• Title/Summary/Keyword: preparation condition

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Preparation of the Anti-Reflective(AR) Coating Film by Sol-Gel Method to Improve the Efficiency of Solar Cell (태양전지 효율 향상용 졸-겔 법에 의한 반사방지 코팅막의 제조)

  • Kim, Hyosub;Kim, Youngho;Choi, Jaeyune
    • Journal of Hydrogen and New Energy
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    • v.25 no.2
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    • pp.145-150
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    • 2014
  • This study investigates the preparation of anti-reflective (AR) coating film to improve the efficiency of solar cell. The AR coating film was successfully obtained by dip-coating with AR coatings prepared by sol-gel method. Fluoroalkylsilane was additionally introduced into the coatings to give the self-cleaning effect of AR coating film. We performed the abrasion test, pencil scratch hardness test and cross-cut test to identify the mechanical strength of AR coating film. As the results, the transmittance of AR coating films with 9.07, 18.13 and 27.20 of IPA/MTMS molar ratios were 93.1, 93.6 and 95.3%, respectively. The water contact angle and transmittance of AR coating film increased by the introduction of hydrophobicity. The prepared AR coating film shows the high level of abrasion, hardness and adhesion. The IPA/MTMS molar ratio of 27.20 and the withdrawing speed range of 0.20 ~ 0.28cm/sec are the optimal coating condition in terms of the transmittance and mechanical strength of AR coating film.

Preparation Conditions of Extracts from Salmon Frame using an Autoclave (고온가압에 의한 연어 frame 추출물의 제조조건)

  • JI, Seong-Gil;Koo, Jae-Geun;Kwon, Jae-Seok;Han, Byung-Wook;Kim, Hyung-Jun;Heu, Min-Soo;Kim, Jin-Soo
    • Korean Journal of Fisheries and Aquatic Sciences
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    • v.42 no.4
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    • pp.307-315
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    • 2009
  • This study was conducted to investigate optimal conditions for preparation of extracts from salmon frame using an autoclave. According to the results of various extraction conditions (extraction method, extraction time, volume and pH of extraction solution, and necessity of re-extracting), higher quality extracts could be prepared by adding salmon frame into 3 times (vol/wt) of water to raw material, and then autoclaving for 4 hrs before filtering extracts with cheese cloth. For efficient use as basic materials of liquid or powder Gomtang, however, fish odor of the extracts prepared under optimal condition should be improved.

A Study on the Lifetime Characteristics of AC-PDP as a Parameter of MgO Preparation (MgO 증착 변수에 따른 AC-PDP의 수명 특성 연구)

  • Choi, M.S.;Kim, Y.R.;Choi, Y.C.;Park, C.S.;Kim, D.H.;Lee, H.J.;Park, C.H.
    • Proceedings of the KIEE Conference
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    • 2002.07c
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    • pp.1631-1635
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    • 2002
  • In order to be good display, the ac PDP lifetime should be guaranteed over 30000 hours. Therefore, to satisfy these demands, it is need to find out main factors in ac PDP affecting the lifetime. In this paper, the characteristics of lifetime as a parameter of the MgO deposition rate conditions is investigated. MgO protective layers is fabricated by E-beam. Before measuring the lifetime we have carefully peformed high temperature evacuation and aging procedure, which is essential for providing the initial condition of our experiment. If MgO deposition rate increased, MgO film becomes dense and an adhesive power of MgO film gets better and because occurrence rate of the MgO cluster decreases, lifetime of MgO will be improved. As a result, ac PDP lifetime can be improved due to the improvement of MgO by MgO preparation conditions.

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Optimization of Shark (Squatina oculata) Cartilage Hydrolysis for the Preparation of Chondroitin Sulfate

  • Jo, Jin-Ho;Do, Jeong-Ryong;Kim, Young-Moung;Kim, Dong-Soo;Lee, Taek-Kyun;Kim, Seon-Bong;Cho, Seung-Mock;Kang, Suk-Nam;Park, Douck-Choun
    • Food Science and Biotechnology
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    • v.14 no.5
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    • pp.651-655
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    • 2005
  • Enzymatic hydrolysis of shark (Squatina oculata) cartilage (SC) was optimized by response surface methodology (RSM) for chondroitin sulfate (CS) preparation. Among 11 commercial proteases, Maxazyme NNP showed highest productivity (CS yield per enzyme cost) of CS. Optimal hydrolysis conditions determined by RSM were 1.63% and 2.87 hr for enzyme concentration and hydrolysis time ($r^2\;=\;0.9527$, p<0.0l), respectively and highest yield of hydrolysate under the conditions was 42.3%. The yield ($43.1{\pm}2.1%$) and CS content ($24.8{\pm}0.1%$) of hydrolysate at optimal condition verified statistical optimization of SC enzymatic hydrolysis was valid.

Preparation of PVDF/PDMS Composite Membrane and Separation of n-butanol/water Mixtures by Pervaporation (PVDF/PDMS 복합막의 제조와 투과증발을 이용한 n-부탄올/물 혼합물의 분리)

  • Lee, Yong-Taek;Jee, Ki-Yong;Jeon, Eun-Joo;Kim, No-Won
    • Membrane Journal
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    • v.19 no.3
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    • pp.212-221
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    • 2009
  • This study focuses on preparation of PVDF/PDMS composite membranes to effectively separate butanol from water-butanol mixture using pervaporation. We prepared various composite membranes by changing PVDF concentration of support layer and PDMS cross-linking condition of active layer. Pervaporation performance was tested by measuring butanol flux and separation factor with various cases of butanol concentration, temperature, and flow rate of feed. As results, performance of our novel PVDF/PDMS membranes surpasses that of PVDF/POMS membrane, manufactured by GKSS (Germany), in term of butanol flux, permeate concentration, and separation factor.

A Study for Target Area Set-up Plan of Environmental Assessment (환경평가 대상지역의 설정방안에 대한 연구)

  • Sun, Hyosung;Choi, Jungyu
    • Journal of Environmental Impact Assessment
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    • v.21 no.2
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    • pp.247-254
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    • 2012
  • This paper seeks for the set-up plan in the reasonable target area of environmental assessment. Domestically, the target area of environmental assessment is set up by the adjustment of opinion collection about the assessment scope result of an environmental factor. In a foreign country, the boundary of the target area for a development project is established with the environmental, economical, and social viewpoint based on the standard for significantly environmental impact. Based on the analysis of the present condition at home and abroad, the first set-up plan for the reasonable target area of environmental assessment is the preparation of the detailed term definition related to the target area of environmental assessment. The second is the arrangement of the judgement standard for significantly environmental impact. The quantitative assesment item can apply the present standard or regulation, and the qualitative assessment item can establish the standard based on factual and objective data. The last is the preparation of the reference material or the guideline for deciding the initial target area by the judgement standard and determining the final target area by opinion collection in the stage of scoping.

Adhesion improvement between metal and ceramic substrate by using ISG process (ISG법에 의한 금속과 세라믹기판과의 밀착력 향상)

  • 김동규;이홍로;추현식
    • Journal of Surface Science and Engineering
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    • v.32 no.6
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    • pp.709-716
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    • 1999
  • Ceramic is select for an alternative substrate material for high-speed circuits due to its low-thermal expansion. As, in this study, ceramic was prepared by ISG (interlayer sol-gel) process using metal salts and a metal alkoxide as the starting materials. Generally ceramic substrate is used electroless copper plating for the metallization. But it has been indicate weakely the adhesion strength between the substrate and copper layer. Therefore, this research, using the ISG process on the preparation of homogeneous and possible preparation at law temperature fabricated sol solution. Using of the dip coating method was coated for the purpose of giving the anchoring effect on the coating layer and enhancing the adhesion strength between the $Al_2$O$_3$ substrate and copper layer. This study examined primary the characteristic of the sol making condition and differential thermal analysis (DTA) X-ray diffraction (XRD) were mearsured to identify the crystal phase of heat treatment specimens. The morphology of the coated films were studied by scanning electron microscopy(SEM). As a resurt, XRD analysis was obtained patterns of $\alpha$-cordierite after heat-treatment about 2 hours at $1000^{\circ}C$. SEM analysis could have seen a large number of voids on coated film. The more contants of$ Al_2$$O_3$ Wt% was increased the more voids was advanced. Peel adhesion strength has a maximum in the contants of the TEOS:ANE of 1:0.7 mole%. In this case, adhesion strength has been measured 1150gf, peel adhesion strength were about 10 times more than uncoated of the ceramics film.

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Research on the Actual Condition and Consciousness of Female College Students and Alternatives for Job-seeking from the Perspective of Gender Equality (여대생들의 취업의식 실태조사 및 성평등적 관점의 취업 증진 방안)

  • Shin, Mal-Shik;Kim, Kyeong-Shin
    • Korean Journal of Human Ecology
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    • v.12 no.2
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    • pp.183-199
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    • 2003
  • The purposes of this research were to analyse the female college students' appraisals and demands about actual conditions of job-seeking and to propose the developmental alternatives from the perspectives of gender equality. The data were obtained through 510 female students living in Gwangju. The major findings were as follows: 1) Women's needs of job-seeking were very intensive but their preparation level was relatively low. Colleges' support system and organization utility were uneffective because their programs were not specified for women. Women generally recognized that social improvement for gender equality in employment system were very important and more practical methods and contents were demanded in education for job-seeking. 2) Women's grade and major were significant variables in the differences of job preparation, consciousness of job-seeking, social support and appraisals. Therefore, college supporting systems must consider students' characteristics. 3) The job-seeking mechanisms must be changed to more effective systems for the achievement of gender equality. Also community members, colleges and students should make collaborate endeavors for the women empowerment.

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Preparation of Biodegradable Poly(2-ethylhexylacrylate) as Oil Sorbers (흡유제인 생분해석 Poly(2-ethylhexylacrylate)의 제조)

  • Yoo, Su-Yong;Lee, Dong-Hwan;Kam, Sang-Kyu;Lee, Min-Gyu
    • Journal of Environmental Science International
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    • v.19 no.1
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    • pp.97-103
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    • 2010
  • The biodegradable oil absorption resin was prepared by the suspension polymerization of the modified starch and 2-ethylhexyl acrylate (2-EHA). The highest oil-absorption capacity of B-PEHA prepared showed at the condition of the modified starch content of 10 g and ethyleneglycol dimethacrylate (EGDMA) of 0.133 wt%. Its maximum oil absorption capacity per g of oil absorber was chloroform 30.88 g, toluene 19.75 g, xylene 18.78 g, tetrahydofuran (THF) 15.96 g, octane 11.43 g, hexane 9.5 g diesel oil 12.80 g, and kerosene 13.79 g, respectively. The biodegradation of poly-2-ethylhexylacrylate (B-PEHA) determined by enzymatic hydrolysis showed approximately 17~20%. The results showed that the preparation of the biodegradable oil absorption resin is available using the modified starch.

Optimization of Barium Titanate Slip for Tape Casting Using Design of Experiments

  • Kwon, Sung-Wook;Darsono, Nono;Yoon, Dang-Hyok
    • Journal of the Korean Ceramic Society
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    • v.43 no.9 s.292
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    • pp.519-526
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    • 2006
  • A full-factorial design of experiments with three input factors and two levels for each factor including center points was utilized for the preparation and characterization of twelve types of $BaTiO_3$ slips for tape casting. Ceramic powders with different particle sizes, different milling methods such as high energy milling and conventional ball milling, and two types of dispersant with different polymeric species were chosen as input factors in order to investigate their effects on slip and on green tape properties. Tape casting, a small rectangular-shaped K-square preparation, characterization and quantitative data analysis using statistical software were followed. Ceramic powder was the most significant among three input factors for the output responses of slip viscosity and green tape density, showing more favorable results with large particles than with very fine ones. In addition, high energy milling for only 30 min was more efficient than 24h of conventional ball milling in terms of powder dispersion and milling. The optimum condition based on the experimental results was a slip exposed to high energy milling with large ceramic particles along with a methylethyl acetate dispersant.