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Stability of Nano-emulsions prepared upon Change of Composition (조성변화에 따라 제조된 나노에멀젼의 안정성)

  • Cho, Wan Goo;Kim, Eun Hee;Jeon, Bong-Ju;Cha, Young-Kweon;Park, Seon-Ki
    • Journal of the Society of Cosmetic Scientists of Korea
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    • v.39 no.1
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    • pp.55-63
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    • 2013
  • Applications of nano-emulsion for cosmetics as a means of promoting dermal absorption have been the subject of interest. In this study, the stability of nano-emulsions prepared by low-energy emulsification method and varying the composition of raw materials was investigated. By measuring the particle size of the nano-emulsion against time, the stability of nano-emulsions prepared by adding polyol to water phase was increased significantly compared with the nano-emulsions prepared by adding polyol to ethanol phase. The speed of adding ethanol phase to water phase did not have a significant impact on the particle size and stability. Depending on the type of oil, stability was not affected. However, there would be a correlation between the initial size of the nano-emulsion droplets and the molecular weight and polarity of the oil. Stability and the initial particle size according to the type of polyols showed a similar trend except 1,2 hexanediol. The initial droplet size was affected by the concentration of surfactant and oil. However, the initial droplet size did not change against time. Concentration of ethanol was observed to have a significant impact on the initial particle size and stability.

Surface Morphology and Preferred Orientation of Gold Bump Layer formed by using $Na_3[Au(SO_3)_2]$ (아황산금나트륨염을 이용한 Au 범프용 금도금층의 표면형상 및 우선적 결정 성장방향)

  • Kim, In-Su;Yang, Seong-Hun;Park, Jong-Wan
    • Korean Journal of Materials Research
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    • v.5 no.6
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    • pp.673-681
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    • 1995
  • Surface morphology and preferred orientation of 20${\mu}{\textrm}{m}$ gold electrodeposit formed from aqueous solution of the sodium gold sulfite were studied in terms of current density, plating temperature and Au concentration. As the current density changed from 13.0mA/$\textrm{cm}^2$ to 4.6mA/$\textrm{cm}^2$, the solution temperature from 3$0^{\circ}C$ to 6$0^{\circ}C$, pH from 12.0 to 9.0, agitation speed from 0 rpm to 3200rpm and Au concentration from 10g/1 to 14 g/1, local Au concentration near the cathodic surface increased. With increasing the Au concentration, the surface morphology chanced from porous structure to fine-grained structure. Furthermore, it was observed that the preferred orentation of the Au layer changed from (111) to (220) upon the same variation In the Au concentration. The surface morphology and the preferred orientation of the Au layer were found to be closely related to each other.

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Temporal and Spatial Variations of Marine Meteorological Elements and Characteristics of Sea Fog Occurrence in Korean Coastal Waters during 2013-2017 (2013~2017년 연안해역별 해양기상요소의 시·공간 변화 및 해무발생시 특성 분석)

  • Park, So-Hee;Song, Sang-Keun;Park, Hyeong-Sik
    • Journal of Environmental Science International
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    • v.29 no.3
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    • pp.257-272
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    • 2020
  • This study investigates the temporal and spatial variations of marine meterological elements (air temperature (Temp), Sea Surface Temperature (SST), and Significant Wave Height (SWH)) in seven coastal waters of South Korea, using hourly data observed at marine meteorological buoys (10 sites), Automatic Weather System on lighthouse (lighthouse AWS) (9 sites), and AWS (20 sites) during 2013-2017. We also compared the characteristics of Temp, SST, and air-sea temperature difference (Temp-SST) between sea fog and non-sea-fog events. In general, annual mean values of Temp and SST in most of the coastal waters were highest (especially in the southern part of Jeju Island) in 2016, due to heat waves, and lowest (especially in the middle of the West Sea) in 2013 or 2014. The SWH did not vary significantly by year. Wind patterns varied according to coastal waters, but their yearly variations for each coastal water were similar. The maximum monthly/seasonal mean values of Temp and SST occurred in summer (especially in August), and the minimum values in winter (January for Temp and February for SST). Monthly/seasonal mean SWH was highest in winter (especially in December) and lowest in summer (June), while the monthly/seasonal variations in wind speed over most of the coastal waters (except for the southern part of Jeju Island) were similar to those of SWH. In addition, sea fog during spring and summer was likely to be in the form of advection fog, possibly because of the high Temp and low SST (especially clear SST cooling in the eastern part of South Sea in summer), while autumn sea fog varied between different coastal waters (either advection fog or steam fog). The SST (and Temp-SST) during sea fog events in all coastal waters was lower (and more variable) than during non-sea-fog events, and was up to -5.7℃ for SST (up to 5.8℃ for Temp-SST).

Physicochemical Properties and Antioxidant Activity of Extruded Rice Flour with Various Cacao (Theobroma cacao L.) Bean Content (카카오 빈 함량에 따른 쌀 압출성형물의 이화학적 특성 및 항산화 활성)

  • Park, Ju-Yeon;Kim, Young-Ho;Ryu, Gi-Hyung
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.46 no.11
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    • pp.1327-1335
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    • 2017
  • This study was carried out to determine the effect of cacao bean addition on the physicochemical properties of extruded rice flour. Rice-based cacao beans (0, 20, 40, 60%) were extruded at a die temperature of $130^{\circ}C$, screw speed of 200 rpm, and moisture content of 25%. As the content of cacao beans increased from 20% to 60%, expansion index decreased, while piece density and specific length increased. The water soluble index and water absorption index of the extrudate increased through extrusion cooking. Lightness decreased as cacao bean content increased while redness increased. As the content of cacao beans increased, paste viscosity decreased. Cold peak viscosity was observed in all extrudates of raw roasted cacao beans. ${\alpha},{\alpha}$-Diphenyl-${\beta}$-picrylhydrazyl (DPPH) radical-scavenging activity increased upon extrusion and cacao bean addition. As content of cacao beans increased, non-roasted cacao beans had higher total phenolic contents than roasted cacao beans. This study showed that addition of cacao beans to extruded rice snack improved antioxidant activity.

A numerical Study for Improvement of Indoor Air Quality of Apartment House (공동주택 단지의 실내 공기질 향상을 위한 수치 해석적 연구)

  • Shin, Mi-Soo;Kim, Hey-Suk;Hong, Ji-Eun;Jang, Dong-Soon
    • Journal of Korean Society of Environmental Engineers
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    • v.31 no.7
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    • pp.521-530
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    • 2009
  • This study has been made to execute a research in order to lead the improvement of indoor air quality, examining the indoor ventilation characteristics by using a numerical analysis method. To this end an extensive parametric investigation are made according to various external flow variables such as main wind direction and wind speed by season, building layout design, and location of ventilators, etc. in Daedeok Techno Valley, one of large-scaled apartment in Daejeon. It is observed there was a significant difference of main wind direction between summer and winter. The main wind direction in summer was a south wind, and on the contrary the direction in winter is northnorthwest, which is similar to the average main wind direction for 10 years. One of the important calculation results is that the change of wind direction causes a significant effect on the apartment ventilation by the change of pressure difference around each complex of apartment. In case of favorable area of ventilation, the indoor ventilation rate can meet 0.7 ACH from the standard value only with natural ventilation. On the contrary, in other area the value was much lower than the standard value. If the calculation result applies to the design of layout apartment or placement of ventilators, it will be greatly helpful to the energy saving because it can be parallel with the natural ventilation to help securing ventilation rate, not much depending on the mechanical ventilation.

INFLUENCE OF APPLICATION METHODS OF A DENTIN ADHESIVE ON SHEAR BOND STRENGTH AND ADHESIVE PATTERN (상이질 접착제의 적용방법에 따른 전단결합강도와 접착양상에 관한 연구)

  • Park, Sung-Taek;Moon, Joo-Hoon;Cho, Young-Gon;Ohn, Yeong-Suck
    • Restorative Dentistry and Endodontics
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    • v.24 no.2
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    • pp.381-391
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    • 1999
  • A new 5th generation adhesive system(ONE-STEP) has been supplied which operators can apply to conditioned tooth surfaces by one simplified step. The purpose of this study was to determine whether different methods of adhesive application and various air drying duration after applying adhesive affect the shear bond strength of composite resin to dentin, and to evaluate the adhesive pattern of composite resin and dentin under SEM. Seventy-seven extracted human molar teeth were cleaned and mounted in palstic test tubes. The occlusal dentin surfaces were exposed with Diamond Wheel Saw and smoothed with Lapping and Polishing Machine (South Bay Technology Co., U.S.A.). Teeth were randomly divided into 7 groups (n=11), In experimental A group, adhesive was applied to dentin with agitation for 20 sec. In experimental N-A group, adhesive were continuously applied to dentin for 20 sec. Also control and experimental 1, 2, 3, 4 groups were dried for 10, 0, 5, 20, 30 seconds after applying adhesive, respectively, Adhesives were light cured for 10 sec. A gelatin capsule 5mm in diameter was filled with Aelitefil$^{TM}$ composite resin, placed on the treated dentin surface and light cured for 40 see, from three sides, All specimens were stored in distilled water at room temperature for 24 hours. The shear bond strengths were measured using a universal testing machine(AGS-1000 4D, Japan) at a crosshead speed of 5mm/min. An one-way ANOVA and LSD test were used for statistical analysis of the data. For SEM evaluation, seven specimens were made and sectioned. Representive postfracture and seven specimens were mounted on brass stubs, sputter-coated with gold and observed under SEM. The results were as follows : 1. The shear bond strength of experimental A group which adhesive were applied to dentin with agitation was higher than that of experimental N-A group (continuous application), and there was significant difference between two groups (p<0.01). 2. The interface between composite and dentin according to different application methods showed close adaptation in experimental A group and showed tinny gap in experimental N-A group. 3. The shear bond strength accoding to various air drying duration was the lowest value(7.57${\pm}$2.60 MPa) in experimental 1 group, so there was significant difference between experimental 1 group and other four groups (p<0.05). But there was no significant difference of shear bond strength between four groups (p>0.05). 4. The interface between composite and dentin according to various air drying duration showed close adaptation in control group and tinny gap in experimental 3 and 4 groups. But experimental 1 and 2 groups showed $30{\mu}$ and 6 - $10{\mu}m$ thick gaps, respectively.

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EFFECT OF CURING METHODS OF RESIN CEMENTS ON BOND STRENGTH AND ADHESIVE INTERFACE OF POST (레진시멘트의 중합방법이 포스트의 결합강도와 접착계면에 미치는 영향)

  • Kim, Mun-Hang;Kim, Hae-Jung;Cho, Young-Gon
    • Restorative Dentistry and Endodontics
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    • v.34 no.2
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    • pp.103-112
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    • 2009
  • The purpose of this study was to compare the effect of curing methods of adhesive resins and resin cements in the root canal. Crown portions of 32 single-rooted mandibular premolars were removed. Routine endodontic treatment was done, and 9 mm deep post spaces were prepared within root canals. No.3 FRC Postec posts (Ivoclar-Vivadent AG, Liechtensteih) were cemented in the post spaces by self-(SC) or light-curing (LC) using two dual-cured adhesives (Adper Scotchbond multi-purpose plus and Exite DSC )and resin cements (RelyX ARC and Variolink II). They were assigned to 4 groups (n=8): R-SC, R-LC, V-SC, V-LC group. After stored in distilled water for 24 hours, each root was transversally sectioned with 1.5 mm thick and made three slices. The specimens were subjected to push-out test in a universal testing machine (EZ Test, Shimadzu Co., Japan) with a crosshead speed of 1 mm/min. The data were analyzed with repeated ANOVA and one-way ANOVA. Also the interface of post-resin cement and resin cement-canal wall of each group was observed under FE-SEM. When fiber posts were cemented into the root canal using total-etch adhesives, the bond strength and adaptation between post and root canal dentin was affected by curing method. Self-cure of adhesives and resin cements showed higher bond strength and closer adaptation than light-cure of them.

EFFECT OF DENTIN SURFACE WETNESS ON TENSILE BOND STRENGTH OF SELF ADHESIVE RESIN CEMENTS (상아질 표면 젖음성이 수종 자가접착레진시멘트의 인장접착강도에 미치는 영향)

  • Yoon, Sung-Young;Park, Se-Hee;Kim, Jin-Woo;Cho, Kyung-Mo
    • Restorative Dentistry and Endodontics
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    • v.34 no.2
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    • pp.113-119
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    • 2009
  • The purpose of this study was to compare the tensile bond strength of several self-adhesive resin cements bonded to dentin surfaces with different wet conditions. Three self-adhesive resin cements: Rely-X Unicem (3M ESPE, St. Paul, MN. USA). Embrace Wetbond (Pulpdent. Oakland. MA. USA). Maxcem (Kerr. Orange. CA. USA) were used. Extracted sixty human molars were used. Each self-adhesive resin cement was adhered to the dentin specimens (two rectangular sticks from each molar) in different wet conditions. Tensile bond strength were measured using universal testing machine (EZ Test. Shimadzu corporation. Kyoto. Japan) at a crosshead speed of 1.0mm/min. After the testing. bonding failures of specimens were observed by Operative microscope (OPMI pro, Carl Zeiss. Oberkochen, Germany). T-test was used to evaluate the effect of dentin surface wetness. One-way ANOVA test was used to evaluate the tensile bond strength of self-adhesive resin cements in the same condition. Scheffe's test was used for statistical analyzing at the 95% level of confidence. The result showed that wetness of dentin surface didn't affect tensile bond strength of self-adhesive resin cements and Maxcem showed the lowest tensile bond strength.

A SEM OBSERVATION ON THE EFFICIENCY PREPARATION OF OVAL CANALS USING HAND AND ENGINE-DRIVEN INSTRUMENTS (수동과 엔진구동형 기구를 이용한 난원형 근관의 형성에 관한 주사전자현미경적 관찰)

  • Song, Uk;Hur, Bock;Lee, Hee-Joo
    • Restorative Dentistry and Endodontics
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    • v.29 no.2
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    • pp.141-146
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    • 2004
  • The purpose of this study was to evaluate the efficiency of the preparation of oval canals using hand and engine-driven instruments with SEM observation. Thirty single-rooted teeth with oval canal were used in this study. The teeth were divided into 3 groups. In group A the teeth were instrumented up to a size 35 K-file using RC-prep and irrigated with 5% NaOCl between each file size. In group B. the teeth were instrumented with Profile according to the manufacture's instructions using RC-Prep and irrigated with 5% NaOCl between each file size. In group C. the teeth were instrumented with GT file according to the manufacture's instructions using RC-prep and irrigated with 5% NaOCl between each file size. Then. in all teeth. a final flush of 5ml of distilled water delivered for 30s. Canals were dried with sterile standardized paper points. After preparing the canals, the teeth were sectioned along their mesial and diatal surfaces by using low-speed diamond disc. chisel and mallet. Each root section was then dehydrated in graded concentration of alcohol (70, 80, 90, 100%). mounted on an aluminum stub. sputter-coated with gold-palladium and observed with scanning electron microscope (HITACHI S-4200) in middle and apical area. The results of this study were as follows: 1. In the middle area. group B and group C showed less smear layer than group A and it was statistically significant (p < 0.05). 2. In the middle area. group B showed greater smear layer than group C. but it was not statistically significant (p > 0.05). 3. In the apical area, group C showed less smear layer than group A. and it was statistically significant (p < 0.05). 4. In the apical area. group A showed greater smear layer than group B. but it was not statistically significant (p > 0.05). 5. In the apical area. group B showed greater smear layer than group C. but it was not statistically significant (p > 0.05). 6. In all groups. the middle area was less smear layer than the apical area. and it was statistically significant (p < 0.05).

Mechanical Properties of Unilateral & Bilateral Movement in Isokinetic Knee Extension and Flexion (등속성 무릎 굴곡과 신전 시 외측 및 양측운동의 역학적 특성)

  • Kim, Yong-Woon;Kim, Yong-Jae
    • Korean Journal of Applied Biomechanics
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    • v.18 no.3
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    • pp.83-92
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    • 2008
  • Y. W. KIM, Y. J. KIM, Mechanical Properties of Unilateral & Bilateral Movements in Isokinetic Knee Extension and Flexion. Korean Journal of Sport Biomechanics, Vol. 18, No. 3, pp. 83-92, 2008. The purpose of this study was to examine the mechanical properties and patterns of bilateral and unilateral movement under varying velocities and movement patterns. The unilateral and bilateral isokinetic knee extension and flexion were taken for three speeds of 13 healthy male subjects. Although there was bilateral facilitation at the speed of $450^{\circ}$/s for the bilateral movement of knee extension, as a whole there was less resultant torque and power of bilateral movement than summed unilateral under knee flexion and extension of 3 velocity condition. There was significant correlations between bilateral deficits within individuals observed for an the same movement($120^{\circ}-240^{\circ}$ flexion, $120-240^{\circ}$ extension, $240^{\circ}-450^{\circ}$ extension), which means that same agonist was recruited. On the contrary, although there was a tendency of a similar pattern of the individuals bilateral deficit according to the varying velocities, there was not a significant correlations between bilateral deficits of flexion and extension within individual, which means that different agonist was recruited. With the analyses of this results the individuals neuromuscular characteristics and the effecting factors for bilateral movement can be speculated upon.