higher purity niobium and tantalum metals showed lower hardness due to smaller solution hardening effect. Temperature dependence of electrical resistivity showed a typical metallic behavior. Remarkable decrease in electrical resistivity was observed for a high purity specimen at low temperature. However, thermal conductivity increased for a high purity specimen, and abrupt increase in thermal conductivity was observed at very low temperature, indicating typical temperature dependence of thermal conductivity for high purity metals. It can be known that reduction of electron-phonon scattering leads to increase in thermal conductivity of high purity niobium and tantalum metals at low temperature.

Purity assignment of 17α-hydroxyprogesterone by mass balance method to establish traceability in measurement

  • Lee, Hwa Shim;Park, Su Jin
    • 분석과학
    • /
    • 제32권6호
    • /
    • pp.225-232
    • /
    • 2019
  • Traceability establishment in chemical measurements is a like a linkage established through an unbroken chain from the measured results to the international system (SI) of units. The primary process for traceability establishment is the purity assignment of a target material to be measured. In this study, we studied the purity assignment of 17α-hydroxyprogesterone (17-OHP). The presence of 17-OHP is indicative of congenital adrenal hyperplasia (CAH) and it builds up due to the deficiency of 21-hydroxylase and 11β-hydroxylase enzyme in the human blood. The purity assignment of 17-OHP was performed by the mass balance method, in which the impurities are categorized into four classes: total related structural impurities, water, residual organic solvents, and nonvolatiles/inorganics. The total related structural impurities were characterized by HPLC-UV; water content was determined by Karl-Fisher coulometer; and the total residual solvents and nonvolatiles/inorganics were determined by TGA. The purity of 17-OHP from a commercial manufacturer was calculated as 993.30 mg/g, and the expanded uncertainty was 0.58 mg/g. The proposed method was validated by uncertainty evaluation and comparing with the actual value of purity.

교류형 플라즈마 디스플레이 패널의 방전 조건변화에 따른 형광막의 발광특성 (Luminescence Properties of Phosphor Layer with Discharge Conditions in AC PDP)

  • 장상훈;태흥식;최경철
    • 대한전기학회논문지:전기물성ㆍ응용부문C
    • /
    • 제48권10호
    • /
    • pp.704-709
    • /
    • 1999
  • The optical properties such as luminance and color coordinates for phosphor layer were studied with applied voltage and gas pressure, Xe mixing ratio, frequency using He and Xe mixing gas in chamber like AC PDP. The luminance of red phosphor layer at constant pressure(300Toor) is increased with increasing voltage, but color purity is not varied. The luminance of red phosphor layer at constant voltage(280V)is decreased with increasing pressure, but the color purity is not varied. But the luminance is increased with increasing Xe mixing ratio at constant pressure(200Toor). And also the color purity is improved by this process. The luminance is increased up to 40kHz, but the color purity with frequency is not varied.

  • PDF