• Title/Summary/Keyword: powder method

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Synthesis of Nanoporous $TiO_2$ Materials Using Sol-gel Combustion Method and Its Photovoltaic Characteristics (나노 다공질 구조의 이산화티타늄 박막 제작과 광전변환 특성 고찰)

  • Heo, Jong-Hyun;Sung, Youl-Moon
    • The Transactions of The Korean Institute of Electrical Engineers
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    • v.58 no.2
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    • pp.322-326
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    • 2009
  • In this work, nanoporous $TiO_2$ powder was fabricated using Ketjen black, and applied in photovoltaic device based on the Dye-sensitized Solar Cells (DSCs). $TiO_2$ powder was fabricated using Ti-isopropoxide and 2-propanol by sol-gel combustion method. For added $0{\sim}2g$ variable of Ketjen black, characteristic of porosity, size of particle and crystallite of obtained $TiO_2$ nano powder was investigated. The photovoltaic efficiency of the prepared DSCs was measured using $TiO_2$ film which prepared on each different heat treatment temperature($100^{\circ}C{\sim}600^{\circ}C$) with paste of $TiO_2$ powder. The porosity and size in particle of $TiO_2$ powder made with Ketjen black Ig was influenced significantly effect to DSCs characteristic. Heat treatment at $500^{\circ}C$ makes the better photovoltaic efficiency which around 6.11%($J_{sc}=13.35mA/cm^2$, $V_{oc}=0.73V$, ff=0.63). The sol-gel combustion method was useful to DSCs fabrication.

Proposal of Rapid Quality Evaluation Method for Powder of OPC that is Received in Raw Concrete Plant using Hydromete's Principle (Hydromete의 원리를 이용한 레미콘 공장에 입고되는 OPC의 분말도 신속 품질평가법 제안)

  • Lee, Jae-Jin;Lee, Jea-Hyun;Hyun, Seong-Yong;Kim, Yeong-Tae;Han, Min-Cheol;Han, Cheon-Goo
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2017.11a
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    • pp.193-194
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    • 2017
  • In this research, the density value of the turbid solution is measured by using the principle of inexpensive but easy Hydrometer method for cement delivered to the actual raw concrete plant, By analyzing the correlation of powder aid, we will try to present a scheme that can be utilized as a method of acquisition acquisition inspection. As a result of the analysis, it was found that there was a large difference between the measured powders assisted with cement powder on the report, and the correlation with the actually measured powder aid Hydrometer density value was good. Therefore, using the method of Fig. 3, it was possible to know that the degree of powder quality of cement delivered to the raw concrete factory can be evaluated quickly and utilized at the time of argument inspection.

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Manufacture of AlSi10Mg Alloy Powder for Powder Bed Fusion(PBF) Process using Gas Atomization Method (가스 분무법을 이용한 Powder Bed Fusion(PBF) 공정용 AlSi10Mg 합금 분말 제조)

  • Im, Weon Bin;Park, Seung Joon;Yun, Yeo Chun;Kim, Byeong Cheol
    • Journal of Powder Materials
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    • v.28 no.2
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    • pp.120-126
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    • 2021
  • In this study, AlSi10Mg alloy powders are synthesized using gas atomization and sieving processes for powder bed fusion (PBF) additive manufacturing. The effect of nozzle diameter (ø = 4.0, 4.5, 5.0 and 8.0 mm) on the gas atomization and sieving size on the properties of the prepared powder are investigated. As the nozzle diameter decreases, the size of the manufactured powder decreases, and the uniformity of the particle size distribution improves. Therefore, the ø 4.0 mm nozzle diameter yields powder with superior properties. Spherically shaped powders can be prepared at a scale suitable for the PBF process with a particle size distribution of 10-45 ㎛. The Hausner ratio value of the powder is measured to be 1.24. In addition, the yield fraction of the powder prepared in this study is 26.6%, which is higher than the previously reported value of 10-15%. These results indicate that the nozzle diameter and the post-sieve process simultaneously influence the shape of the prepared powder as well as the satellite powder on its surface.

Effects of Different Planting Method and Amount of Applied Compost Powder on Yield of Rapeseed (Brassica napus L.) (유채의 재식방법과 퇴비 시용량 차이가 수량에 미치는 영향)

  • Shin, Dong-Young;Kim, Sang-Kon;Kwon, Byung-Sun;Jung, Dong-Soo;Lim, June-Taeg;Hyun, Gyu-Hwan;Kuk, Yong-In
    • Korean Journal of Plant Resources
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    • v.22 no.1
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    • pp.37-41
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    • 2009
  • In order to find out the optimum compost powder, fertilizer level and planting method of high yielding F1 variety, Cheongpungyuchae, this experiment was conducted with 2 compositions of compost powder level and 3 different planting method at the experiment paddy field of Mokpo Experiment Station, National Institute of Crop Science, RDA. Cheongpungyuchae, rapeseed variety was grown under different compost powder level and planting method with the highest yielding variety. Yield components such as ear length, total branch, number of pods per ear and oil content were highest at the plots with compost powder 1,500 kg/10a at level and planting method, Oct.30, transplanting with 50 ${\times}$ 30 cm. Judging from the results reported above, at optimum compost powder level and planting method of rapeseed seemed to be 1,500 kg/10a compost powder and transplanting method with 50 cm row spacing and 30 cm planting space.

Application of Rapid Sample Preparation Method and Monitoring for Cholesterol Content in Chicken Egg and Egg powder

  • Park, Jung-Min;Jeong, In-Seek;Kwak, Byung-Man;Ahn, Jang-Hyuk;Leem, Donggil;Jeong, Jayoung;Kim, Jin-Man
    • Food Science of Animal Resources
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    • v.33 no.5
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    • pp.672-677
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    • 2013
  • The aim of this study was to develop sample preparation method and evaluate the exact cholesterol content in egg and egg powder purchased from Korean markets, and to determine whether significant differences exist among various egg products, since a variety of products are available in Korean markets and there are no recent databases for cholesterol. To evaluate the cholesterol content in chicken egg sold in Korean local market, a simple method using non-heated saponification to determine cholesterol for emulsified foods was applied. The results of recovery for egg and egg powder were in a range of 92.4-105.0%, with a relative standard deviation between 1.1% and 2.8% by using gas chromatography-flame ionization detector. Therefore, the total cholesterol content in whole egg was estimated between 160.8 and 226.3 mg/egg (AV(average) $186.8{\pm}3.5$), which is similar or lower than previously reported levels. The value for cholesterol in egg powder was estimated between 2.94 and 3.49 mg/g (AV $3.23{\pm}0.15$). We suggested method that can be applicable to chicken egg and egg powder matrix as providing rapid and accurate determination of cholesterol in egg and egg powder. This information will be helpful for processed food producers for deciding food labels of cholesterol content.

Preparation of PZT-Ceramics by Coprecipitation Method (공침법에 의한 PZT-Ceramics의 제조)

  • 안영필;최석홍;이병우
    • Journal of the Korean Ceramic Society
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    • v.25 no.2
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    • pp.168-172
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    • 1988
  • In order to prevent the PbO vaporization during calcination and to produce the powder of good sinterability, a coprecipitation method for preparing homogeneous Lead-Zirconate-Titanate (PZT) powder from aqueous salt solution is described. In this method, the PZT-ceramics show low calcining and sintering temperature, and they have good sintering and electronic properties.

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A Study on the Effect of Frozen Dough after Fermentation with Sweet Dough Bread (단과자빵의 1차 발효 후 냉동생지에 관한 연구)

  • 윤미숙;이정훈
    • The Korean Journal of Food And Nutrition
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    • v.14 no.4
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    • pp.317-321
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    • 2001
  • Sweet dough bread is made by using sponge & dough method with the sweet dough formula which consists of wheat gluten and baking powder. The effect of wheat gluten and baking powder to the bread has been studied after the dough frozen, stored, thawed, fermented. and baked. The bread quality has been evaluated by measuring the product volute and also by the sensory evaluation after baking. When 4% of wheat gluten and 4% of baking powder were added into the dough. the bread has a larger volume than that of 2% wheat gluten and 2% baking powder in volume. However. wheat gluten shows better result than baking powder in terms of volume. In sensory evaluation, the bread has higher score when 2% of wheat gluten and 2% of baking powder were added into the dough than that of 4% wheat gluten and 4% baking powder. Consequently, breads show better result when 2% wheat gluten and 2% baking powder were added into the dough than that of 4% wheat gluten and 4% baking powder.

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The effect of process parameters on copper powder particle size and shape produced by electrolysis method

  • Boz, Mustafa;Hasheminiasari, Masood
    • Steel and Composite Structures
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    • v.15 no.2
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    • pp.151-162
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    • 2013
  • In this study, an electrolyzing device for the production of metal powders was designed and fabricated. The production of copper powders was performed using a variety of current densities, anode-cathode distances and power removal times. The effect of these parameters on powder particle size and shape was determined. Particle size was measured using a laser diffraction unit while the powder shape was determined by SEM. Experimental results show that an increase in current density leads to a decrease in powder particle size. In addition particle shape changed from globular dendritic to acicular dendritic with increasing the current density. Distance between the cathode and anode also showed a similar influence on powder particle size and shape. An increase in time of powder removal led to an increase in powder particle size, as the shape changed from acicular dendritic to globular dendritic.

The Effect of Ni Addition on the Sintering Kinetics of Ball-milled Mosi$_2$ Powder Compacts (Ni 첨가가 볼밀링한 MoSi$_2$분말성형체의 소결속도에 미치는 영향)

  • 최선호;홍경태;김영도;문인형
    • Journal of Powder Materials
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    • v.5 no.4
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    • pp.241-249
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    • 1998
  • Sintering kinetics of ball-milled $MoSi_2$ was studied with the addition of Ni. $MoSi_2$ powder with the average particle size of 1 $\mu\textrm{m}$ was obtained from ball-milling of 10 $\mu\textrm{m}$ powder. Small amount of Ni was added to the ball-milled $MoSi_2$ powder by salt solution and reduction method. The powder was compacted into cylindrical shape at 200 MPa and isothermally sintered in a $H_2$ atmosphere at the temperature range of 1100~$1400^{\circ}C$ for 3~600 minutes. The changes of linear shrinkage and sintered density were monitored as a function of sintering time. The microstructure was observed by using optical microscopy and scanning electron microscopy. Phases were identified by X-ray diffratometer and electro-probe micro analysis. Sintering kinetics of Ni-added powder was compared to as-milled powder and the apparent activation energy was calculated from Arrhenius plot.

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Parameter Investigation for Powder Compaction using Discrete-Finite Element Analysis

  • Choi, Jinnil
    • Journal of Powder Materials
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    • v.22 no.5
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    • pp.337-343
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    • 2015
  • Powder compaction is a continually and rapidly evolving technology where it is a highly developed method of manufacturing reliable components. To understand existing mechanisms for compaction, parameter investigation is required. Experimental investigations on powder compaction process, followed by numerical modeling of compaction are presented in this paper. The experimental work explores compression characteristics of soft and hard ductile powder materials. In order to account for deformation, fracture and movement of the particles, a discrete-finite element analysis model is defined to reflect the experimental data and to enable investigations on mechanisms present at the particle level. Effects of important simulation factors and process parameters, such as particle count, time step, particle discretization, and particle size on the powder compaction procedure have been explored.