• 한국식생활문화학회지
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• 제12권3호
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• pp.265-274
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• 1997

This study was conducted in ordor to find the most suitable conditions for producing the Doenjang with optimal odor compound contents. Three sample groups with the different preparing methods -Doenjang that has not gone through the soy sauce separation process (Doenjang A), Doenjang that has gone through the soy sauce separation process; Meju-20% salt water ratio of 1 : 4 (Doenjang B), and that with the ratio of 1.3 : 4 (Doenjang C)- were tested during different ripening periods. Odor compound contents were analyzed through Solvent Extraction Method and Simultaneous Steam Distillation Extraction (SDE). The number of odor compounds was greatest in Doenjang A and during the mid to late stage in each groups. In the sensory evaluation of Doenjang odors, Doenjang A received the highest scores in the categories of overall preferences, while Doenjang C got the lowest scores. Individual odor didn't vary significantly during ripening periods, but the overall odor and taste preference was highest in the samples ripened for 75 to 120 days. Stepwise multiple regression analysis of major odor compounds of Doenjang revealed that benzeneacetaldehyde is the major explanatory variable for offensive odor. Benzeneethanol, 3-methylthio-propanal and 4-methyl-phenol are the explanatory variables for salty odor, nutty odor and rancid odor, respectively. Odor compounds that contribute to the overall odor preference varied from the compounds that affect the taste preference.

• 한국수산과학회지
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• 제35권6호
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• pp.696-701
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• 2002

Cellulase를 이용하여 키토산 올리고당을 제조하기 위한 최적조건을 반웅표면 분석법을 이용하여 설정하였다 키토산 분해능과 산업적 활용의 측면에서 유리한 Pen. funiculosum 유래의 cello-lase를 예비 실험을 통해 결정하였다. 이 효소의 적정 반응 조건에서 경시적 키토산 분해율을 측정한 결과, 반응 10시간까지는 대수적 증가를 보였으나, 10시간 이후로는 완만한 분해율을 나타내었다. 중심합성계획에 의해 총 26개의 실험을 행한뒤 반응표면분석법으로 설정한 키토산 분해 최적 조건은 기질 농도 $0.5\%$에 대해 효소 농도 143(U), 반응 온도 $49^{\circ}$, 반응 시간 13.2hr및 pH는 3.8이었다. 본 연구에서 설정된 최적의 조건에서 얻어진 키토산 분해물은 dimer와 trimer가 주된 올리고당이었고, 소량의 tetramer와 hexamer 그리고 monomer 등의 총 8종 정도의 올리고당이 검출되었다.

• 대한토목학회논문집
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• 제38권1호
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• pp.167-174
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• 2018

본 연구는 현실 적용성을 고려한 버스 최적 배차간격 모형 구축을 통해 현실적 운행계획 작성에 기여하고자 한다. 부산시가 제시한 시내버스 운행계획의 적정성 검토를 통해, 배차간격 및 운행시간이 현실적 여건을 고려하지 않고 계획되어 있음을 파악하였다. 이에 실제 도로 여건과 운행환경을 고려한 운행시간 제약조건과 해당 노선의 수요 충족을 위한 시간대별 배차간격 도출 모형을 구축하였고 부산시 10번과 27번 노선을 사례로 모형의 적용성을 검증하였다. 본 연구는 교통카드 및 BIMS (Bus Information Management System)가 제공하는 방대한 자료(Big-Data)로부터 필요 정보를 추출하였으며, 그 과정에서 분석에 필요한 자료와 정보 추출 과정도 요약 제시하였다. 본 연구의 결과는 현실적 운행계획 작성과 향후 보다 정밀한 여건을 고려한 연구에 기여할 것으로 기대한다.

• 동아시아식생활학회지
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• 제18권2호
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• pp.190-197
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• 2008

The aim of this study was to determine the optimal cooking conditions in preparing jujube concentrates using various boiling times (5, 10, 15, 20 hours). The moisture contents of the concentrate samples ranged from 38.86 to 42.36%. Crude protein content was highest in the 15 hr-boiled concentrate, crude fat was highest in the 20 hr-boiled concentrate and both the 15 and 20 hr boiled concentrates had high crude fiber contents. There were no differences in color L- and a-values by boiling time; however, the b-value decreased with increasing boiling time. The pH levels of the concentrates ranged from 5.24 to 5.27, and the brix level increased with increasing boiling time. Glucose was the primary of free sugar in the concentrates and its highest level was 102.3 ${\mu}M$ in the 20 hr-boiled concentrate. The 15 hr-boiled concentrate had the highest electron donating ability to 46.68%. The total polyphenol contents of the concentrates ranged from 21.53 to 24.56%, in which the 15-boiled concentrate had the highest level (24.56%). In the sensory evaluation, the 15-hr-boiled concentrate again performed well, showing the highest overall acceptability scores. From these results, 15 hrs was the optimal boiling time for preparing jujube concentrate in terms of obtaining functional compounds and overall product acceptability.

• 한국건설관리학회논문집
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• 제20권1호
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• pp.133-140
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• 2019

콘크리트 타설현장의 조건은 콘크리트 강도에 커다란 영향을 주며, 따라서 콘크리트 배합은 콘크리트 타설시 현장조건을 반영할 수 있도록 설계되어야 한다. 즉, 콘크리트 배합은 현장양생온도, 작업환경, 타설방법 등을 고려하여 최적화하는 노력이 필요하다. 본 연구목적은 현장 콘크리트 타설시 발생하는 양생온도와 작업지연 등 외부영향인자를 고려하여 가장 대응을 잘 할 수 있는 콘크리트 배합설계를 제공하는 것이다. 연구목적을 달성하기 위해서 본 연구에서는 로버스트 설계방법을 콘크리트 배합설계에 적용했다. 사례분석에서는 양생온도와 작업지연 등 외부영향요인과 함께 콘크리트 성분의 조합을 적용하여 콘크리트 실내 테스트를 실시했다. 실험결과 로버스트 설계방법을 적용할 경우 외부영향요인이 주어 졌을 때 가장 효과적으로 대응을 할 수 있는 콘크리트 배합설계를 선정할 수 있다는 것을 알 수 있었다.

• Korean Chemical Engineering Research
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• 제61권2호
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• pp.322-327
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• 2023

A design of experiments was evaluated in optimizing MOF-5 synthesis for acetylene adsorption. At first, mixture design was used to optimize precursor concentration, terephthalic acid, zinc acetate dihydrate and N,N-dimethylformamide. More specifically, 13 conditions with various molar ratios were designed by extreme vertices design method. After preparing the samples, XRD, N₂ physisorption and SEM analysis were performed for their characterization. Moreover, acetylene adsorption experiments were carried out over the samples under identical conditions. The optimal precursor composition for MOF-5 synthesis was predicted on a molar basis as follows: terephthalic acid : acetate dihydrate : dimethylformamide = 0.1 : 0.4 : 0.5. Thereafter, multi-level factorial design was designated to investigate the effect of synthesis reaction conditions such as temperature, time and stirring speed. By the statistical analysis of 18 samples designed, 4 reaction parameters were determined for additional adsorption experiments. Therefore, MOF-5 prepared under the synthesis time and temperature of 100 ℃ and 12 h, respectively, showed the maximum adsorption capacity of 15.1 mmol/g.

• 한국응용과학기술학회지
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• 제28권1호
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• pp.85-94
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• 2011

Expanded graphites were used as anode materials of high power Li-ion secondary battery. The expanded graphite was prepared by mixing the graphite with $HClO_4$ as a intercalation agents and $KMnO_4$ as a oxidizing agents. The physical and electrochemical properties of prepared expanded graphites through the variation of process variables such as contents of intercalation agent and oxidizing agent, and heat treatment temperature were analyzed for determination of optimal conditions as the anode of high power Li-ion secondary battery. After examing the electrochemical properties of expanded graphites at the different preparing conditions, the optimal conditions of expanded graphite were selected as 8 wt.% of oxidizing agent, 400 g of intercalation agent for 20 g of natural graphite, and heat treatment at $1000^{\circ}C$. The sample showed the improved charge/discharge characteristics such as 432 mAh/g of initial reversible capacity, 88% of discharge rate capability at 10 C-rate, and 24 mAh/g of charge capacity at 10 C-rate. However, the expanded graphite had the problems of potential plateaus like natural graphite and lower initial efficiency than the natural graphite.

• Bulletin of the Korean Chemical Society
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• 제31권9호
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• pp.2575-2580
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• 2010

We present a method for chemically reducing silver alkylcarbamate complex with hydrazine to synthesize silver nanocolloids in an organic solvent using polyvinylpyrrolidone (PVP) as the stabilizer. To determine the optimal conditions for preparing stable silver colloids of controlled size and shape, the silver 2-ethylhexylcarbamate (Ag-EHCB) complex, PVP, hydrazine, and 2-propanol solvent concentrations in the reaction mixture were varied. The initial colloid has a mean particle diameter of 5-80 nm, and it exhibits an absorption band with various shapes in the UV region with a maximum near 420 nm. UV-vis spectroscopy, TEM, and X-ray diffraction techniques were used to investigate the formation and growth process of the metallic silver nanocolloids.

• Biotechnology and Bioprocess Engineering:BBE
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• 제2권2호
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• pp.105-108
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• 1997

A search was undertaken to screen microorganisms that produce an enzyme capable of deacylating glutary1-7-amincephalosporanic acid to 7-aminocephalosporanic acid in soil samples. The screening was carried out by preparing enrichment cultures containing glutary-7ACA and cephalosporin C as selective carbon sources. A non-${\beta}$-lactam model compound,, glutary-p-nitroanilide, was synthesized as a substrate suitable for the rapid screening of microorganisms isolated from the enrichment cultures. Two isolates exhibiting acylase activity, designated BY7.4 and BY8.1, were identified as strains of Pseudomonas species. Pseudomonas BY8.1 showed higher acylase activity toward G1-7ACA than Pseudomonas BY7.4. Environmental conditions for the optimal acylase activity of Pseudomonas BY8.1 were shown to be pH9 and 30$^{\circ}C$.

• 한국전기전자재료학회논문지
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• 제11권7호
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• pp.527-534
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• 1998

Thin film deposition of InN, which is a less-studied III-nitride compound semiconductor because of the difficulty if crystal growth, was performed by rf reactive sputtering method using In target and $N_2$reactive gas. The structrual, electrical, and optical properties of the produced films were measured and disussed according to the sputtering parameters such as deposition pressure, rf power, and substrate temperature. From the result of deposition pressure, rf power, and substrate temperature, we could obtain optimal conditions of 5m Torr, 60W, $60^{\circ}C$ for preparing InN thin film with high crystallinity, low carrier concentration, and high Hall mobility. The carrier concentration, Hall mobility, and optical bandgap of the fabricated InN thin films at optimal condition were $6.242\times10^{18}cm^{-3}, 212.526cm^2/V\cdot$ｓ, and 1.912eV, respectively.