• Title/Summary/Keyword: parameter characterization

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Characteristics of Poly(methylphenyl)silane Photoreists (Poly(methylpheny) Silane Photoresist의 특성)

  • Kang, Doo-Whan;Chung, Nak-Jin
    • Applied Chemistry for Engineering
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    • v.1 no.2
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    • pp.161-167
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    • 1990
  • Polymethylphenylsilane(PMPS) was synthesized with methylphenyldichlorosilane using metal sodium. Various sample coated on quartz plate were exposed and the yield of residual film was calculated. To obtain the fine image forming after developing and drying, optical transmittance characterization have to be considered. Exposure is described by three optical parameters X, Y, and Z. There parameters are normally determined from optical transmittance measurements of exposed PMPS films. Z parameter was determined from the initial slope of a transmittance according to exposure time. This set of function parameters provided a complete description of photoresist exposure and development and became the basis for the theoretical process models.

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Synthesis and Characterization of ZnAl2O4 Nanopowders by a Reverse Micelle Processing

  • Hoon, Son-Jung;Sohn, Jeongho;Shin, Hyung-Sup;Bae, Dong-Sik
    • Korean Journal of Materials Research
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    • v.25 no.11
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    • pp.598-601
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    • 2015
  • Using reverse micelle processing, $ZnAl_2O_4$ nanopowders were synthesized from a mixed precursor(consisting of $Zn(NO_3)_2$ and $Al(NO_3)_3$). The $ZnAl_2O_4$ was prepared by mixing the aqueous solution at a molar ratio of Zn : Al = 1 : 2. The average size and distribution of the synthesized powders with heat treatment at $600^{\circ}C$ for 2 h were in the range of 10-20 nm and narrow, respectively. The average size of the synthesized powders increased with increasing water to surfactant molar ratio. The XRD diffraction patterns show that the phase of $ZnAl_2O_4$ was spinel(JCPDS No. 05-0669). The synthesized and calcined powders were characterized using a thermogravimetric - differential scanning calorimeter(TG-DSC), X-ray diffraction analysis (XRD), and high resolution transmission electron microscopy(HRTEM). The effects of the synthesis parameter, such as the molar ratio of water to surfactant, are discussed.

Growth and characterization of YBa2Cu3O7-$\delta$ thin films using pulsed laser (펄스레이저 증착에 의한 YBa2Cu3O7-$\delta$박막의 성장과 특성분석)

  • Chung, J.K.;Ko, R.K.;Choi, S.J.;Song, K.J.;Park, C.
    • Proceedings of the Korea Institute of Applied Superconductivity and Cryogenics Conference
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    • 2003.02a
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    • pp.117-119
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    • 2003
  • YBa$_2$Cu$_3$O$_{7-{\delta}}$(YBCO) high temperature superconducting thin films were grown on SrTiO$_3$single crystal substrates by pulsed laser deposition(PLD). The texture and lattice parameter of the YBCO films were analysed using the GADDS (general area detector diffraction system) which enables XRD analyses to be done faster and with fewer sample movement than with the XRD system with point detector. The XRD results of the films grown in different deposition conditions are reported together with the SEM microstructure analysis results.ysis results.

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Estimation of Energetic and Charge Transfer Properties of Iridium(III) Bis(2-phenylpyridinato-N,C2')acetylacetonate by Electrochemical Methods

  • Cha, Joeun;Ko, Eun-Song;Shin, Ik-Soo
    • Journal of Electrochemical Science and Technology
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    • v.8 no.2
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    • pp.96-100
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    • 2017
  • Iridium(III) bis(2-phenylpyridinato-$N,C^{2^{\prime}}$)acetylacetonate ($(ppy)_2Ir(acac)$), a green dopant used in organic light-emitting devices (OLEDs), was subjected to electrochemical characterization to estimate its formal oxidation potential ($E^{o^{\prime}}$), HOMO energy level ($E_{HOMO}$), electron transfer rate constant ($k^{o^{\prime}}$), and diffusion coefficient ($D_o$). The employed combination of voltammetric methods, i.e., cyclic voltammetry (CV), chronocoulometry (CC), and the Nicholson method, provided meaningful insights into the electron transfer kinetics of $(ppy)_2Ir(acac)$, allowing the determination of $k^{o^{\prime}}$ and $D_o$. The quasi-reversible oxidation of $(ppy)_2Ir(acac)$ furnished information on $E^{o^{\prime}}$ and $E_{HOMO}$, allowing the latter parameter to be easily estimated by electrochemical methods without relying on expensive and complex ultraviolet photoemission spectroscopic (UPS) measurements.

Synthesis and Characterization of Brilliant Yellow Color Pigments using α-FeOOH Nanorods (α-FeOOH 나노로드를 이용한 선명한 황색 안료 합성 연구)

  • Yun, JiYeon;Yu, Ri;Kim, YooJin
    • Journal of Powder Materials
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    • v.23 no.6
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    • pp.453-457
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    • 2016
  • In this work, we synthesize brilliant yellow color ${\alpha}$-FeOOH by controlling the rod length and core-shell structure. The characteristics of ${\alpha}$-FeOOH nanorods are controlled by the reaction conditions. In particular, the length of the ${\alpha}$-FeOOH rods depends on the concentration of the raw materials, such as the alkali solution. The length of the nanorods is adjusted from 68 nm to 1435 nm. Their yellowness gradually increases, with the highest $b^*$ value of 57 based on the International Commission on Illumination (CIE) Lab system, by controlling the nanorod length. A high quality yellow color is obtained after formation of a silica coating on the ${\alpha}$-FeOOH structure. The morphology and the coloration of the nal products are investigated in detail by X-ray diffraction, scanning electron microscopy, UV-vis spectroscopy, and the CIE Lab color parameter measurements.

Characterization of Non-linear Consolidation of Dredged Soil from Incheon Area (인천 지역 준설토의 비선형 압밀특성 연구)

  • Oak, Young-Suk;An, Yong-Hoon;Lee, Chul-Ho;Choi, Hang-Seok
    • Proceedings of the Korean Geotechical Society Conference
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    • 2008.10a
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    • pp.1693-1706
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    • 2008
  • It is of importance to determine the zero effective stress void ratio($e_{00}$), which is the void ratio at effective stress equal to zero, and the relationships of void ratio-effective stress and of void ratio-hydraulic conductivity for characterizing non-liner finite strain consolidation behavior for ultra-soft dredged materials. The zero effective stress void ratio means a transitional status from sedimentation to self-weight consolidation of very soft soil deposits, and acts as a starting point for self-weight consolidation in the non-linear finite strain numerical analysis such as PSDDF. In this paper, a new method for determining the zero effective stress void ratio has been introduced with the aid of measuring electrical resistivity of the specimen. A correlation between the zero effective stress void ratio and the initial slurry void ratio has been proposed, which can be used in PSDDF analysis as an input parameter. Combining all of the accessible experimental data, the consolidation characteristics of a dredged soil from the Incheon area has been studied in detail.

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The Characterization and Analysis of the simulated meander inductor for RF application (RF 응용을 위한 meander 인덕터의 특성 및 분석연구)

  • Kim, Sung-Hoon;Lee, Yong-Jun;Chang, Kun-Hyuk;Koh, Jung-Hyuk
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2008.06a
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    • pp.352-352
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    • 2008
  • 폐 자기회로 구조를 갖는 Meander 형태의 Inductor 설계를 위해 HFSS 프로그램을 이용하여 Meander Inductor를 시뮬레이션 하였다. Meander Inductor의 turn 수(N) 및 폭(W), 두께(T), 랩(G)의 변화에 따른 인덕턴스(L), S-parameter(S)와 Q-factor(Q)의 변화를 HFSS 를 통해 측정하였다. Al2O3 기판과 MgO의 두께는 각각 680um, 50um로 고정하였고, silver electrode를 이용하여 Meander 타입의 Inductor를 설계하였다. Meander Inductor의 turn수(6,7,8turn)의 변화를 측정한 결과, 8턴이었을 때 Q-factor가 19로서 가장 높은 결과를 얻었다. L의 결과 값은 공진 주파수와 의 관계에 의해 6turn일 때 L값은 17GHz에서 공진현상이 나타났다. 또한 W, G, T에 변화를 주어 설계한 뒤 시뮬레이션의 결과 값을 측정하였다. 그 값을 서로 비교한 결과, 변수들의 변화에 따라 L값과 Q-factor가 변화되었다. 이 논문에서는 각 변수에 따른 meander inductor의 특성을 HFSS 시뮬레이션을 통해 비교하고자 한다.

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The Simulation and Characterization of Interdigital Capacitor for Microwave Applications (마이크로 웨이브 응용을 위한 Iterdigital 캐패시터의 시뮬레이션 및 특성분석)

  • Woo, Tae-Ho;Yoon, Sang-Oh;Koh, Jung-Hyuk
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2008.06a
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    • pp.353-353
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    • 2008
  • 트랜지스터 속도는 현저하게 향상되어지는 반면에 RFICs(RF integrated circuits)는 대용량화, 고속화, 고집적화, 소형화, 고 효율화 온칩(on-chip) 수동소자의 부재에 의해 발전을 이루지 못하였다. 즉, 최근 전자기기의 집적화, 초소형화 됨에 따라 실장 밀도를 높이기 위해 부품의 소형화가 강하게 요구되는 동시에 Radio Frequency(RF)에서 이용가능한 수동소자인 capacitor를 개발하고자 본 논문에서는 손가락 모양(interdigital configuration)을 갖는 RF capacitor를 Ansoft사의 HFSS를 이용하여 이상적인 S-parameter, 정전용랑(capacitance), 손실계수(loss tangent)를 도출하고자 한다. 680um의 $Al_2O_3$ 기판에 BST doped MgO을 30um, Chromium과 gold를 각각 5um로 증착시켰다. 핑거 개수 (n, number), 핑거 길이(1, length), 핑거 간격(g, gap), 핑거 너비(w, width)를 변화 시켜가면서 이상적인 결과 값에 가까운 모양 (interdigital configuration)을 얻을 수 있었다. 핑거 수 3 개 일 때 입력 값에 대하여 손실 없는 출력 값(투과값)을 갖는 $S_{21}$이 1.5GHz에서 6dB이하로 떨어졌으며 핑거 간격이 줄고 핑거 너비가 커지고 핑거길이가 커질수록 높은 캐패시턴스 값을 갖는 것을 확인 할 수 있었다.

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Characterization of Al-doped ZnO Thin Films by Atomic Layer Deposition (원자층 증착법으로 증착한 Al을 도핑한 ZnO 박막의 특성평가)

  • Shin, Woong-Chul;Choi, Kyu-Jeong
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2008.06a
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    • pp.175-175
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    • 2008
  • 투명전극으로 사용되고 있는 Indium tin oxide (ITO) 박막은 전기적 전도도와 기판과의 접확성, 화학적 안정성, 광투과율 등의 특성과 함께 우수한 전기 광학적 거동을 보이고 있다. 그러나 ITO는 고가의 재료이기 때문에 대체 투명전극으로 Al을 도핑한 ZnO 박막의 연구가 활발히 진행되고 있다. ZnO:Al 박막은 chemical vapor deposition, reactive magnetron sputtering, electron-beam evaporation, pulsed laser deposition 등의 당양한 방법을 이용하여 증착하였다. 그러나 최근 낮은 온도에서 대면적의 균일성과 우수한 특성 때문에 atomic layer depositon (ALD) 방법을 이용하여 많은 연구가 진행되고 있으며, 이런 투명전극은 태양전지를 위해 연구되어지고 있다. 따라서 본 연구에서는 ALD 방법으로 Al의 도핑 양을 조절하여, ZnO:Al 박막을 제조하여 그 특성을 평가하고, 또한 ZnO TFT를 제작하여 발표하고자 한다. ZnO와 ZnO:Al 박막은 실리콘과 유리 기판 위에 ALD (Lucida-D200, NCD Technology) 장치로 증착하였다. DEZn, TMA, $H_2O$는 ZnO와 ZnO:Al 박막을 증착하기 위한 전구체와 반응가스로 사용하였다. 증착된 박막은 XRD와 HRTEM을 이용하여 결정구조와 미세구조를 분석하였다. AFM과 4-point probe를 이용하여 증착된 박막의 표면 거칠기와 면저항을 관찰하였다. semiconductor parameter 분석기를 이용하여 제작된 ZnO TFT를 평가하였다.

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Characterization and Field Measurements of NB-PLC for LV Network

  • Masood, Bilal;Ellahi, Manzoor;Khan, Waheed Aftab;Akram, Waqar;Usman, Muhamad;Gul, Muhammad Talha
    • Journal of Electrical Engineering and Technology
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    • v.13 no.1
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    • pp.521-531
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    • 2018
  • This paper presents a procedure for field measurements which provides a generalized Narrowband Power Line Communications (NB-PLC) channel model for low voltage (LV) access network in order to deploy advanced metering infrastructure (AMI) within Lahore, Pakistan. The measurements of allocated sites were performed in the residential (urban and rural), industrial and commercial electricity consumers for the NB-PLC channel modeling of overhead transmission lines (TLs). On the basis of extensive field measurement results, the average attenuation profile and transfer functions are presented. The results obtained from field measurements are validated by comparing them with a proposed Simulink model. A close agreement in the measured and simulated transfer function (TF) results is observed. The proposed Simulink model is an effort to model the NB-PLC channels in an effective way, especially in South Asian countries.