• 대한기계학회논문집
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• 제15권6호
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• pp.1982-1989
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• 1991

본 연구에서는 AISI 강은 대부분 열처리후에 사용되는 고강도강으로 용접시 발생하는 높은 잔류응력 분포를 제거 또는 감소시키기 위해서 여러가지 방법이 사용된 다. 잔류응력 제거는 용접후 풀림처리를 하면 잔류응역이 제거된다. 그러나 풀림 처리 하기전에 용접부에 높은 잔류응력 제거는 용접후 풀림처리를 하면 잔류응력이 제 거된다. 그러나 풀림처리 하기전에 용접부에 높은 잔류응력에 의해 균열이 생성될 수 있으므로 용접시 높은 잔류응력이 생성되지 않도록 예열 및 후열처리를 필요로한 다. 그러므로 본 연구에서는 예열 및 후열이 잔류응력 분포에 어떠한 영향을 주는가 를 실험적인 방법에 의해 연구하였다.

• Journal of Welding and Joining
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• 제17권5호
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• pp.83-88
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• 1999

In this paper resistance projection weldability of Zn coated steels with post treatment has been discussed. Projection welding was performed by a condenser discharge type power source which was equipped with welding parameter monitoring system. Mechanical test results indicated that the effect of post coatings on the projection front changed showing very small very small spattering at the weld strength was negligible. However, contamination rate of the block electrode varied depending on the post treatment coatings. Test results also showed that projection height before welding should be kept to be 80-100% of the specimen thickness as far as the surface quality was taken into consideration. Based on the high speed photography, discharge condition at the beginning stage of the welding process. It was considered that the spattering reduced the weld strength slightly at the optimum heat input range.

• 열처리공학회지
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• 제16권1호
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• pp.16-25
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• 2003

Recently, semi-solid forming (SSF) Process has been applied in many automobile parts for improved weight reduction, better environmental protection and energy savings. SSF process was well developed for high volume production of light weight aluminum components. In this paper, knuckle has been manufactured by SSF and then the microstructures and mechanical properties were investigated followed by various heat-treatment conditions. It was found that the examined microstructure was equiaxed at the whole cross-section area.

• 대한기계학회논문집A
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• 제30권4호
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• pp.402-408
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• 2006

Dissimilar friction welding were produced using 15(mm) diameter solid bar in chrome molybedenum steel(KS SCM440) to carbon steel(KS S45C) to investigate their mechanical properties. The main friction welding parameters were selected to endure good quality welds on the basis of visual examination, tensile tests, Vickers hardness surveys of the bond of area and H.A.Z and microstructure investigations. The specimens were tested as-welded and post-weld heat treated(PWHT). The tensile strength of the friction welded steel bars was increased up to 100% of the S45C base metal under the condition of all heating time. Optimal welding conditions were n=2,000(rpm), $P_1=60(MPa),\;P_2=100(MPa),\;t_1=4(s),\;t_2=5(s)$ when the total upset length is 5.4 and 5.7(mm), respectively. The peak of hardness distribution of the friction welded joints can be eliminated by PWHT. Two different kinds of materials are strongly mixed to show a well-combined structure of macro-particles without any molten material and particle growth or any defects.

• Journal of Welding and Joining
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• 제18권5호
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• pp.70-76
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• 2000

The effect of Post Weld Heat Treatment(PWHT) of RE36 steel for marine structure was investigated with parameters such as micro-vickers hardness, corrosion potential and corrosion current density of weld metal(WM), base metal(BM) and heat affected zone(HAZ), and both Al alloy anode generating current and Al alloy anode weight loss quantity etc. Hardness of post-weld heat treated BM, WM and HAZ is lower than that of As-welded condition of each region. However, hardness of HAZ was the highest among those three parts regardless of PWHT temperature and corrosion potential of WM was the highest among those three parts without regard to temperature and corrosion potential of WM was the highest among those three parts without regard to PWHT temperature. The amplitude of corrosion potential difference of each other three parts at PWHT temperature $550^{\circ}C$, $650^{\circ}C$ are smaller than that of three parts by As-welded condition and corrosion current density obtained by PWHT was also smaller than that of As-welded condition. Eventually, it was known that corrosion resistance was increased by PWHT. However both Al anode generating current and anode weight loss quantity were also decreased by PWHT compare to As-welded condition when RE36 steel is cathodically protected by Al anode. Therefore, it is suggested that the optimum PWHT temperature with increasing corrosion resistance and cathodic protection effect is $550^{\circ}C$.

• The Journal of Advanced Prosthodontics
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• 제8권2호
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• pp.94-100
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• 2016

PURPOSE. To evaluate the effects of hydrogen peroxide pretreatment and heat activation of silane on the shear bond strength of fiber-reinforced composite posts to resin cement. MATERIALS AND METHODS. The specimens were prepared to evaluate the bond strength of epoxy resin-based fiber posts (D.T. Light-Post) to dual-curing resin cement (RelyX U200). The specimens were divided into four groups (n=18) according to different surface treatments: group 1, no treatment; group 2, silanization; group 3, silanization after hydrogen peroxide etching; group 4, silanization with warm drying at $80^{\circ}C$ after hydrogen peroxide etching. After storage of the specimens in distilled water at $37^{\circ}C$ for 24 hours, the shear bond strength (in MPa) between the fiber post and resin cement was measured using a universal testing machine. The fractured surface of the fiber post was examined using scanning electron microscopy. Data were analyzed using one-way ANOVA and post-hoc analysis with Tukey's HSD test (${\alpha}=0.05$). RESULTS. Silanization of the fiber post (Group 2) significantly increased the bond strength in comparison with the non treated control (Group 1) (P<.05). Heat drying after silanization also significantly increased the bond strength (Group 3 and 4) (P<.05). However, no effect was determined for hydrogen peroxide etching before applying silane agent (Group 2 and 3) (P>.05). CONCLUSION. Fiber post silanization and subsequent heat treatment ($80^{\circ}C$) with warm air blower can be beneficial in clinical post cementation. However, hydrogen peroxide etching prior to silanization was not effective in this study.

• 열처리공학회지
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• 제36권5호
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• pp.285-297
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• 2023

The effects of aging treatment sequence, specifically pre-aging and post-aging, on the microstructure and mechanical properties of Al-Zn-Mg-Cu aluminum alloys has been studied in comparison to symmetrically rolled specimens. In symmetrically rolled specimens, a straight-band precipitation distribution was observed, whereas asymmetrically rolled specimens exhibited a curved-band microstructure of fine precipitates. Notably, the asymmetrically rolled specimens displayed higher strengths. In the case of post-aging, the aging process occurred after rolling, and the dislocations generated during rolling acted as nucleation sites for precipitates during aging. This resulted in the formation of fine precipitates, contributing to improved mechanical properties compared to symmetric rolling. To enhance strength of the Al-Zn-Mg-Cu aluminum alloys, asymmetric rolling proves to be more effective than symmetric rolling, with post-aging showing greater efficacy than pre-aging.

• 대한치과재료학회지
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• 제44권4호
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• pp.337-348
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• 2017

본 연구에서는 소성 시 냉각속도를 조절하는 것과 동시에 소성 후 추가적인 후열처리를 시행하는 것이 후열처리를 시행하지 않는 것보다 합금의 경도 상승에 더욱 효과적인지 알아보고자, 다목적용 Ag-Pd-Zn-In-Sn계 합금을 이용하여 모의소성 시 냉각속도의 조절이 소성 및 후열처리에 따른 합금의 경도변화에 미치는 영향을 조사하여 다음과 같은 결과를 얻었다. 다목적용 Ag-Pd-Zn-In-Sn계 합금의 모의소성 시 냉각속도를 조절함에 따라 합금의 연화가 억제되었다. Stage 0(4단계의 냉각속도 중 가장 빠른 속도; 소성로 챔버가 소성 종료 즉시 전체가 열린 상태로 냉각되는 단계)으로 냉각속도를 조절하여 합금을 소성한 경우, 모의소성 과정에서 합금이 연화되었으며, 적절한 시간동안의 후열처리가 경도상승에 효과적이었다. Stage 3(4단계의 냉각속도 중 가장 느린 속도; 소성로 챔버가 소성완료 후 닫혀진 상태로 냉각되는 상태)으로 냉각속도를 조절하여 합금을 소성한 경우, 모의소성 과정에서 합금이 연화되지 않았으며, 추가적인 후열처리는 합금의 경도를 하강시켰다. Stage 0으로 모의소성 된 합금에서 30분간의 후열처리에 의해 경도가 크게 상승한 원인은 소성에 의해 기지 내로 고용되었던 석출물이 다시 기지 밖으로 활발하게 석출된 것에 기인하였다. Stage 3으로 모의소성 된 합금에서는 후열처리에 의해 석출물이 기지 내로 다시 고용되었고, 새로운 석출상의 생성이 미미하여 후열처리가 경도 상승에 기여하지 못하였다.

• 열처리공학회지
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• 제24권4호
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• pp.199-202
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• 2011

Ga doped ZnO thin films were deposited with RF magnetron sputtering on glass substrate without intentional substrate heating and then the effect of post deposition annealing temperature on the structural, optical and electrical properties of the films was investigated. The post deposition annealing process was conducted for 30 minutes in a vacuum of $1{\times}10^{-3}$ Torr and the vacuum annealing temperatures were 150 and $300^{\circ}C$, respectively. As increase annealing temperature, GZO films show the increment of the prefer orientation of ZnO (002) diffraction peak in the XRD pattern and the optical transmittance in a visible wave region was also increased, while the electrical sheet resistance was decreased. The figure of merit obtained in this study means that GZO films which vacuum annealed at $300^{\circ}C$ have the highest optoelectrical performance in this study.

• 열처리공학회지
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• 제25권2호
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• pp.85-89
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• 2012

Transparent conductive ZnO/Ag/ZnO (ZAZ) multilayer films were deposited by Radio frequency (RF) magnetron sputtering and direct current (DC) magnetron sputtering. The effects of post deposition vacuum annealing temperature on the structural, electrical and optical properties of the ZAZ multilayer films were investigated. The thickness of ZAZ films is kept constant at ZnO 50 nm/Ag 5nm/ZnO 45 nm, while the vacuum annealing temperatures were varied from 200 and $400^{\circ}C$, respectively. As-deposited ZAZ films exhibit a sheet resistance of $6.1{\Omega}/{\Box}$ and optical transmittance of 72.7%. By increasing annealing temperature to $200^{\circ}C$, the resistivity decreased to as low as $5.3{\Omega}/{\Box}$ and optical transmittance also increased to as high as 82.1%. Post-deposition annealing of ZAZ multilayer films lead to considerably lower electrical resistivity and higher optical transparency, simultaneously by increased crystallization of the films.