• Journal of the Korean Applied Science and Technology
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• v.30 no.1
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• pp.57-63
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• 2013

Ammonium dinitramide (AND) is one of the most promising oxidizers in propellants without chlorinated pollution to the atmosphere in these days. Potassium sulfamate (PS) is a key substance in ADN synthesis as forming nitrates such as $-N(NO_2)_2$. In this paper, potassium sulfamate as a starting material for ADN synthesis was prepared in a lab scale through crystallization with ethanol solvent, and observed the effects on the yield and purity of KDN. The prepared potassium sulfamates were analyzed using FE-SEM, XRD, BET and TGA-DSC. The lab-made PS, which was ground to $20{\mu}m$ showed more beneficial than a commercial product achieving high yield and purity of the synthesized KDN. It would be associated closely with crystallinity, porosity and pore size of prepared PS.

• Proceedings of the Materials Research Society of Korea Conference
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• 2010.05a
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• pp.24.1-24.1
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• 2010

In practical operation, the exposed surfaces may get dirty thus degrade the performance of devices. So the combination of self cleaning and antireflection is very desirable for use in outdoor photovoltaic and displaying devices, self cleaning windows and car windshields. For the purpose of self cleaning, the surface needs to be either superhydrophobic or superhydrophilic. However, in practice AR in the visible region and self cleaning are a pair of competitive properties. To satisfy the requirements for superhydrophobic or superhydrophilic surfaces, high surface roughness is required. But it usually cause severely light scattering. Photo-responsive coatings (TiO2, ZnO etc.) can lead to superhydrophilic. However, the refractive indices are high. Thus for porous structure, controlling pore size in the underwavelength scale to reduce the light scattering is very crucial for highly transparent and self cleaning antireflection coating. Herein, we demonstrate a simple method to make high performance broadband antireflection layer on the glass surface, by "carving" the surface by hot alkali solution. Etched glass has superhydrophilic surface. By chemical modification, it turns to superhydrophobic. Enhanced transparency (up to 97%) in a broad wavelength range was obtained by short time etching. Also antifogging effect has been demonstrated, which may offer advantage for devices working at high humidity environment or underwater. Compositional dependence of the properties was observed by comparing three different commercially available glasses.

• Journal of Korean Society on Water Environment
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• v.22 no.5
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• pp.865-870
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• 2006

The behavior and influence of EPS on membrane fouling by changing of hydraulic retention time was investigated, using lab. scale submerged membrane bio-reactor, which was operated with gravitational filtration and fed supernatant of primary sedimentation in waste water treatment plant as influent. The membrane was adopted micro-filter of polyethylene hollow fiber. EPS was analysed as polysaccharides and protein especially, into soluble and bound EPS separately. The concentration of soluble EPS was increased at short HRT, then membrane fouling was rapidly progressed and flux was depressed. The most of EPS clogged membrane pore were polysaccharides, while protein was important parameter affected on membrane fouling because of it's more accumulating in the more term operating.

• Geomechanics and Engineering
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• v.9 no.2
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• pp.243-259
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• 2015

Comparative study has been performed to investigate the behavior of dredged fills on rigid (Model 1) and flexible (Model 2) containers. The study was focused on the sedimentation of soil fills and the development of total stresses. Model 1 is made of an acrylic cylinder and Model two is a scale-size geotextile tube. Results indicate that for rigid containers, significant decrease of the sediment height is apparent during the dewatering process. On the other hand, because the geotextile is permeable, the water is gradually dissipated during the filling process on flexible containers. Hence, significant loss in the tube height is not apparent during the duration of the test. Pressure spikes are apparent on rigid containers during the filling process which can be attributed to the confining effect due to hydrostatic pressure. For the flexible containers, the pressure readings gradually increases with time during the filling process and normalize at the end on the filling stage. No pressure spikes were apparent due to the gradual dissipation of pore water pressure.

• Macromolecular Research
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• v.17 no.9
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• pp.666-671
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• 2009

Water repellent elastomeric surfaces were fabricated successfully on SBS/MWNT nanocomposites films using the breath figure method and subsequent thermal treatment. The uniformly dispersed CNTs were found to play significant roles in tuning the size and ordering of the macroporous morphology at the nanocomposite surface as well as enhancing the mechanical properties of nanocomposites. In particular, the CNTs dispersed in a nanocomposite solution retarded the coarsening process of aqueous droplets during the breath figure process and decreased the pore size in the finally fabricated film. The water contact angle measurement showed that the double-scale structure comprised of self-organized macropores and surface the roughness induced by a thermal treatment produced a highly water-repellent nanocomposite surface.

• Polymer(Korea)
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• v.26 no.6
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• pp.821-828
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• 2002

Regular and highly interconnected macroporous poly(L-lactic acid) (PLLA) scaffolds with pore size of 10∼300 ㎛ were fabricated through thermally induced phase separation of a PLLA-dioxane-water ternary system in the presence of a small amount of Pluronics. Addition of Pluronics to the ternary system raised the cloud-point temperature curve in the order of P-123< F-68< F-127. The Pluronics act as nuclei for the phase separation. This assistance is enhanced with increasing length of the hydrophilic PEO blocks in the Pluronics molecules. Liquid-liquid spinodal phase separation was induced at higher temperatures in the systems containing Pluronics because the spinodal region is raised to higher temperature. The absorption of Pluronics onto the interface stabilizes a macro scale structure and increases the interconnection of pores.

• Proceedings of the Korean Institute Of Construction Engineering and Management
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• 2008.11a
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• pp.804-807
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• 2008

Recently, with the increase of high rise and huge scale building construction, the use of high strength concrete has been increasing. High strength concrete has dense pore structure, which is susceptible to be damaged due to fire attack. For this, many researchers provide proper fire endurance method. In this paper, to provide the priority for selecting fire endurance method in high strength concrete execution, AHP technique is applied based on expert questionnaire. Fire endurance performance efficiency and ordinary performance efficiency was selected for level 1. Fire endurance performance efficiency had larger weight than ordinary one.

• Magazine of the Korean Society of Agricultural Engineers
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• v.39 no.3
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• pp.128-137
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• 1997

In this study, examined influence of consolidation effect that had affected by location of pump inlet that was set collection well for drainage of pore water discharged by embankment on soft ground through the field test. The results of this study are summarized as follows; 1 Initial consolidation curve value were larger than theoritic value, the cause of these phenomena were thought influence of secondary consolidation and three dimensional strain of soft clay. 2. The settlement value of Hosino method was larger than that of Hyperbolic method, but settlement value of Hyperbolic method was accurate more than that of Hosino method in the prediction of settlement. 3. When pump inlet in collection well came down from GL+O.3m to GL-1.5m, settlement value increased about 10cm and when the ground water level was made insitu after pumping had completed , settlement was expanded about 7~8cm. So it is found that location change of pump inlet bad an influence on settlement remarkably. 4. If location of pump inlet in collection well for large scale estate or wide road site is lowered than original ground level, the settlement will be accelerated effectively, and at this stage automatic pump must be used in pumping.

• Journal of Surface Science and Engineering
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• v.35 no.1
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• pp.17-32
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• 2002

Electroplating methods by molten salts and non-aqueous melts were employed for aluminium coating on STS 316L stainless steel. After coated with Ni or non-coated surface on stainless steel, Al pulse plating was carried out in two different types of electrolytes at room temperature. The Al layer from $AlCl_3$-TMPAC melts could not obtain appreciable thickness for engineering application due to chemical reactions between deposits and moisture of air. However, The Al coating by pulse plating in the Ethylbenzene-Toluene-$AlBr_3$ systems was found to be solid coating layer with a few $\mu\textrm{m}$ scale. The conductivity of Ethylbenzene-Toluene-$AlBr_3$ electrolyte was as functions of time and agitation. By seven days exposure after mixing of the electrolyte, Al-deposited layer shows uniform and near by pore-free with high current density (higher than 30mA/$\textrm{cm}^2$). The roughness and imperfection of coating layer were decreased with a increasing agitation speed. It was found that the optimum condition for the Al pulse plating on the 316L stainless steel was a 400mA peak current, duty cycle, $t_{on}$ $t_{ off}$=3ms/1ms, and a current density of 30mA/$\textrm{cm}^2$.

• Journal of the Korean Crystal Growth and Crystal Technology
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• v.3 no.1
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• pp.45-58
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• 1993

Owing to consecutive start of operation of large-scale coal-fired power plants in Korea, the ash production amounts to about 2 million tons per year. The impact of rising disposal costs, looming environmental problems and increased ash tonnages has heightened the concerns about coal ash utilization. The paper mainly describes the correlation between bending strength and microstructure of brick body from fly ash and clay mixture. The results show that bending strength depends mainly on the size and quantity of pore, the sinterability of matrix, and the crack due to the coarse quarts grain, and that the brick body added 15 wt.% fly ash has the best bending strength over the whole firing range.