• 제목/요약/키워드: preparation condition

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Permeation Properties of Surface Modified Nanofiltration Membrane (표면 개질된 나노복합막의 투과 특성)

  • Tak Tae-Moon;Park Hyung-Kiu;Jang Gyung-Gug
    • Membrane Journal
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    • v.14 no.3
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    • pp.207-217
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    • 2004
  • In this study, we prepared nanofiltration membrane by applying the interfacial polymerization method as a way of manufacturing composite membranes. We have examined the effects of various preparation factors such as monomer concentration and composition, thermal curing condition, post treatment condition. In addition to preparation conditions, we also monitored the effects of operation conditions such as feed solution concentration and operation pressure on the permeation properties of the resulting nanofiltration membrane. We intended to increase the permeation rate of nanofiltration membrane by the enlargement of effective surface area using additives during interfacial polymerization step. With increasing the monomer concentration, membrane permeation rate are decreased with maintaining almost constant rejection. With respect to curing condition, with increasing the curing temperature both permeation rate and rejection are decreased. With increasing the ratio of MPD in amino monomer composition, permeation rate decreased drastically with high rejection. With increasing the feed solution concentration, both permeation rate and rejection decreased. Both permeation rates and rejection increased with increasing the operating pressure. Nanofiltration membrane have higher surface roughness with increasing additive concentration in the case of using MPD contained amine composition than using piperazine alone. Permeation rates are much lower than the nanofiltration membrane prepared by piperazine.

A Study on the Relation of the Later Personality Adjustment Types and the Aged Perception of the Conflict with their Married Children -Focus on the Relationships with their Eldest Sons and Wives- (노후 성격적응성향과 노인이 지각하는 기혼자녀와의 갈등관계연구 -장남부부와의 관계를 중심으로-)

  • 유영주
    • Journal of Families and Better Life
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    • v.15 no.2
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    • pp.155-172
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    • 1997
  • The purpose of this study is to examine the relation between the later personality adjustment types and the elderly percepted conflict with their married children. The subjects for this study are the aged over 60 years in Seoul both having the eldest sons' couples and perceiving their own economics level as the middle-upper. The results based on this are as followed: 1) The Active Integrated Coper is appeared in the higher educational level group in the better health condition in the 11-30 thousand won of personal expense in the professional and management occupation and in the more vigorous for social activity. The Failing Overcoper the Dependent Passive Coper and the Self-negating Undercoper is appeared in th female elder group in the later group of the older age in the lower educational level in the worse health condition in the group without spouse in one without income in the below 10 thousand won in the less preparation for the later life. 2) The problems of emotion and iew of values bring about the conflicts between them and theirs rather than the financial problem. when they are in the worse health condition in the group without religion in the group not cohabiting their eldest sons' couples and in the group not well-prepared for their later life as the socio-demographic variables the old recognized the seriousness of the conflict with their eldest sons' couples. 3) The lower the Active Integrated Coper is and the higher the Failing Overcoper is the more intense the conflict between them and their eldest sons' couples is. 4) The t-test to examine the difference in the old's conflict with their eldest sons' couples among the later groups shows that it is in the less the Active Integrated Coper and in the more the Failing Overcoper that the conflict is more surfaced. 5) The educational level the level of the later life preparation the contact frequency with their daughter the level of their social activity as the socio-demographic variables and the Failing Overcoper as the later personality adjustment type answer for 22 percentage of the conflict.

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Strength Development Properties of Latex Modified Concrete For New Concrete Bridge Deck Overlay (신설 콘크리트 교면 덧씌우기를 위한 라텍스 개질 콘크리트의 강도발현 특성)

  • Yun, Kyong-Ku;Kim, Ki-Heoun;Lee, Joo-Hyung;Hong, Chang-Woo;Kim, Dong-Ho
    • International Journal of Highway Engineering
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    • v.3 no.3 s.9
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    • pp.135-146
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    • 2001
  • This study focused on the investigation of compressive and flexural strengths development, and bond strength of latex modified concrete in order to validate the feasibility of application into concrete bridge deck overlay. Pull-out bond test was used for evaluating the bond strength of latex modified concrete to substrate. The main experimental variables were latex-cement ratio, surface preparation and moisture levels. The compressive strength of latex modified concrete decreased slightly and the flexural strength increased as the latex content increased from 5% to 20%. This might be due to the flexibility latex filled in voids and interconnections of hydrated cement and aggregates by a film of latex particles, respectively. In general, increasing the amount of latex will produce concrete with increased tensile and flexural strength and lower modulus of elasticity. Significant improvements in bond strength between new and existing concrete were achieved through the modification of the new concrete bridge deck overlay by latex polymers. The effect of surface preparation on bond of latex modified concrete to conventional concrete were significant at the conditions by sand paper and wire brush. A better bond could be achieved by rough surface rather than smooth. The saturated condition of surface is the most appropriate moisture level among the considered followed by dry condition and wet condition.

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Studies on the effects of rearing condition in the inducing of silkworm virus disease (가잠의 Virus병 유발에 미치는 사육조건의 영향에 관한 연구)

  • 한계용
    • Korean Journal of Microbiology
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    • v.8 no.1
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    • pp.21-34
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    • 1970
  • This experiment was undertaken to examine the injurious environment conditions for occuring of the virus disease, grasserie and cytoplasmic polyhedrosis in rearing of silk worms, to observe of cytoplsamic polyhedrosis diseased silkworms with histological preparation and to define the virus origin on the gattine and the disease of shrinked form after moulting (Okichijimi). The results obtained are as follows. 1) The grasserie in spring season rearing was remarkably infected in highly percent with 20.1 % in high temperature condition during 3rd to 4th instar, the high temperature during 1st to 2nd instar and 5th instar in 16.5% and 16.3%, respectively. In the fall season rearing, the disease was infected by the feeding of soft leaves plot in 5.3% and 4.8%, respectively with significant difference in 5% level, accordingly, it was thought to the nutritional condition is a factor in occuring of the disease. 2) In spring season rearing, the number ofl infected silk worms of cytoplasmic polyhedrosis was increased in the high temperautre and high humidity conditions, and in fall season rearing, order of the low temperature and high humidity plot, first feeding plot and feeded with hard leaves plot were found insome high infected ratio of the disease than control plot. 3) The occuring of cytoplasmic polyhedrosis was observed even in control rearing plot with the examining of anatomical and histological preparation in spring and fall. 4) It was found that the high diseased ratio of the gattine and disease of shrinked form after moulting in 21.8% of control and 93.2% in feeded with inocylated plot in the biosassay of inoculum. It was defined as a virus flacherie acoording to the Danaka and Shimizu's examine method.

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Preparation of Nano-sized Zirconia Powders by the Impregnation Method (함침법에 의한 지르코니아 나노 분말의 합성)

  • Han, Cheong-Hwa;Kim, Soo-Jong
    • Journal of the Korean Ceramic Society
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    • v.49 no.5
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    • pp.454-460
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    • 2012
  • The nano-sized zirconia powders were synthesized in an impregnation method using pulp and $ZrOCl_2{\cdot}8H_2O$ as an initial material. The synthesized powders were characterized by XRD and FE-SEM. The particle size of the powder was controlled by preparation conditions, such as drying temperature and time. As a result of the various drying and calcination conditions, 30~50 nm sized homogeneous zirconia particles were obtained at $800^{\circ}C$ for 1 h. Crystallization and the rapid growth of particles were accelerated with increasing calcination temperature and time. Tetragonal phase generated below $800^{\circ}C$ were transferred to monoclinic phase with increasing calcination temperature and time. Moreover, above $800^{\circ}C$, heat treatment time had very large influence on the particle growth, and the change of drying condition also had large influence on the growth of a crystal.

Intake Valve Temperature Effect on the Mixture Preparation in a SI Engine During Warm-up

  • 신영기
    • Transactions of the Korean Society of Automotive Engineers
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    • v.5 no.5
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    • pp.51-66
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    • 1997
  • A heat transfer model of the intake valve in a spark ignition engine is presented, which is calibrated with a number of the valve temperature profiles measured during engine warm-up for the gaseous fuel(propane). The valve is divided into four identical elements for which the assumption of lumped thermal mass is applied. The calibration is made so that the difference between the measued and simulated valve temperatures becomes minimal. Then the model is applied to the cases of the liquid fuel(indolene) to estimate the amount of the liquid fuel vaporized from the intake valve by assuming that fuel evaporation accounts for the deficit of the heat balance budget. The results of the model show quantitative contribution of each heat transfer source to the heat balance. The behavior of the calculated mass fraction of the fuel vaporized from the intake valve explains how the liquid fuel evaporate during engine warm-up. The mass fraction at warmed-up condition is closely related with the fraction directly targeted on the valve back by the fuel spray geometry.

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Pressurized Pneumatic Grit Conveying Characteristics in Pipeline for Open Blasting Robot (오픈 블라스팅 로봇에서 관로내의 그리트 가압이송 특성)

  • Kim, Won-Bae;Yang, Seok-Won;Lee, Sang-Bum;Kim, Soo-Ho
    • Proceedings of the KSME Conference
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    • 2007.05a
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    • pp.1185-1189
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    • 2007
  • In this paper, to improve the efficiency of pressurized pneumatic grit conveying for ship block open blasting process. Pressurized pneumatic grit conveying is defined as the transportation of grit(abrasive) in a compressed air flow. Total Pressure loss in flexible hose for pneumatic conveying is sum of pressure losses due to gas and grit and needle type pressure transmitter for measured pressure loss. haracteristics of grit open blasting by pneumatic conveying were studied experimentally. Studies variables were blasting nozzle ID, length and ID of flexible hose, grit flow rate, flow rate and pressure of transport air. It was experimentally proved that optimal open blasting condition and cost effective operation regarding grit blasting, obtaining a high qulity surface preparation(Sa $2^{\frac{1}{2}}$).

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A Study on the Preparation of Antibacterial Biopolymer Film

  • Cho, Dong-Lyun;Na, Kun;Shin, Eun-Kyung;Kim, Hyun-JIn;Lee, Ki-Young;Go, Jin-Hwan;Choi, Choon-Soon
    • Journal of Microbiology and Biotechnology
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    • v.11 no.2
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    • pp.193-198
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    • 2001
  • Preparation of antibacterial biopolymer film which is suitable for food packaging film was investigated using K-carrageenan as a base material. K-Carrageenan showed good biodegradability and film-forming characteristic but poor mechanical properties under humid condition. Also, various bacteria grew well on its surface. The poor mechanical properties could be improved by mixing with alginate at a 1:1 ratio and crosslinking with $CaCl_2$ solution. Antibacterial property coul be provided by modifying the K-carrageenan film surface with acrylic acid plasma followed by ion-exchange with $Ag^+$ ions. Such prepared film still showed good biodegradability by various fongi.

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Facile preparation of superhydrophobic thin films using non-aligned carbon nanotubes

  • Goh, Yee-Miin;Han, Kok Deng;Tan, Lling-Lling;Chai, Siang-Piao
    • Advances in nano research
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    • v.2 no.4
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    • pp.219-225
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    • 2014
  • A simple preparation method on creating superhydrophobic surface using non-aligned carbon nanotubes (CNTs) was demonstrated. Superhydrophobic CNT thin films were prepared by doping a sonicated mixture of CNTs and chloroform onto a glass slide. Water contact angles of the CNT thin films were measured using a contact angle goniometer. The thin films were characterized using laser microscope and scanning electron microscope. Experimental results revealed that the highest average contact angle of $162{\pm}2^{\circ}$ was achieved when the films' thickness was $1.628{\mu}m$. The superhydrophobic surface was stable as the contact angle only receded from $162{\pm}2$ to $157{\pm}2^{\circ}$ after 10 min under normal atmospheric condition.

Preparation and Characterization of Antireflective Film in $TiO_2-SiO_2$ System by Sol-Gel Method (Sol-Gel법에 의한 $TiO_2-SiO_2$계 저반사 박막의 제조 및 특성)

  • 윤태일;최세영;이용근;이재호
    • Journal of the Korean Ceramic Society
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    • v.30 no.9
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    • pp.775-783
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    • 1993
  • TiO2-SiO2 system anti-reflective(AR) film was prepared to decrease reflectance on the glass surface. The experiments were carried out as fellow, 1) preparation & hydrolysis of TiO2-SiO2 system sols. 2) glass dipping, and 3) drying & heat treatment. We investigated the refractive index and thickness of film with viscosity, zeta-potential of sol, sol concentration, withdrawal speed, drying and heat treatment condition. As a result, we prepared good qualitative Quarter-Half-Quarter type anti-reflective film that had minimum, 0.02% and average reflectance, 0.087% in the visible region.

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