• The Journal of Advanced Prosthodontics
• /
• v.8 no.4
• /
• pp.259-266
• /
• 2016

PURPOSE. The purpose of this study was to assess the effect of surface treatments on shear bond strength of resin composite bonded to thermocycled and non-thermocycled CAD/CAM resin-ceramic hybrid materials. MATERIALS AND METHODS. 120 specimens ($10{\times}10{\times}2mm$) from each material were divided into 12 groups according to different surface treatments in combination with thermal aging procedures. Surface treatment methods were airborne-particle abrasion (abraded with 50 micron alumina particles), dry grinding (grinded with $125{\mu}m$ grain size bur), and hydrofluoric acid (9%) and silane application. According to the thermocycling procedure, the groups were assigned as non-thermocycled, thermocycled after packing composites, and thermocycled before packing composites. The average surface roughness of the non-thermocycled specimens were measured after surface treatments. After packing composites and thermocycling procedures, shear bond strength (SBS) of the specimens were tested. The results of surface roughness were statistically analyzed by 2-way Analysis of Variance (ANOVA), and SBS results were statistically analyzed by 3-way ANOVA. RESULTS. Surface roughness of GC were significantly lower than that of LU and VE (P<.05). The highest surface roughness was observed for dry grinding group, followed by airborne particle abraded group (P<.05). Comparing the materials within the same surface treatment method revealed that untreated surfaces generally showed lower SBS values. The values of untreated LU specimens showed significantly different SBS values compared to those of other surface treatment groups (P<.05). CONCLUSION. SBS was affected by surface treatments. Thermocycling did not have any effect on the SBS of the materials except acid and silane applied GC specimens, which were subjected to thermocycling before packing of the composite resin.

• Journal of the Korean Ceramic Society
• /
• v.31 no.9
• /
• pp.989-994
• /
• 1994

This study aims at finding the closest packings of regular shape particles such as sphere, circle rod and hexagonal rod type. As the ratio of particle size to container lowered to less than 1/10, the wall effect decreased gradually. The tap density of spherical particles with almost orthorhombic arrangement was 59.5%, while those of circle rod and hexagonal rod type particles were 63.5% and 63.0% respectively. And it was decreased with increasing the aspect ratio of regular particles. The tap density of binary mixtures was larger than that corresponding to the monosized particles packing by about 15%. The tap density of ternary mixtures was larger than that of corresponding to the packing of binary mixtures by about 9%. This work employed the binary mixture of 60% coarse particles and 40% fine particles with size ratio of 1.0 to 1/10 and the ternary mixture of 60% coarse particles, 20% medium and 20% fine particles with size ratio of 1:1/10:1/400 respectively.

• Journal of Korea Technical Association of The Pulp and Paper Industry
• /
• v.36 no.2
• /
• pp.47-53
• /
• 2004

In this experiment the effects of the packing structure of pigment on the surface characteristics (smoothness and gloss) of coated paper are studied. Four different kinds of inorganic pigments(clay), ground calcium carbonate(GCC), two of precipitated calcium carbonates(PCC), and two organic pigments(solid bead and hollow type) were used. The method of measuring the relative sediment volume(RSV) was used to analyze the packing structure of coating layer. The relative sediment volume was measured, using the pressure dewatering dry-cake method(PDDM) and centrifuge method. Also, the particle size distribution of coating pigment was determined. The results showed that small amount of organic pigment, added to inorganic pigment, improved smoothness and its effect was greater when GCC was used as inorganic pigment. The efficiency of organic pigment depended upon the inorganic pigment since the organic pigment is packed in the pores formed by the inorganic pigment.

• Journal of the Korea Academia-Industrial cooperation Society
• /
• v.18 no.1
• /
• pp.715-723
• /
• 2017

This study investigates the properties of a high-performance cementitious composite with partial substitution of stone dust for fine aggregate. The relationship between the properties and particle size distribution was analyzed using several analytical models. Experiments were carried out to examine the flowability, rheology, and strength of cement mortars with different stone-dust replacement ratios of 0-30 wt.%. The results showed improved flowability, lower rheological parameters (yield stress and plastic viscosity), and improved strength as the amount of stone dust increased. These results are closely related to the packing density of the solid particles in the mortar. The effect was therefore estimated by introducing an optimum particle size distribution (PSD) model for maximum packing density. The PSD with a higher amount of stone dust was closer to the optimum PSD, and the optimization was quantified using RMSE. The improvement in the PSD by the stone dust was proven to affect the flowability, strength, and plastic viscosity based on several relevant analytical models. The reduction in yield stress is related to the increase of the average particle diameter when using stone dust.

• Computers and Concrete
• /
• v.11 no.1
• /
• pp.39-49
• /
• 2013

The use of ground fly ash in concrete can increase the risk of slump loss due to the drastic surface change of the particles after the grinding treatment and the accelerated reaction compared to the untreated ash. This study is aimed at the early age hydration and time-dependent rheology changes of cement paste containing ground fly ash. An original fly ash is ground into different fineness and the hydration of cement paste containing the ground fly ash is monitored with the ultrasound propagation method. The zeta potentials of the solid particles are measured and the changes of rheological parameters of the cement pastes with time are analyzed with a rheometer. A particle packing model is used to probe packing of the solid particles. The results show that the early age hydration of the paste is strongly promoted by replacing Portland cement with fly ash up to 30 percent (by mass), causing increase of the yield stress of the paste. The viscosity of a paste containing ground fly ash is lower than that containing the untreated ash, which is explained by the denser packing of the solid particles.

• Journal of the Korean Ceramic Society
• /
• v.34 no.11
• /
• pp.1173-1181
• /
• 1997

Effects of particle size distribution of alumina ceramics on behaviors of tape casting were investigated with emphases on the rheological characteristic of slurry, green density, green sheet strength, and sintering density. For the control of particle size distribution of alumina, the commercial grade low soda alumina, which had different mean particle size of 3.58 ${\mu}{\textrm}{m}$ and 0.42 ${\mu}{\textrm}{m}$, were chosen and blended together. As results, the mixing of 80 wt% fine powder and 20 wt% coarse powder(designated to FC20) led to the increase of packing density and strength of green sheet, and made it easy to handle during processing without lowering of sintering density. Besides, the pseudoplastic behavior of slurry decreased with increase of the fraction of coarse alumina powder.

• Journal of the Korean Ceramic Society
• /
• v.33 no.5
• /
• pp.547-555
• /
• 1996

Porous alumina ceramics were fabricated by pseudo-boehmite phydosol-gel process within/without commercial $\alpha$-alumina particles average 1 and 40 micron respectively. The pore characteristics of fired specimens were studied by the measurement of bulk density total porosity thyermal analysis pore volume pore distribution BET area XRD and SEM. with increasing of firing temperature pore volume and BET surface area were decreased and the average pore size was increased to approximately 146$\AA$ upto 80$0^{\circ}C$ by de-watering of [OH] and formation of $\alpha$-alumina. The fired relative density of the alumina-dispersed specimen with average 1 micron particle was increased with the amounts of dispersed particle by bimodal packing theory which is compared to the ones of specimen including of average 40 micron particle. It was confirmed that the percola-tion threshold in porous ceramics with coarser particle (40 micron) has formed between the transformed-alumina from hydrogel and dispersed-alumina of above 50 vol% particle and the total porosity was increased at the threshold point above.

• Journal of Photoscience
• /
• v.10 no.2
• /
• pp.199-202
• /
• 2003

The relationship between the morphology of nanostructured TiO$_2$ films and the photo-injected electron transport has been investigated using intensity-modulated photocurrent spectroscopy (IMPS). For this purpose, three different TiO$_2$ films with 5 ${\mu}{\textrm}{m}$ thickness are prepared: The rutile TiO$_2$ film with 500 nm-sized cluster-like spherical bundles composed of the individual needles (Tl), the rutile TiO$_2$ film made up of non-oriented, homogeneously distributed rod-shaped particles having a dimension of approximately 20${\times}$80 nm (T2), and the anatase TiO$_2$ film with 20 nm-sized spherically shaped particles (T3). Cross sectional scanning electron micrographs show that all of the TiO$_2$films have a quite different particle packing density: poorly packed Tl film, loosely packed T2 film and densely packed T3 film. The electron transport is found to be significantly influenced by film morphology. The effective electron diffusion coefficient D$_{eff}$ derived from the IMPS time constant is an order of magnitude lower for T2 than for T3, but the D$_{eff}$ for the Tl sample is much lower than T2. These differences in the rate of electron transport are ascribed to differences in the extent of interparticle connectivity associated with the particle packing density.ity.

• Journal of the Korean Magnetics Society
• /
• v.6 no.5
• /
• pp.334-339
• /
• 1996

In order to investigate the influence of the magnetic paticle size and its properties on the particulate magnetic material, we evaluated the dispersion of magnetic particles and the electromagnetic properties in magnetic tape made from the magnetic paints by use of each magnetic particles witch were different from particle size and its propertis. The dispersion of magnetic particles depends on the surface chemical properties rather than particle size. As particle size is smaller, the packing ratio of magnetic particle and the magnetic flux density in tape increase. The output levels in playing back of tape incerase in wide frequency range from 315 Hz to 10 kHz and the noises decrease. It is very important to choose the size, the shape, the surface chemical properties and the magnetic properties of the magnetic particle in producing the high quality magnetic tape.

• Applied Chemistry for Engineering
• /
• v.9 no.6
• /
• pp.852-856
• /
• 1998

Effects of packing materials on the pressure fluctuations in a fluidized bed have been analysed using statistical method to interpret fluidized bed behavior. The experiments were carried out in a fluidized bed of 6.7cm - ID, and the experimental variables were particle size and its distributions, fluidizing velocity, aspect ratio, and packing materials, etc. Screen packings are used as packing material, the properties of the pressure fluctuations in the fluidized bed were measured by a differential pressure transducer. The measured properties for the pressure fluctuations were the mean, the standard deviation, and the major frequency of the power spectral density functions, etc. The standard deviations of the pressure fluctuations have been slightly affected in the radial directions of fluidized bed, and almost constant in axial directions the height above 4.5cm of the distributor of fuidized bed without packing materials. The major frequency decreased with increaing packing size, whereas it showed maximum at 10% of packing materials. It has been found that the standard deviation of the pressure fluctuations can effectively explain the fluidized phenomena, and the packing materials severely affected the properties of the pressure fluctuations.