• Title/Summary/Keyword: organic content

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Centrifugal Liquid Chromatography with Application of the N-hexadecyl-L-proline Coated Reversed Phase for Separation of amino Acid Enantiomers (N-hexadecay-L-proline이 코팅된 역상 원심 액체크로마토그래피에 의한 아미노산 이성질체의 분리)

  • Sun Haing Lee;Tae Sub Oh;Hae Woon Lee
    • Journal of the Korean Chemical Society
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    • v.36 no.6
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    • pp.849-856
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    • 1992
  • We prepared a simple, economic and versatile preparative system for an enantiomeric separation. Hydrophobic amino acid enantiomers were resolved in the preparative scale by a centrifugal liquid chromatography on the N-hexadecyl-L-proline coated reversed phase. The factors controlling the retention and resolution of racemic amino acids such as the concentration of Cu(Ⅱ), pH of the eluent, the type and content of organic modifier, and rpm of CLC were examined. Several mg of hydrophobic amino acid enantiomers were separated preparatively. To separate all of different amino acid enantiomers, various coating material will be investigated.

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Fabrication and Magnetic Properties of A New Fe-based Amorphous Compound Powder Cores

  • Xiangyue, Wang;Feng, Guo;Caowei, Lu;Zhichao, Lu;Deren, Li;Shaoxiong, Zhou
    • Journal of Magnetics
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    • v.16 no.3
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    • pp.318-321
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    • 2011
  • A new Fe-based amorphous compound powder was prepared from Fe-Si-B amorphous powder by crushing amorphous ribbons as the first magnetic component and Fe-Cr-Mo metallic glassy powder by water atomization as the second magnetic component. Subsequently by adding organic and inorganic binders to the compound powder and cold pressing, the new Fe-based amorphous compound powder cores were fabricated. This new Fe-based amorphous compound powder cores combine the superior DC-Bias properties and the excellent core loss. The core loss of 500 kW/$m^3$ at $B_m$ = 0.1T and f = 100 kHz was obtained When the mass ratio of FeSiB/FeCrMo equals 3:2, and meanwhile the DC-bias properties of the new Fe-based amorphous compound powder cores just decreased by 10% compared with that of the FeSiB powder cores. In addition, with the increasing of the content of the FeCrMo metallic glassy powder, the core loss tends to decrease.

A Basic Study on Growth Characteristics of Dendropanax morbifera in Southern Part of Korea

  • Choi, Seong-Kyu
    • Plant Resources
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    • v.3 no.2
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    • pp.148-151
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    • 2000
  • This study was carried out obtain basic information for growth characteristics by different age of Dendropanax morbifera in southern part of Korea, such as at Sunchon, Haenam, Gangjin, Wando. The pH of soil in cultivation area was 5.2 to 5.6 and organic matter was very high up to 10.6%. P$_{2}$O$_{5}$, content of soil in cultivation area was 35.3 to 42.1 mg/1, C.E.S was 13.9 to 14.4 me/100g, and moisture rate was 19.2 to 21.1 %. The flowering of Dendropanax morbifera began from 6~7 years old tree. The flowering date was at 10th of July at Wando. The growth characteristics of 12 years old tree was 929.5cm in stem height, 134.1mm in stem diameter, and 15 years old tree was 1,117.9cm in stem height, 160.8mm in stem diameter. The number of leaf was 13.9 at five years old tree, and the petioles length was 12.6 at five years old tree. Xylem sap can be had at more than 10 years old tree with good growth more than 10 cm stem diameter.r.

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Study on Antioxidant and Cytotoxic Activities in Ethanol Extract from Prunus mume (오매 에탄올 추출물의 항산화 활성 및 항암 활성 연구)

  • Jeon, Yeon-Hee;Kwon, Ji-Eun;Kim, Mee-Ra
    • Journal of the East Asian Society of Dietary Life
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    • v.20 no.5
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    • pp.751-758
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    • 2010
  • Prunus mume is well known contain many functional materials that play beneficial roles in the human body. Studies have found that many organic acids and polyphenol compounds exist in Prunus mume. In this study, content of total polyphenols and flavonoids, antioxidative activity and cytotoxicity of ethanol extract from Prunus mume were measured Contents of total polyphenolic and total flavonoid compounds in ethanol extract from Prunus mume were 16.92 mg/g and 59.95 mg/g, respectively. The $IC_{50}$ of ethanol extract from Prunus mume were $237.72 {\mu}g$/assay and $239.58 {\mu}g$/assay by DPPH and ABTS radical cation scavenging test, respectively. Additionally, ferric ion reducing antioxidant power (FRAP) value of ethanol extract from Prunus mume was 0.94 mM ($FeSO_4$ eq.) by $800 {\mu}g$/assay. Cytotoxicity of Prunus mume against five kinds of cancer cell lines increased as the extract concentration increased Especially, cytotoxicity of the ethanol extract against A-549 (lung cancer line) was higher than that against any other cancer cell line by both MTT and SRB assay. These results show that ethanol extract of Prunus mume has considerably high antioxidative and cytotoxic activities.

The effect of propolis concentration on the antibacterial activity (프로폴리스 농도가 항균활성에 미치는 영향)

  • Kim, Byoung-Moon;Song, Kun-Ho;Lee, Kwang-rae
    • Journal of Industrial Technology
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    • v.27 no.B
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    • pp.161-167
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    • 2007
  • The objetives of this study are to set up optimum extraction temperature, time and organic solvent for propolis extraction, to investigate chemical properties, and to develop health foods from propolis preparation. In this study, ethanol and ultrasonic extracts method performed to optimum extraction temperature was at 60, $20^{\circ}C$, optimum extraction time was at 12, 4 hours and optimum extraction amount of solvent was at 20, 15 times of propolis weight. When various ethanol solutions were used, whereas flavonoid content was highest in 70, 80% aqueous ethanol, respectively. So the ultrasonic extracts method used gave better results than the ethanol extracts method in this work. Extraction of propolis with etanol and ultrasonic extracts method was performed by using the water and various concentrations of aqueous ethanol as solvent. Sensitivity of propolis samples to Staphylococcus aureus was investigated and the results were shown. Samples of water extract did not inhibit microbial growth, where as 50% aqueous ethanol extract the largest inhibitory zone for Staphylococcus aureus, then decreased inhibition with increasing ethanol concentrations.

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Linkage of Agricultural Research and Extension in Paraguay - Interview to Key Actors - (파라과이 농업연구와 지도의 연계 - 핵심 담당자 인터뷰 -)

  • Park, Duk-Byeong;Ma, Sang-Jin
    • Journal of Agricultural Extension & Community Development
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    • v.23 no.2
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    • pp.181-193
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    • 2016
  • The linkages between agricultural research and extension are important to enhance farmers' competence. The objectives of the study were to explore the linkage between research and extension for the family farm. Data including quantitative and qualitative were obtained from the key actors about the public management regarding linkage which were the method, the topic of the agricultural technology dissemination, and the agricultural research topics. Results show that the main structural problems of the agricultural technology dissemination were technical support services, credit services, and farm planning and infrastructure deficit. Furthermore, as for the topics or content of agricultural technology dissemination, organic agriculture, soil management and conservation, agricultural credit, organizational strengthening, marketing, participatory research, dissemination of technology, equipment, infrastructure and agricultural mechanization were preferred.

Effect of Organic Content on Anaerobic Biodegradability by Agricultural Waste Biomass

  • Shin, Kook-Sik;Yoon, Young-Man;Sonn, Yeon-Kyu
    • Korean Journal of Soil Science and Fertilizer
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    • v.47 no.3
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    • pp.155-164
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    • 2014
  • Recently interest on production of biogas from biomass resources has increased because of climate change in worldwide. In this study, anaerobic digestion efficiency of 17 different types of agricultural waste was evaluated using biochemical methane production potential estimated from the International biochemical methane potential standard method (Germany VDI4630). As a result, theoretical biochemical methane potential ($B_{th}$) of agricultural waste biomass ranged from 0.266 to $0.488Nm^3kg^{-1}$-Volatile Solid $(VS)_{added}$. Ultimate biochemical methane potential ($B_u$) of agricultural waste biomass ranged between 0.176 and $0.417Nm^3kg^{-1}-VS_{added}$. The agricultural waste biomass anaerobic biodegradability with $B_u/B_{th}$ and VDI4630 determined by VS contents was 36.0~95.9% and 30.8~91.1%, respectively. Ultimate methane potential and anaerobic biodegradability given by the VS term showed more reasonable results.

Effect of FTO coated on stainless steel bipolar plate for PEM fuel cells

  • Park, Ji-Hun;Jang, Won-Yeong;Byeon, Dong-Jin;Lee, Jung-Gi
    • Proceedings of the Materials Research Society of Korea Conference
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    • 2009.05a
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    • pp.55.2-55.2
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    • 2009
  • A polymer electrolyte membrane (PEM) fuel cell has been getting large interest as a typical issue in useful applications. The PEMFC is composed of a membrane, catalyst and the bipolar plate. SnOx:F films on SUS316 stainless steel were prepared as a function of substrate with using electron cyclotron resonance-metal organic chemical vapor deposition (ECR-MOCVD) in order to achieve the corrosion-resistant and low contact resistance bipolar plates for PEM fuel cells. The SnOx:F films coated on SUS316 substrate at surface plasma treatment for excellent stability, before/after heat treatment for good crystalline structure and microwave power for were characterized by X-ray diffraction (XRD), auger electron microscopy (AES) and field emission-scanning electron microscopy (FE-SEM). The SnOx:F film coated on SUS316 substrate with various process parameters were able to observe optimum interfacial contact resistance (ICR) and corrosion resistance. It can be concluded that fluorine-doping content plays an important function in electrical property and characteristic of corrosion-protective film.

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Reinforcement of Calcium Phosphate-Calcium Sulfate Injectable Bone Substitute Using Citric Acid and Hydroxypropyl-Methyl-Cellulose

  • Thai, Van Viet;Kim, Min-Sung;Song, Ho-Yeon;Lee, Byong-Taek
    • Proceedings of the Materials Research Society of Korea Conference
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    • 2009.05a
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    • pp.45.1-45.1
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    • 2009
  • In this study, we investigated a calcium phosphate-calcium sulfate injectable bone substitute (IBS) with organic reinforcement of chitosan, citric acid and hydroxypropyl-methyl-cellulose (HPMC). The powder component of IBS consisted of tetra calcium phosphate (TTCP), dicalcium phosphate dihydrate (DCPD) and calcium sulfate dihydrate (CSD). The liquid component was a solution of citric acid and chitosan. The effect of HPMC in terms of setting time, compressive strength and apatite forming ability on this IBS was investigated. The mass content of HPMC in liquid phase was varied in array of 0%, 2%, 3% and 4%. The setting times obtained between 20 and 45 minutes. Compressive strength was achieved over 20 MPa after incubation at 370C and in 100% humidity for 28 days. Porosities were evaluated in relation with compressive strength. Elastic moduli of the 28 days after-incubation IBS were obtained around 4GPa

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Monthly Variation in the Salmonella Mutagenicity by Suspended Particulate according to Particle Size in Seoul City (서울시 대기중 부유분진의 입도별 돌연변이원성의 월변화)

  • Jang, Jae-Yeon;Kim, Bak-Kwang;Jo, Seong- Joon;Chung, Yong
    • YAKHAK HOEJI
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    • v.32 no.5
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    • pp.362-369
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    • 1988
  • Monthly variation of mutagenicity by airborne particulate were studied according to particle size of the particulate. Airborne particulates were collected in Shinchon of Seoul which is commocial and traffic area in 1986. And those were separately collected into two parts such as fine particle (less than $2.5{\mu}m$ aerodynamic diameter) and coarse particle (greater than $2.5{\mu}m$). Extractable organic matters(EOM) were extracted and mutagenicity of the EOM was tested in Salmonella thyphimurium TA 98 by Ames method. While the concentration of coarse particle did not show the seasonal variation, that of fine particle showed great seasonal variation. The contents and mutagenicity of EOM in fine particles were higher than those of coarse particles. So fine particles were expected to contribute to the 90% of mutagenicity in atmosphere by suspended particulates. The content of EOM and mutagenicity by suspended particulates in atmosphere were highest in January all the year around and also higher as much as 6 and 30 times than in July, respectively.

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