• 제목/요약/키워드: preparing room temperature

검색결과 43건 처리시간 0.024초

고분자 기판상에 제작한 Al이 첨가된 ZnO 박막에 관한 연구

  • 김경환;조범진;금민종
    • 한국반도체및디스플레이장비학회:학술대회논문집
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    • 한국반도체및디스플레이장비학회 2006년도 추계학술대회 발표 논문집
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    • pp.60-63
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    • 2006
  • Preparing AZO thin films on the polymer substrate has been widely studied Because AZO thin film has the potential applications. In this study, we prepared AZO thin films on polyethersulfon (PES) at room temperature. The AZO thin films were prepared at $O_2$ gas flow rate of 0.05 and sputtering power of 100W with different film thickness by facing targets sputtering method. The electrical, optical and crystallographic properties of AZO thin films were measured by Hall Effect measurement system, UV/VIS spectrometer, SEM and XRD. From the results, we obtained AZO thin films with a low resistivity, a transmittance of over 80% and c-axis preferred orientation.

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에멀젼을 이용한 Al2O3-ZrO2 복합분체의 제조 : II. 에멀젼-가열석유 증발법 (Preparation of Al2O3-ZrO2 Composite Powders by the Use of mulsions : II. Emulsion-Hot Kerosene Drying Method)

  • 현상훈;백종규
    • 한국세라믹학회지
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    • 제25권3호
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    • pp.284-292
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    • 1988
  • Alumina-zirconia composite powders for the purpose of improving fracture toughness and thermal shock resistance of alumina were prepared by the emulsion-kerosene drying method. The average particle size of composite powders was less then 1 $\mu\textrm{m}$ and their shapes were spherical. It was shown that the average particle size of composite powders decreased with the concentration of metal-salt in solution and the amount of span 80 added when preparing emulsions. The structure of all zirconia in composite powders heat-treated at 1200$^{\circ}C$ was a tetragonal form at room temperature. This result implied that fine zirconia particles were homogeneously dispersed in the alumina matrix.

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폴리머 기판 상에 제작한 AZO 박막의 특성 (Properties of AZO thin film prepared on polymer substrate)

  • 조범진;금민종;김경환
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 2006년도 제37회 하계학술대회 논문집 C
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    • pp.1500-1501
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    • 2006
  • Because AZO thin film has the potential applications, Preparing AZO thin films on the polymer substrate has been widely studied. In this study, we prepared AZO thin films on polyethersulfon (PES) at room temperature. The AZO thin films were prepared at $O_2$ gas flow rate of 0.05 and sputtering power of 100W with different film thickness by facing targets sputtering method. The electrical, optical and crystallographic properties of AZO thin films were measured by Hall effect measurement system, UV/VIS spectrometer, SEM and XRD. From the results, we obtained AZO thin films with a low resistivity, a transmittance of over 80% and c-axis preferred orientation.

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어깨와 대퇴부위에 건열과 습열 적용이 피부온도와 심부체온에 미치는 영향 (Effect of Heat Therapy to Superficial and Deep Body Temperatures according to Applying Dry and Moist Heats on Shoulder and Thigh)

  • 임난영;정현철;이승원;김우진
    • Journal of Korean Biological Nursing Science
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    • 제13권3호
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    • pp.269-275
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    • 2011
  • Purpose: This study was designed to help preparing the evidence-based data for the manual of heat applications by finding the differences of superficial and core temperatures after applying dry and moist heats on shoulder and thigh. Methods: Moist and dry heats were alternately applied on the 33 subjects a day apart from May 15, 2010 through June 9, 2010. The experiment was conducted with $23^{\circ}C$ to $25^{\circ}C$ room temperature and 50% to 66% of moisture from 2 to 6 p.m. After heat was applied on the shoulder of the subjects wearing shorts and gowns for 30 minutes, their superficial and core temperatures were measured. The same method was used on the thigh after two hours. Results: Both superficial and core temperatures on the shoulder and thigh increased significantly after heat therapy. There was no significant difference between the temperatures before and after intervention according to applying methods and regions. Conclusion: This study provides a theoretical basis that a dry heat is a convenient nursing intervention for hypothermic patients.

선형 대향 타겟 스퍼터를 이용하여 제작한 ITO 박막의 특성과 이를 이용하여 제작한 유기발광소자 특성 (Characteristics of ITO films grown by linear facing target sputtering (FTS) and OLEDs properties fabricated on FTS-grown ITO anode)

  • 김한기;문종민;김지환;김장주;강재욱
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2007년도 하계학술대회 논문집 Vol.8
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    • pp.401-402
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    • 2007
  • The preparation and characteristics of ITO anode films grown using a linear facing target sputtering (FTS) technique for use in organic light emitting diodes (OLED) and flexible OLED is described. The electrical, optical, and work function of the ITO anode, which was prepared by linear FTS at room temperature, were comparable to those of commercial ITO anode films. In particular, linear FTS-grown ITO films shows very smooth surface without defects such as pin hole and cracks due to low substrate temperature. Furthermore OLED with the linear FTS-grown ITO anode film shows comparable electrical and optical properties to those of OLED with the commercial crystalline-ITO anode film. This suggested that linear FTS is promising thin film technology for preparing high quality anode film in OLEDs and flexible OLEDs.

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파라-페닐렌디아민이 함유(含有)된 산화형(酸化形) 영구염모제(永久染毛制)의 물리화학적(物理化學的) 특성평가(特性評價)에 관(關)한 연구(硏究) (A Study on the Physico-Chemical Property Evaluation of Oxidative Permanent Hair Color Products Containing p-Phenylene Diamine)

  • 하병조;전동원;김경선
    • 패션비즈니스
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    • 제9권5호
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    • pp.136-144
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    • 2005
  • Oxidative hair color is currently widely used because of its beautiful light color and good dyeability. In this study, hair color, oxidative agents, and dye intermediate were reacted. Modifier, which changes color with various hue, and alkaline agent, which opens the cuticle of hair fiber and enhances the dyeing reaction, were added. For gel formation, isocetyl alcohol was used as solvent in preparing three kinds of permanent oxidative hair color. Physiochemical study of prepared permanent oxidative hair color was done for basic information acquisition. Acid perspiration test, pH measurement both at room temperature and at high temperature, drop movement test, dyeability efficiency upon the amount of hydrogen peroxide added, and humidity fastness were studied. Shampoo fastness and light fastness of prepared permanent oxidative hair color dyed hair sample were also investigated. All three kinds of hair color prepared showed good properties overall, however, dyed hair sample became reddish upon shampoo fastness and lightfastness tests.

이온성 액체를 이용한 dodecanethiol로 안정화된 금속 나노입자 합성 (Synthesis of Dodecanethiol-Capped Nanoparticles Using Ionic Liquids)

  • 이영은;이성윤;유성식
    • Korean Chemical Engineering Research
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    • 제50권5호
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    • pp.795-801
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    • 2012
  • 가장 널리 이용되고 있는 금속나노입자 중 금과 은을 친환경용매인 RTILs (room temperature ionic liquids)를 이용하여 제조하고자 하였다. 본연구에서는 두 종류의 이온성 액체, 즉 비수용성인 [BMIM][$PF_6$] (1-Butyl-3-methylimidazolium hexafluorophosphate)과 수용성인 [BMIM][Cl](1-Buthy-3-methylimdazolium chloride)를 이용하여 리간드로 안정화된 금속 나노입자를 제조하고자 하였다. 이 중 [BMIM][Cl]은 논연구에서 Dupont 등의 방법으로 직접 합성하여 물성 분석 후 사용하였으며, [BMIM][$PF_6$]은 완제품을 구입하여 사용하였다. 금과 은의 나노입자들을 습식으로 제조하는 경우의 Brust et al.[6]의 방법이 널리 알려져 있으며, 본 연구에서도 이를 기초로 하여 나노입자를 제조하였다. [BMIM][$PF_6$]로 나노입자 제조시는 이 용매가 물에 녹지 않으므로 기본적으로는 유기용매 대신 [BMIM][$PF_6$]를 사용하는 것 외에는 Brust 등과 같은 방법제조하였다. [BMIM][Cl]로 나노입자를 제조하는 경우는 이 용매가 수용성이므로 상전이제와 ethanol은 사용하지 않고 입자를 제조하였다. 이렇게 얻어진 나노입자들의 경우 [BMIM][$PF_6$]로 합성한 경우는 FT-IR, UV-vis, TEM 그리고 TGA 분석을 통하여 Brust 등이 합성한 경우와 유사한 결과를 얻었지만, [BMIM][Cl]의 경우는 형태학적으로 다른 나노입자를 얻었다. 기존의 나노입자를 제조하는 과정에서 이용되는 유기용매를 이용하는 방법을 그린용매인 이온성 액체로 대체할 수 있다는 가능성을 확인할 수 있었고, 이온성 액체의 특성에 따라서 형태학적으로 다른 입자를 얻을 수 있었으나, 이 부분은 추후 더 많은 연구가 필요하다.

난소화성 획분이 높은 난소화성 덱스트린의 제조 방법 (Methods for Preparing Indigestible Dextrin with High Indigestible Fraction)

  • 우동호;문태화
    • 한국식품과학회지
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    • 제32권3호
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    • pp.610-617
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    • 2000
  • 높은 난소화성 획분을 갖는 난소화성 덱스트린은 열처리 덱스트린의 효소 가수분해액을 에탄올 또는 강산성 양이온 교환수지(UBK 530)로 처리함으로써 제조하였다. 난소화성 획분, 식이섬유 및 수출을 고려하여 ${\alpha}-amylase$와 amyloglucosidase를 반응시킨 가수분해액으로부터 난소화성 덱스트린을 제조하기 위한 에탄올 처리의 최적 조건은 에탄올을 30%(w/w) 효소 반응액에 고형분 대비 5배로 첨가하여 상온에서 3시간 동안 방치시키는 공정이었다. 포도당을 포함하는 저분자 당류와 고분자 당류를 강산성 양이온 교환수지에 의해 분리한 결과 내열성 ${\alpha}-amylase$와 amyloglucosidase에 의한 초기 효소 반응액은 43.6%의 DPI(glucose)과 51.5%의 DP4+(maltotetaos이상)를 나타낸 반면, 양이온 교환수지에 의해 초기 효소 반응액의 50%까지 분취한 난소화성 덱스트린은 7.1%의 DPI(glucose)과 91.2%의 DP4+(maltoteoaose이상)를 나타내었다. 따라서, 초기 효소 반응액의 난소화성 획분 44.5%는 저분자 당류의 분리 후 78.9%까지 증가하였다.

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Copper(II) Selective PVC Membrane Electrodes Based on Schiff base 1,2-Bis (E-2-hydroxy benzylidene amino)anthracene-9,10-dione Complex as an Ionophore

  • Jeong, Eun-Seon;Lee, Hyo-Kyoung;Ahmed, Mohammad Shamsuddin;Seo, Hyung-Ran;Jeon, Seung-Won
    • Bulletin of the Korean Chemical Society
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    • 제31권2호
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    • pp.401-405
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    • 2010
  • The Schiff base 1,2-bis(E-2-hydroxy benzylidene amino)anthracene-9,10-dione has been synthesized and explored as ionophore for preparing PVC-based membrane sensors selective to the copper ($Cu^{2+}$) ion. Potentiometric investigations indicate high affinity of these receptors for copper ion. The best performance was shown by the membrane of composition (w/w) of ionophore: 1 mg, PVC: 33 mg, DOP: 66 mg and KTpClPB as additive were added 50 mol % relative to the ionophore in 1 ml THF. The proposed sensor's detection limit is $2.8{\times}10^{-7}$ M over pH 5 at room temperature (Nernstian slope 31.76 mV/dec.) with a response time of 15 seconds and showed good selectivity to copper ion over a number of interfering cations.

DEVELOPMENT OF A CRYOGENIC TESTING SYSTEM FOR MID-INFRARED DETECTORS ON SPICA

  • Nishiyama, Miho;Kaneda, Hidehiro;Ishihara, Daisuke;Oseki, Shinji;Takeuchi, Nami;Nagayama, Takahiro;Wada, Takehiko
    • 천문학논총
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    • 제32권1호
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    • pp.355-357
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    • 2017
  • For future space IR missions, such as SPICA, it is crucial to establish an experimental method for evaluating the performance of mid-IR detectors. In particular, the wavelength dependence of the sensitivity is important but difficult to be measured properly. We are now preparing a testing system for mid-IR Si:As/Si:Sb detectors on SPICA. We have designed a cryogenic optical system in which IR signal light from a pinhole is collimated, passed through an optical filter, and focused onto a detector. With this system, we can measure the photoresponse of the detector for various IR light using optical filters with different wavelength properties. We have fabricated aluminum mirrors which are adopted to minimize thermal distortion effects and evaluated the surface figure errors. The total wavefront error of the optical system is $1.3{\mu}m$ RMS, which is small enough for the target wavelengths ($20-37{\mu}m$) of SPICA. The point spread function measured at a room temperature is consistent with that predicted by the simulation. We report the optical performance of the system at cryogenic temperatures.