• Title/Summary/Keyword: p-dodecylaniline

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The Synthesis of p-Dodecylbenzylidene-p'-hexyloxyaniline (p-Dodecylbenzylidene-p'-hexyloxyaniline의 합성)

  • Jeong, Noh-Hee;Kwack, Kwang-Soo
    • Journal of the Korean Applied Science and Technology
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    • v.20 no.3
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    • pp.198-203
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    • 2003
  • In this study, we synthesized p-hexyloxybenzaldehyde(HBA) by using p-hydroxybenzaldehyde and n-hexylchloride. p-dodecylaniline(DDA) prepared by nitration and reduction of dodecylbenzene. The schiff base, p-dodecylbenzylidene-$p^\prime$-hexyloxyaniline (DBHA) was synthesized by reaction of HBA and DDA. The color of synthetic compound was pale-brown and the yield was 62%. All the synthetic compounds were identified by TLC, FT-IR and ${^{i}H}$-NMR.In this study, we synthesized p-hexyloxybenzaldehyde(HBA) by using p-hydroxybenzaldehyde and n-hexylchloride. p-dodecylaniline(DDA) prepared by nitration and reduction of dodecylbenzene. The schiff base, p-dodecylbenzylidene-p'-hexyloxyaniline(DBHA) was synthesized by reaction of HBA and DDA. The color of synthetic compound was pale-brown and the yield was 62%. All the synthetic compounds were identified by TLC, FT-IR and $^1H$-NMR.