• Title/Summary/Keyword: preparation condition

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Development of Preparation Technique of Sintered Ni Electrode (소결식 니켈극 제조기술 개발)

  • Kim, Chan-Jung;Kim, Dai-Ryong
    • Journal of Hydrogen and New Energy
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    • v.10 no.3
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    • pp.159-170
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    • 1999
  • Recently Ni/MH secondary battery have been studied very extensively because of containing no pollutants as well as superior performance. However comparing to widely studying high capacity of hydrogen storage alloys electrode, the capacity of Ni electrode is inferior. Using for high capacity Ni/MH battery as a anodic materials, the study about high capacity Ni electrode is necessary. To making high capacity Ni electrode, active materials were impregnated in various polarization impregnation conditions. Plaque, milling for 6hr and sintered at $800^{\circ}C$, indicated porosity over 80%, and porosity were increased with proper condition electrochemical etching treatment. Proper impregnation condition was 40~80mA/cm, polarizing time was 5~10min.

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Measurement of Indoor Air Quality in a Kindergarten (유치원내 실내공기환경 측정)

  • Kim, Yun-Deok;Lim, Soo-Young
    • Journal of the Korean Institute of Educational Facilities
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    • v.14 no.1
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    • pp.52-57
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    • 2007
  • Kindergarten children are engaged in the age of physical immaturity as well as the rapid growth. The indoor air contaminants that are proved to affect even the full grown adults are obvious to have no little influence to immature small children in a growth period. In May 2004, for the multi purpose facilities and newly constructed apartments, the Ministry of Environment announced "Indoor Air Quality Control Law for the Multi Purpose Facility," which made the interests to be focused in the urgent understanding of current condition and preparation of measures about the indoor air pollution. In Dec 2005, the law was revised to obligatorily notify the amount of Formaldehyde and Volatile Organic Compounds in the case of newly constructed apartments with more than 100 houses. However, since the kindergarten takes none of the classifications, even the current condition is not grasped although it is directly connected to the health of growing children. Therefore, the study aims to analyze indoor air pollution of one selected kindergarten in Incheon city.

Synthesis of $Fe_4N$ Powder and Its Magnetic Properties for Magnetic Recording (자기기록용 $Fe_4N$ 분말의 합성 및 자기특성)

  • 변태봉;오재희
    • Journal of the Korean Ceramic Society
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    • v.28 no.2
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    • pp.93-100
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    • 1991
  • For determination the optimum manufacturing condition Fe4N powder for magnetic recording media, we have studied the following important conditions : the effect of particle size of metal powder on the nitridation, the condition of nitridation on the formation and magnetic properties of Fe4N, and stability of Fe4N powder against temperature and change on standing. The results can be summarized as : 1) Single phase Fe4N is formed at 50v/o of ammonia concentration during the nitridation reaction, 2) Single phase Fe4N is formed above 40$0^{\circ}C$, 15min regardless of the metal powder sizes, 3) Coercivity and saturation magnetization of Fe4N powder almost constant value until 20 day-passing from preparation date.

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Optimization of Iced cookiess with the Addition of Pine leaf Powder (솔잎 가루 첨가 냉동 쿠키의 제조 배합비의 최적화)

  • Jin So-Yeon;Joo Na-Mi;Han Young-Sil
    • Korean journal of food and cookery science
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    • v.22 no.2 s.92
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    • pp.164-172
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    • 2006
  • The purpose of this study was to find the optimal mixing condition of three different amounts of pine leaf powder, butter and sugar for preparation of pine leaf cookies. The optimum mixing condition for pine leaf cookies was optimized by response surface methodology The optimum mixing rates of pine leaf powder, butter and sugar were 8.6 g, 252.8 g and 154.1 g for color, 8.4 g, 240.7 g and 149.8 g for appearance, 8.8 g, 246.5 g and 154.7 g for flavor and 10.9 g, 277.1 g and 134.6 g for texture respectively. The optimum mixture ratio which fulfilled all items was pine leaf powder 9.4 g, butter 270.5 g and sugar 141 g.

Preparation of Red Ginseng Extract Rich in Acidic Polysaccharide from Red Tail Ginseng Marc Produced After Extraction with 70% Ethyl Alcohol (홍미삼 알콜 추출박을 이용한 산성다당체 다량 함유 홍삼 엑기스 제조)

  • 도재호;이종원
    • Journal of Ginseng Research
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    • v.20 no.1
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    • pp.60-64
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    • 1996
  • In this study, we investigated the appropriate conditions to extract acidic polysaccharide and to prepare red ginseng extract being rich in acidic polysaccharide from red tail ginseng marc produced after manufacturing alcoholic extract from red tail ginseng. Amount of acidic polysaccharide in red tail ginseng marc was about 11%. The best condition for the extraction of acidic polysaccharide from the marc was using of 3~5 mg of $\alpha$-amylase/g residue/15 ml of distilled water, and the amount of acidic polysaccharide in water extract of the residue treated with $\alpha$-amylase was about 27%. So, it is possible to manufacture red ginseng extract being rich in acidic polysaccharide using water extract of red tail ginseng alcoholic residue as extraction solvent. From the above results, we suggest that red tail ginseng residue produced by manufacturing alcoholic extract of red tail ginseng has high potencies in the utilization of waste material.

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The Effect of Reaction Parameters in the Characteristic of PZT Powders Synthesized by SHS (SHS법으로 합성된 PZT분말의 특성에 미치는 반응변수의 영향)

  • Kim, Byeong-Beom;Yang, Beom-Seok;Yun, Ki-Seok;Won, Chang-Whan
    • Journal of the Korean Ceramic Society
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    • v.42 no.5 s.276
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    • pp.314-318
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    • 2005
  • The effect of reaction parameters in the characteristic of $Pb(Zr_{0.52}Ti_{0.48})O_3$ (below nominal PZT) powders by SHS was investigated in this study. In the preparation of PZT, the effect of starting material contents, pressure, additive on phase fraction and morphology was investigated respectively. The optimum condition of PZT powders were prepared by SHS is $0.37Pb_3O_4+0.52ZrO_2+0.48TiO_2+0.35KClO_3+0.5C,\;(P_{Ar}= 50 atm)$. The PZT powder synthesized in this condition had an spherical shape and the particle size of 0.8$\mu$m.

A Study on the Preparation of Thin-Film Composite Membrane with Polyethersulfone Supporting Membrane (역삼투 복합막 제조(II) 폴리에테르설폰막의 제조와 복합막 제조에 관한 연구)

  • 이동진;민병렬;이병철;송희열
    • Membrane Journal
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    • v.4 no.1
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    • pp.46-56
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    • 1994
  • The performane of prepared Thin-Film Composite membrane depends on supporting membrane, concentration of monomers, dipping time of supporting membrane into monomer solution, reachon time between monomers, curing temperature and time and posttreatment. This study was conducted for searching the optimal condition for making the composite membrane. For this purpose, supporting membrane and composite membrane was made under various condition and at each step were tested.

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Preparation of Nanosized Palladium-Graphene Composites and Photocatalytic Degradation of Various Organic Dyes

  • Kim, Jae Jin;Ko, Weon Bae
    • Elastomers and Composites
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    • v.51 no.1
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    • pp.10-16
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    • 2016
  • Nanosized palladium particles were synthesized using palladium(II) chloride, trisodium citrate dihydrate, and sodium borohydride under stirring condition. Nanosized palladium-graphene composites were prepared from palladium nanoparticles, and graphene was enclosed with polyallylamine under stirring condition for 1 h followed by ultrasonication for 3 h. Nanosized palladium-graphene composites were heated in an electric furnace at $700^{\circ}C$ for 2 h and characterized by X-ray diffraction, scanning electron microscopy, and transmission electron microscopy. UV-vis spectrophotometry was used to evaluate the nanosized palladium-graphene composites as a catalyst in the photocatalytic degradation of various organic dyes such as methylene blue, methyl orange, rhodamine B, and brilliant green under ultraviolet light at 254 nm.

A Study on the Operational Environment of Railway Signalling System (철도 신호시스템 환경요구사양 및 시험사양에 관한 연구)

  • Joung, E.J.;Hwang, J.G.;Lee, J.W.;Kim, Y.M.
    • Proceedings of the KIEE Conference
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    • 2000.07b
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    • pp.1384-1386
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    • 2000
  • To determine operational requirement, the environmental condition for an equipment must be investigated, and to certify equipment's normalized operation, appropriate test must be carried out under the considered environmental condition. The actual environmental conditions to which equipment is likely to be exposed are normally complex and will comprise a number of environmental factors and corresponding parameters, When defining the environmental conditions for a certain application it is, therefore, necessary to list the factors involved and select the appropriate severity. The operational environment is structured in two separate such as requirements, guidance and test specifications. For the preparation to determine operational requirement, operational environment of railway signalling equipment is investigated.

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Preparation and Analysis of Activated Carbon Fiber from PAN Precursor(I) (PAN 선구체로부터 활성 탄소섬유의 생산과 분석(I))

  • 김진홍;이화선;박병기;정경락;김공주
    • Textile Coloration and Finishing
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    • v.4 no.4
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    • pp.90-96
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    • 1992
  • In the PAN-based ACF manufacturing system stabilization step was improved with chemical treatment (preoxidation) in order to yield higher carbon content and to avoid excessive fragmentation during carbonization and activation process. The optimal condition of preoxidation was at 18$0^{\circ}C$ for 4 minutes in sodium glyceroxide in glycerine (concentration of NaOH was 0.02 meq/g). To investigate low temperature stabilization effect, preoxidized PAN fiber heated 22$0^{\circ}C$ to 26$0^{\circ}C$ as a function of treatment time and oxidative gas atmosphere, and analysed by infrared spectrum and TGA. As a results of IR and TGA, it was clear that impregnated[preoxidative] PAN had 14% higher residual than untreated PAN at 100$0^{\circ}C$ and the optimal condition of stabilization was at 26$0^{\circ}C$ for 3.5 hours within $N_2$ atmosphere.

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