• 제목/요약/키워드: preparation condition

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Preparation and Analysis of Activated Carbon Fiber from PAN Precursor(II) (PAN 선구체로부터 활성 탄소섬유의 생산과 분석(II))

  • 김진홍;최중열;박병기;정경락;김공주
    • Textile Coloration and Finishing
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    • v.4 no.4
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    • pp.97-103
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    • 1992
  • For manufacturing a high sorptive ACF, we used orthognal array experimental design to get optimum condition. The ability of ACF was measured by $CCl_4$ adsorption and showed those manufacturing conditions were effective in the order of treatment time>oxidative gas>treatment temperature. The optimal condition presented the maximum adsorption rate was at 90$0^{\circ}C$ for 6 minutes with $CO_2$/$H_2O$ gas in the PAN based ACF manufacturing process. The adsorption rate of developed ACF in this experiment was over 100%.

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The Investigation of Reaction Parameters on the Reactivity in the Preparation of TiB2 by SHS (자전연소합성법에 의한 TiB2 분말의 제조에 있어 반응성에 대한 반응변수의 고찰)

  • Shin, Chang-Yun;Park, Young-Chul;Lee, Huk-Hee;Nersisyan, Hayk;Won, Chang-Whan
    • Journal of the Korean Ceramic Society
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    • v.43 no.1 s.284
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    • pp.16-21
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    • 2006
  • The preparation of $TiB_2$ by SHS in $B_2O_3-Mg-TiO_2$ system was investigated in this study. In the preparation of $TiB_2$, the effect on reactivity and reaction products of the initial pressure of inert gas in reactor, the content of Mg and $TiO_2$ in mixture was investigated. The minimum initial pressure of inert gas in reactor for SHS reaction in this system was 5atm, and as the pressure increased, the concentration of unreacted Mg decreased and combustion temperature increased. At the initial inert gas pressure in reactor of 50atm, the optimum composition for the preparation of pure $TiB_2$ was $B_2O_3+5Mg+TiO_2$. The $TiB_2$ synthesized in this condition had an irregular shape and the particle size of $1\~3{\mu}m$.

Preparation of Ti−TiH2−C−N2Powder by Combustion Reaction in the System of TiC0.7N0.3 (Ti−TiH2−C−N2계에서 연소반응에 의한 TiC0.7N0.3 분말의 제조)

  • Shin, Chang-Yun;Nersisyan, Hayk;Won, Chang-Whan
    • Journal of the Korean Ceramic Society
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    • v.44 no.1 s.296
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    • pp.37-42
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    • 2007
  • The preparation of $TiC_{0.7}N_{0.3}$ powder by SHS in the system of $Ti-TiH_2-C$ ($N_2$ atmosphere) was investigated in this study. In the preparation of $TiC_{0.7}N_{0.3}$ powder, the effect of gas pressure, compositions such as Ti, $TiH_2$, C, and additive in mixture on the reactivity were investigated. At 50 atm of the initial inert gas pressure in reactor, the optimum composition for the preparation of pure $TiC_{0.7}N_{0.3}$ was $0.75Ti+0.25TiH_2+0.7C+0.5NaCl$. The $TiC_{0.7}N_{0.3}$ powder synthesized in this condition was a single phase with irregular shape.

Preparation of FeB by SHS (Self Propagating High Temperature Synthesis) (자전연소합성법에 의한 FeB 분말의 제조)

  • Shin, Chang-Yun;Won, Chang-Whan
    • Journal of the Korean Ceramic Society
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    • v.45 no.7
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    • pp.418-422
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    • 2008
  • The preparation of FeB by SHS in $B_2O_3-Mg-Fe-Fe_3O_4$ system was investigated in this study. In the preparation of FeB, the effects of the initial pressure of inert gas in reactor, the content of Mg and $Fe_3O_4$ in mixture on the reactivity and reaction products was investigated. The minimum initial pressure of inert gas in reactor for SHS reaction in this system was 25 atm, and as the pressure increased, the concentration of unreacted Mg decreased and combustion temperature increased. At the initial inert gas pressure in reactor of 25 atm, the optimum composition for the preparation of pure FeB was $1.5B_2O_3$+3.43Mg+ 1.7Fe+$0.1Fe_3O_4$. The FeB synthesized in this condition had an irregular shape and the particle size of $5\;{\mu}m$.

Preparation and Stability of Microemulsion Containing Quaternary Ammonium Salt (4급 암모늄염을 함유한 마이크로에멀젼의 제조 및 안정성)

  • Lee, Jang-Weon;Jeong, Noh-Hee
    • Journal of the Korean Applied Science and Technology
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    • v.20 no.1
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    • pp.44-50
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    • 2003
  • We studied on the preparation and evaluation of O/W type microemulsion containing "wax, liquid paraffine and quaternary ammonium salt". And also it was obtained to stability of microemulsions by mono ethylene glycol(MEG) addition. The microemulsions were generally prepared at 96${\sim}$97$^{\circ}C$ by the phase inversion method. We used polyoxyethylene(20) sorbitan monooleate(POE(20)SMO) and distearyl dimethyl ammonium chloride(D.D.A.C.) as the emulsifiers at microemulsion preparation. From the results, we could get best condition for microemulsion preparation, in case of oil phase, montanic ester wax ; 1.1wt%, paraffine wax ; 1.1wt%, liquid paraffine ; 3.1wt%, propylene glycol ; 0.6wt% and ethylene glycol monobutyl ether ; 0.6wt%, when the ratio(wt%) of D.D.A.C. and POE(20)SMO were 2 : 3. And also we could obtained that the distributed particle size of the final microemulsions were about 8${\pm}$1.5nm and the mean particle size was 7${\pm}$0.5nm. We got following results from final microemulsions that the percent of transmittance; 96${\sim}$98% at 700nm. And the microemulsion blended with MEG of 5${\sim}$15wt% showed smaller particle size and more stable distribution than non-containing MEG.

Financial Soundness and Retirement Preparation of Korean Households (가계의 재무건전성과 은퇴준비에 관한 연구)

  • Kim, Soon-Mi
    • Journal of Family Resource Management and Policy Review
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    • v.18 no.4
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    • pp.27-52
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    • 2014
  • This study aims to investigate the financial soundness of Korean households and its effects on the retirement preparation of these households. The sample consisted of 1,031 households selected from the 4th Korean Retirement and Income Study (KReIS) by the National Pension Research Institute in 2012. The empirical results are as follows. According to the logistic regression model, the statistically significant factors affecting the retirement preparation of Korean households are gender, occupation type, residence, satisfaction with economic condition, and type of financial soundness-sound households or insolvency-risky households. In other words, more female-headed households and households with higher levels of occupation are less likely to prepare for retirement. The households that are more likely to prepare for retirement are those that are lived in metropolitan areas as opposed to the countryside; further, households that are more economically sound are also more likely to prepare for retirement. In particular, sound households and insolvency-risky households are less likely to prepare for retirement compared to liquidity-risky households.

Preparation of β-SiAlON Powder by Combustion Reaction in the System of Si-Al-SiO2-NH4F(β-Si3N4) (Si-Al-SiO2-NH4F(β-Si3N4)계에서 연소반응에 의한 β-SiAlON분말의 제조)

  • Min, Hyun-Hong;Shin, Chang-Yun;Won, Chang-Whan
    • Journal of the Korean Ceramic Society
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    • v.43 no.10 s.293
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    • pp.595-600
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    • 2006
  • The preparation of $\beta$-SiAlON powder by SHS in the system of $Si-Al-SiO_2-NH_4F(\beta-Si_3N_4)$ was investigated in this study. In the preparation of SiAlON powder, the effect of gas pressure, compositions such as Si, $NH_4F$, \beta-Si_3N_4$ and additive in mixture on the reactivity were investigated. At 50 atm of the initial inert gas pressure in reactor, the optimum composition for the preparation of pure $\beta$-SiAlON was $3Si+Al+2SiO_2+NH_4F$. The $\beta$-SiAlON powder synthesized in this condition was a single phase $\beta$-SiAlON with a rod like morphology.

Difference of Neuronal Recovery by Incubation Condition after Transient Hypoxia (배양조건에 의한 일과성 저산소상태 후 신경세포회복의 차이)

  • Moon, Soo-Hyeon;Oh, Jae-Inn;Park, Youn-Kwan;Chung, Heung-Sub;Lee, Hoon-Kap;Lee, Ki-Chan
    • Journal of Korean Neurosurgical Society
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    • v.29 no.9
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    • pp.1161-1170
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    • 2000
  • Objective : The transverse hippocampal slice is one of the most commonly studied in vitro models of mammalian brain physiology. However, despite its broad usage, there has been no standardization of slice preparation techniques or recording condition. It is well known that variations in recording conditions can result in profound different effects to neuronal responses. Evoked field potentials, recorded extracellularly, were used to investigate the effects of variations in hippocampal slice preparation protocol on hypoxia responses of CA1 neurones. Material & Methods : Before hypoxic injury, hippocampal slices were incubated for 4 hours. During incubation period, the slices were placed in a incubation chamber($21^{\circ}C$) for recovery from preparation injury and then transferred to recording chamber($34^{\circ}C$) for more recovery and baseline electric recording with current stimulation(0.1Hz). Various time periods in incubation chamber and recording chamber were applied to each experimental group(group 1=60min : 180min, group 2=90min : 150min, group 3=180min : 60min, time in incubation chamber : time in recording chamber) before 10 min hypoxia produced by replacing 95% $O_2$+5% $CO_2$ mixed gas to 95% $N_2$+5% $CO_2$ gas. Calcium, Magnesium ions and several drugs effecting on glutamate receptor also were studied. Recoveries from hypoxic injury of hippocampal slices were estimated by percent recovery of population spike(PS). Statistic analysis of study were performed using paired t-test. Results : The percent recovery of PS after 10min hypoxia was considerably enhanced by increasing the period of current stimulation during incubation period before hypoxic injury. Temperature effect on the result of this experiment was also studied(group 4) but the result from this showed no statistic significance. Low magnesium ion concentration of artificial CSF(Mg-free aCSF) during incubation period enhanced the recovery of PS but low calcium (calcium-free) and high magnesium ion concentration(2mM) reduced it after hypoxic injury. L-glutamate($100{\mu}M$) and AP-5($50{\mu}M$) had no effect on the recovery of PS but CNQX($10{\mu}M$) in artificial CSF during incubation period markedly enhanced the recovery of PS. Co-treatment of AP-5($50{\mu}M$), CNQX($10{\mu}M$) and high magnesium concentration(2mM) enhanced recovery of PS in immediate following period of hypoxic injury but the effect of cotreatment after then decayed rapidly and lost statistic significance. Conclusions : Judging from above results, the condition of baseline recording is important in observing the recovery of population spike after hypoxia, and the time and the condition should be controled more strictly to obtain reliable results.

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The Study of Thinned Young Apples Fermentation by Manipulating Preparation Treatment and Sugar Content (꼬마사과를 활용하여 다양한 발효 제조방법과 설탕량이 발효에 미치는 영향)

  • Chung, Sung Won;Supeno, Destiani;Pratama, Pandu Sandi;Choi, Won Sik
    • Journal of the Korean Society of Industry Convergence
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    • v.19 no.4
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    • pp.237-244
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    • 2016
  • This paper investigates the possibility to increase the economic value of the thinned young apple trough fermentation process. It is studies the optimal fermentation condition of thinned young apple by manipulating preparation treatment and sugar content. To do this following steps are done. Firstly, different preparation treatment for thinned young apple such as whole apple, cutting apple, and blending apple were done. The different sugar content such as $24^{\circ}Brix$, $15^{\circ}Brix$ and $4^{\circ}Brix$ was added. Secondly, the sugar contents and pH level were measured during fermentation process. Finally, statistical analysis was used to examine the relation between the preparation treatment, sugar content and pH level during the fermentation process. The experimental result shows that the different preparation treatment influences to the fermentation process. The blending apple treatment gave lower pH level compared to other kind treatments. The sugar content of thinned young apple was decrease during the fermentation process. The statistical analysis shows that the manipulation preparation treatment and sugar content affect the final pH level and whole fermentation process. Experimental result shows that the thinned young apple fermentation could be proposed as new alternative product in the market. The best fermentation process was obtained from blending thinned young apple treatment with $24^{\circ}Brix$.

Preparation of Monodispersed Titania from TPOT (TPOT로부터 단분산 TiO2분말 합성)

  • 안영필;최석홍
    • Journal of the Korean Ceramic Society
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    • v.25 no.6
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    • pp.677-684
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    • 1988
  • Titania powders were obtained from the various hydrolysis condition the variation of Alkoxide, water/Alcohol, REaction, Temp., reaction time and solvent system were investigated. In this result, spherical monodisperesed titania gel powders(≒0.7${\mu}{\textrm}{m}$) were obtained using EtOH(as solvent), and this method had rapid reaction time compare with iso-PrOH(as solvent).

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