• Title/Summary/Keyword: parameter characterization

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Preparation and Characterization of KOH-Activated Carbons Developed from Petroleum Coke

  • Sayed Ahmed, S.A.;Abo El-Enin, Reham M.M.;El-Nabarawy, Th.
    • Carbon letters
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    • v.10 no.4
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    • pp.293-299
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    • 2009
  • Potassium hydroxide activated carbons were prepared from Egyptian petroleum cokes with different KOH/coke ratios and at different activation temperatures and times. The textural properties were determined by adsorption of nitrogen at $-196^{\circ}C$. The adsorption of iodine and methylene blue was also investigated at $30^{\circ}C$. The surface area and the non-micropore volume increased whereas the micropore volume decreased with the increase of the ratio KOH/coke. Also the surface area and porosity increased with the rise of activation temperature from 500 to $800^{\circ}C$. Textural parameter considerably increased with the increase of activation time from 1 to 3 h. Further increasing of activation time from 3 to 4 h was associated with a less pronounced increase in textural parameters. The adsorption of iodine shows the same trend of surface area and porosity change exhibited by nitrogen adsorption, with KOH/coke ratio and temperature of activation. Adsorption of methylene blue follows pseudo-first-order kinetics and its equilibrium adsorption follows Langmuir and D-R models.

Effect of Process Parameter on Piezoelectric Properties of PZT Thin films (PZT 박막의 압전특성에 미치는 공정변수의 효과)

  • 김동국;지정범
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.15 no.12
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    • pp.1060-1064
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    • 2002
  • We have studied the effect of crystallization temperature, composition and film thickness, which are the fundamental processing parameters of lead zirconate titanate(PZT) thin film fabrication, in the respect of the piezoelectric properties by our pneumatic loading method(PLM). A great deal of research has been done in the field of characterization for piezoelectric thin films after the first report on the measurement for the piezoelectric coefficient of thin films in 1990. Even though the piezoelectric properties of thin films are very critical factors in the micro-electro mechanical system(MEMS) and thin film sensor devices, a few reports for the piezoelectric characterization are provided for the last decade unlikely the bulk piezoelectric devices. We have found that the piezoelectric properties of thin films are improved as the increase of crystallization temperature up to 750$\^{C}$ and this behavior can be also explained by the analysis of dielectric polarization hysteresis loop, X-ray diffraction and scanning electron microscopy. The effect of Zr/Ti composition has been also studied. This gives us the fact that the maximum piezoelectricity is found near Morphotropic Phase Boundary(MPB) as bulk PZT system does.

Magnetic Flux Leakage (MFL) based Defect Characterization of Steam Generator Tubes using Artificial Neural Networks

  • Daniel, Jackson;Abudhahir, A.;Paulin, J. Janet
    • Journal of Magnetics
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    • v.22 no.1
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    • pp.34-42
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    • 2017
  • Material defects in the Steam Generator Tubes (SGT) of sodium cooled fast breeder reactor (PFBR) can lead to leakage of water into sodium. The water and sodium reaction will lead to major accidents. Therefore, the examination of steam generator tubes for the early detection of defects is an important requirement for safety and economic considerations. In this work, the Magnetic Flux Leakage (MFL) based Non Destructive Testing (NDT) technique is used to perform the defect detection process. The rectangular notch defects on the outer surface of steam generator tubes are modeled using COMSOL multiphysics 4.3a software. The obtained MFL images are de-noised to improve the integrity of flaw related information. Grey Level Co-occurrence Matrix (GLCM) features are extracted from MFL images and taken as input parameter to train the neural network. A comparative study on characterization have been carried out using feed-forward back propagation (FFBP) and cascade-forward back propagation (CFBP) algorithms. The results of both algorithms are evaluated with Mean Square Error (MSE) as a prediction performance measure. The average percentage error for length, depth and width are also computed. The result shows that the feed-forward back propagation network model performs better in characterizing the defects.

Seismic Response Characterization of Shear Wall in Auxiliary Building of Nuclear Power Plant (지진에 의한 원전 보조건물 전단벽의동적 응답 특성 추정)

  • Rahman, Md Motiur;Nahar, Tahmina Tasnim;Baek, Geonhwi;Kim, Dookie
    • Journal of the Earthquake Engineering Society of Korea
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    • v.25 no.3
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    • pp.93-102
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    • 2021
  • The dynamic characterization of a three-story auxiliary building in a nuclear power plant (NPP) constructed with a monolithic reinforced concrete shear wall is investigated in this study. The shear wall is subjected to a joint-research, round-robin analysis organized by the Korea Atomic Energy Research Institute, South Korea, to predict seismic responses of that auxiliary building in NPP through a shake table test. Five different intensity measures of the base excitation are applied to the shaking table test to get the acceleration responses from the different building locations for one horizontal direction (front-back). Simultaneously to understand the global damage scenario of the structure, a frequency search test is conducted after each excitation. The primary motivation of this study is to develop a nonlinear numerical model considering the multi-layered shell element and compare it with the test result to validate through the modal parameter identification and floor responses. In addition, the acceleration amplification factor is evaluated to judge the dynamic behavior of the shear wall with the existing standard, thus providing theoretical support for engineering practice.

Extraction of Extrinsic Circuit Parameters of HEMT by Minimizing Residual Errors (잔차 오차 최소에 의한 HEMT의 외인성 파라미터 추출)

  • Jeon, Man-Young
    • The Journal of the Korea institute of electronic communication sciences
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    • v.9 no.8
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    • pp.853-859
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    • 2014
  • This study presents a technique for extracting all the extrinsic parameters of HEMTs by minimizing the residual errors between a pinch-off cold-FET's gate and drain pad de-embedded Z-parameters and its modeled Z-parameters calculated by the cold-FET's remaining parameters. The presented technique allows us to successfully extract the remaining extrinsic parameter values as well as the gate and drain pad capacitance value without the additional fabrications of the gate and drain dummy pad.

Evaluation of Rapid filtration System with Particle Size Distribution and Turbidity in Different Effective Sizes

  • Park, J.A.;Eo, S.M.;Shin, J.S.;Kim, M.H.;Yu, M.J.;Chung, S.H.
    • Proceedings of the Korean Environmental Health Society Conference
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    • 2005.06a
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    • pp.381-385
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    • 2005
  • Characterization of particle behavior is becoming more important in performance evaluation of water treatment system as well as in operation of the system because conventional parameter, turbidity has lack of explaining ability on small sized microorganisms such like Cryptosporidium etc. Accordingly, particle counter has been introduced in evaluation and operation of the treatment system. However researches on the relationship between turbidity, particle count and/or different sand/anthracite sizes have not been concurrent. Therefore in this study, the relationship was investigated to improve performance evaluation of sand filter so as to help choosing sand/anthracite effective size as a design parameter of water treatment facility. According to the results, too small or too large effective size media filter reached to turbidity limit(0.1 NTU)earlier. However, because shallow sand layer may cause early breakthrough, the depth of sand layer should be provided enough in order to compromise water quality and productivity.

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Identification of isotropic and orthotropic constitutive parameters by FEA-free energy-based inverse characterization method

  • Shang, Shen;Yun, Gun Jin;Kunchum, Shilpa;Carletta, Joan
    • Structural Engineering and Mechanics
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    • v.45 no.4
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    • pp.471-494
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    • 2013
  • In this paper, identification of isotropic and orthotropic linear elastic material constitutive parameters has been demonstrated by a FEA-free energy-based inverse analysis method. An important feature of the proposed method is that it requires no finite element (FE) simulation of the tested material. Full-field displacements calculated using digital image correlation (DIC) are used to compute DIC stress fields enforcing the equilibrium condition and DIC strain fields using interpolation functions. Boundary tractions and displacements are implicitly recast into an objective function that measures the energy residual of external work and internal elastic strain energy. The energy conservation principle states that the residual should be zero, and so minimizing this objective function inversely identifies the constitutive parameters. Synthetic data from simulated testing of isotropic materials and orthotropic composite materials under 2D plane stress conditions are used for verification of the proposed method. When identifying the constitutive parameters, it is beneficial to apply loadings in multiple directions, and in ways that create non-uniform stress distributions. The sensitivity of the parameter identification method to noise in both the measured full-field DIC displacements and loadings has been investigated.

Fabrication and Characterization of Tunable Bandpass Filter using BST Thin Films

  • Kim, Il-Doo;Kim, Duk-Su;Park, Kyu-Sung;Kim, Ho-Gi
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2002.07b
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    • pp.581-584
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    • 2002
  • In this work, a CPW resonator was designed and fabricated to investigate the basic microwave properties, such as effective dielectric constant, of BST thin films. Their properties were used as basic data to simulate and design CPW tunable bandpass filter. We also report on gold/$Ba_{0.5}Sr_{0.5}TiO_3$(BST) ferroelectric thin film C-band tunable bandpass filters(BPFs) designed and fabricated on magnesium oxide substrates using CPW structure. The 2 pole filter was designed for a center frequency of 5.88 GHz with a bandwidth of 9 %. The BST based CPW filter offers a high sensitivity parameter as well as a low loss parameter. The tuning range for the bandpass filter with CPW structure was determined to be 170 MHz.

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Characterization of Pervaporation Membranes and Its Operation Parameters for Alcohol Concentration (알코올 농축을 위한 투과증발막의 특성 및 조업변수 연구)

  • 임군택;김현일;김성수
    • Membrane Journal
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    • v.9 no.2
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    • pp.107-113
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    • 1999
  • Alcohol concentration via pervaporation process was performed by using commercial PDMS(polydimethylsiloxane) composite membrane and plasma treated PP(polypropylene) membranes. Effects of operating parameters of pcrvaporation process were examined. With the increase of butanol concentration in the feed, flux and selectivity increased due to the greater affinity of butanol with PDMS than that of water. As the operating temperature increased, free volume as well as the solubilities and diffusivities of alcohol and water increased to result in the greater flux and less selectivity of the membrane. As solubility parameter difference between alcohol and PDMS membrane decreased, high flux and good selectivity were obtained. When PP membrane was plasma treated with methanol, it has 6 times greater flux than PDMS membrane with equivalent separation factor. With the increase of plasma treatment time, flux and selectivity were enhanced. However, excess treatment time caused pore blocking to result in the flux decrease.

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Creep Characterization of Type 316LN and HT-9 Stainless Steels by the K-R Creep Damage Model

  • Kim, U-Gon;Kim, Seong-Ho;Ryu, U-Seok
    • Journal of Mechanical Science and Technology
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    • v.15 no.11
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    • pp.1463-1471
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    • 2001
  • The Kachanov and Rabotnov (K-R) creep damage model was interpreted and applied to type 316LN and HT-9 stainless steels. Seven creep constants of the model, A, B, $textsc{k}$, m, λ, ${\gamma}$, and q were determine d for type 316LN stainless steel. In order to quantify a damage parameter, the cavity was interruptedly traced during creep for measuring cavity area to be reflected into the damage equation. For type 316LN stainless steel, λ= $\varepsilon$R/$\varepsilon$* and λf=$\varepsilon$/$\varepsilon$R were 3.1 and increased with creep strain. The creep curve with λ=3.1 depleted well the experimental data to the full lifetime and its damage curve showed a good agreement when r=24. However for the HT-9 stainless steel, the values of λ and λf were different as λ=6.2 and λf=8.5, and their K-R creep curves did not agree with the experimental data. This mismatch in the HT-9 steel was due to the ductile fracture by softening of materials rather than the brittle fracture by cavity growth. The differences of the values in the above steels were attributed to creep ductilities at the secondary and the tertiary creep stages.

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