• Title/Summary/Keyword: optimal analytical method

검색결과 361건 처리시간 0.027초

시아노아크릴레이트 진공 훈증법에 의한 잠재지문 현출 최적화에 관한 연구 (A study on the optimal conditions for latent fingerprint development using cyanoacrylate fuming method in vacuum chamber)

  • 유제설;정진성;임승;박성우
    • 분석과학
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    • 제25권3호
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    • pp.164-170
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    • 2012
  • 시아노아크릴레이트 훈증법은 비다공성 표면에 유류된 잠재지문을 현출할 때 효과적이다. 본 연구는, 진공챔버에서 시아노아크릴레이트를 훈증할 때 온도, 습도, 훈증 방법 등이 잠재지문 현출에 미치는 영향을 확인한 후 최적 반응 조건을 찾는데 있다. 진공챔버의 온도가 높을수록 시아노아크릴레이트 증발량은 증가했지만, 지문 융선에서 시아노아크릴레이트의 중합반응은 $30^{\circ}C$에서 가장 잘 일어났다. 상대습도가 40%, 50% 조건에서는 좋은 상태의 지문이 현출되었지만, 30%보다 낮거나 60%보다 높은 조건에서는 지문 융선에서 시아노아크릴레이트 중합반응 속도가 느려졌다. 진공챔버에서 시아노아크릴레이트를 자연적으로 증발시키는 방법보다는 $OMEGA-PRINT^{TM}$ dispersal pads와 수산화나트륨을 포함한 솜을 이용해 시아노아크릴레이트 훈증하는 방법이 효과적이란 사실을 확인할 수 있었다. 진공챔버에서 시아노아크릴레이트 처리시간은 상대습도에 비해 큰 영향을 주지 않았다.

Development of official assay method for loperamide hydrochloride capsules by HPLC

  • Le, Thi-Anh-Tuyet;Nguyen, Bao-Tan;Kim, Min-Ho;Kim, Bit;Kim, Hyun-Soo;Jeong, Seung-Won;Kang, Jong-Seong;Na, Dong-Hee;Chun, In-Koo;Kim, Kyeong Ho
    • 분석과학
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    • 제33권6호
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    • pp.252-261
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    • 2020
  • Currently, the potentiometric titration and the high pressure liquid chromatography (HPLC) method were utilized in Korean Pharmacopoeia XII (KP XII) as well as other pharmacopoeias (USP, EP, BP) for determination of loperamide hydrochloride in raw materials and capsules, respectively. The research objective is to overcome the remaining drawbacks from current methods such as solubility of mobile phase (KP XII), less scientific approach (USP 43) or using paired-ion chromatography reagent which shows some limitations (BP2017 and other formulation monographs). The proposed method was optimized by Design of Experiment (DoE) tool to obtain the satisfied method for determination of loperamide hydrochloride. The optimal condition was performed on the common C18 column (150 mm × 4.6 mm; 5 ㎛) using isocratic elution with the mobile phase containing 40 mM of potassium phosphate monobasic (pH 3.0) and acetonitrile (56:44), at a flow rate of 0.7 mL/min. The optimized method was validated and met the requirements of the International Conference on Harmonization. The developed method was applied to determine loperamide hydrochloride in capsules and can be used to update the current monograph in KP XII.

Data Interpolation and Design Optimisation of Brushless DC Motor Using Generalized Regression Neural Network

  • Umadevi, N.;Balaji, M.;Kamaraj, V.;Padmanaban, L. Ananda
    • Journal of Electrical Engineering and Technology
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    • 제10권1호
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    • pp.188-194
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    • 2015
  • This paper proposes a generalized regression neural network (GRNN) based algorithm for data interpolation and design optimization of brushless dc (BLDC) motor. The procedure makes use of magnet length, stator slot opening and air gap length as design variables. Cogging torque and average torque are treated as performance indices. The optimal design necessitates mitigating the cogging torque and maximizing the average torque by varying design variables. The data set for interpolation and ensuing design optimisation using GRNN is obtained by modeling a standard BLDC motor using finite element analysis (FEA) tool MagNet 7.1.1. The performance indices of the standard motor obtained using FEA are validated with an experimental model and an analytical method. The optimal design is authenticated using particle swarm optimization (PSO) algorithm and the performance indices of the optimal design obtained using GRNN is validated using FEA. The results indicate the suitability of GRNN as an interpolation and design optimization tool for a BLDC motor.

천정 크레인의 모델링 및 위치제어 (The Modelling and Position Control of Overhead Cranes)

  • 이종규
    • 대한기계학회논문집A
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    • 제25권12호
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    • pp.1919-1925
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    • 2001
  • Overhead cranes consist of trolley, girder, rope, objects, trolley motor, girder motor, and hoist motor. If objects are regarded as mass point, and the acceleration of hoisting motion for objects is neglected, analytical model of overhead cranes becomes a nonlinear model because the length of a rope changes. Equations of motion this model is derived of simultaneous differential equations fur motors and object. Positions of the model are controlled by optimal inputs which obtain from a nonlinear optimal control method. From the results of computer simulation, even if initial states of objects suing, it is founded that position of overhead cranes is controlled, and that swing of objects is suppressed.

광픽업 액추에이터 판스프링 서스펜션의 최적설계 (Optimal Design of the Plate Spring Suspension in an Optical Pickup Actuator)

  • 홍혁수;유정훈;이호철
    • 한국소음진동공학회논문집
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    • 제15권2호
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    • pp.232-238
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    • 2005
  • This paper proposed an optimal plate spring design for the optical pickup suspension. This method requires an analytic solution of plate spring suspension and it can be obtained by Castigliano's theorem and moment equilibrium. However, it is very complex due to the many design variables coupled and some constraints such as pitching angle in focusing motion caused by the characteristics of plate spring. Because of the complex formulation of the analytical solution that is used as the design objective, the genetic algorithm is used to find the optimal design value satisfying design constraints.

An analytical investigation of soil disturbance due to sampling penetration

  • Diao, Hongguo;Wu, Yuedong;Liu, Jian;Luo, Ruping
    • Geomechanics and Engineering
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    • 제9권6호
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    • pp.743-755
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    • 2015
  • It is well known that the quality of sample significantly determines the accuracy of soil parameters for laboratory testing. Although sampling disturbance has been studied over the last few decades, the theoretical investigation of soil disturbance due to sampling penetration has been rarely reported. In this paper, an analytical solution for estimating the soil disturbance due to sampling penetration was presented using cavity expansion method. Analytical results in several cases reveal that the soil at different location along the sample centerline experiences distinct phases of strain during the process of sampling penetration. The magnitude of induced strain is dependent on the position of the soil element within the sampler and the sampler geometry expressed as diameter-thickness ratio D/t and length-diameter ratio L/D. Effects of sampler features on soil disturbance were also studied. It is found that the induced maximum strain decreases exponentially with increasing diameter-thickness ratio, indicating that the sampling disturbance will reduce with increasing diameter or decreasing wall thickness of sampler. It is also found that a large length-diameter ratio does not necessarily reduce the disturbance. An optimal length-diameter ratio is suggested for the further design of improved sampler in this study.

접지임피던스의 변동이 최소가 되는 동축형 탄소접지전극의 길이의 산정 (Determination of the Length of Coaxial Type Carbon Grounding Electrode to Minimize the Fluctuation of Grounding Impedance)

  • 이강수;김종호;이복희
    • 조명전기설비학회논문지
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    • 제24권12호
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    • pp.164-170
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    • 2010
  • For the surge currents like lightning or ground fault currents containing high frequency components which cause the electromagnetic interferences for the electronic devices and communication equipment, the grounding impedances give the significantly composite characteristics which are dependent on the frequency of surge currents. In this paper, the analytical model and method for determining the optimal length of the newly developed coaxial type carbon ground electrode which has a little fluctuation in grounding impedance with frequency. The length of minimizing the fluctuation of grounding impedance by changing frequency from 100[Hz] to 1[MHz] was determined, and the validity of this proposed method was confirmed by comparing with the simulated and measured data.

분산전원이 연계된 배전계통의 최적 설비투자 방안에 관한 연구 (A Study on the Optimal Investment Method for Distribution Systems Interconnected with Dispersed Generations)

  • 노대석
    • 전기학회논문지
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    • 제57권12호
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    • pp.2179-2185
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    • 2008
  • This paper deals with the optimal investment method for distribution facilities, based on the analytical approach for the reliability assessment in distribution systems interconnected with new dispersed generations. The existing approach can estimate the expected reliability performance of distribution systems by a direct assessment of the configuration of the systems using the reliability indexes such as NDP(Non-Delivery Power) and NDE(Non-Delivery Energy). The indexes can only consider the number and configuration of the load, but can not consider the characteristics of the load which is the one of the most important factor in the investment cost for the distribution systems. Therefore, this paper presents the new performance indexes for the investment of the distribution facilities considering both the expected interruption cost for the load section and the operation characteristics of dispersed generations. The results from a case study show that the proposed methods can be a practical tool for the voltage management in distribution systems including dispersed sources.

Q-Learning based Collision Avoidance for 802.11 Stations with Maximum Requirements

  • Chang Kyu Lee;Dong Hyun Lee;Junseok Kim;Xiaoying Lei;Seung Hyong Rhee
    • KSII Transactions on Internet and Information Systems (TIIS)
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    • 제17권3호
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    • pp.1035-1048
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    • 2023
  • The IEEE 802.11 WLAN adopts a random backoff algorithm for its collision avoidance mechanism, and it is well known that the contention-based algorithm may suffer from performance degradation especially in congested networks. In this paper, we design an efficient backoff algorithm that utilizes a reinforcement learning method to determine optimal values of backoffs. The mobile nodes share a common contention window (CW) in our scheme, and using a Q-learning algorithm, they can avoid collisions by finding and implicitly reserving their optimal time slot(s). In addition, we introduce Frame Size Control (FSC) algorithm to minimize the possible degradation of aggregate throughput when the number of nodes exceeds the CW size. Our simulation shows that the proposed backoff algorithm with FSC method outperforms the 802.11 protocol regardless of the traffic conditions, and an analytical modeling proves that our mechanism has a unique operating point that is fair and stable.

Efficient Simulation Method for Dielectric Barrier Discharge Load

  • Oleg, Kudryavtsev;Ahmed, Tarek;Nakaoka, Mutsuo
    • Journal of Power Electronics
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    • 제4권3호
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    • pp.188-196
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    • 2004
  • The dielectric barrier discharge is recognized as one of the efficient methods of ultraviolet light generation and ozone production. As well, it is widely utilized for gaseous wastes neutralization and other technological processes in industry. This electrochemical reaction is electrically equivalent to a nonlinear capacitive load that represents some difficulties for designing the power supply. Therefore, a conventional power supply is designed for a drastically simplified model of the load and generally is not optimal. This paper presents a fast simulation approach for the nonlinear capacitive model representation of the dielectric barrier discharge load lamp. The main idea of the proposed method is to use analytical solutions of the differential state equations for the load and find the unknown initial conditions for the steady state by an optimization method. The derived expressions for the analytical solutions are rather complicated, however they greatly reduce the calculation time, which make sense when a deeper analysis is performed. This paper introduces the proposed simulation method and gives some examples of its application such as estimation of the load equivalent parameters and load matching conditions.