• Title/Summary/Keyword: non-isothermal

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A Study on the Bainite Phase Control of Direct-Quenched Low Carbon Steels (저탄소 직접 소입강의 베이나이트상 조절에 관한 연구)

  • An, Byeong-Gyu;Go, Yeong-Sang;Lee, Gyeong-Seop
    • Korean Journal of Materials Research
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    • v.6 no.8
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    • pp.841-851
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    • 1996
  • In a recent investigation, the formation of bainite phase in direct-quenched low carbon non heat-treated steel was reported. In this study the effects of bainite phase on the mechanical properties of direct-quenched microalloying steels were investigated. By isothermal transformation at $480^{\circ}C$ for 7 sec., volume fraction of bainite lath was 15~20%, and the UTS and impact energy were increased. In this case $B_{ll}$ and $B_{lll}$ type bainite was observed and the fractography of impact test specimen showed a ductile fracture tendency. Isothermal transformation for 100sec., yielded 30% volume fraction of granular bainite and the mechanical properties were decreased. The f ractography of impact test specimen showed a brittle fracture tendency. The addition of Mo was more effective than B for improving impact energy because amounts of boron aditions were restricted to considerably lower levels, typically 10~ 30ppm. From this study, it is predicted that 15~20% volume fraction of lath bainite on the direct quenching process is procduced by addition of Mo up to 1.2wt. % and controlling the finish forging proc¬ess at $1000^{\circ}C$ and using oil as direct quenching media. This will improve mechanical properties of the direct- quenched steel.

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Rapid and Sensitive Detection of Hepatitis C Virus in Clinical Blood Samples Using Reverse Transcriptase Polymerase Spiral Reaction

  • Sun, Wenying;Du, Ying;Li, Xingku;Du, Bo
    • Journal of Microbiology and Biotechnology
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    • v.30 no.3
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    • pp.459-468
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    • 2020
  • This study established a new polymerase spiral reaction (PSR) that combines with reverse transcription reactions for HCV detection targeting 5'UTR gene. To avoid cross-contamination of aerosols, an isothermal amplification tube (IAT), as a separate containment control, was used to judge the result. After optimizing the RT-PSR reaction system, its effectiveness and specificity were tested against 15 different virus strains which included 8 that were HCV positive and 7 as non-HCV controls. The results showed that the RT-PSR assay effectively detected all 8 HCV strains, and no false positives were found among the 7 non-HCV strains. The detection limit of our RT-PSR assay is comparable to the real-time RT-PCR, but is more sensitive than the RT-LAMP. The established RT-PSR assay was further evaluated for detection of HCV in clinical blood samples, and the resulting 80.25% detection rate demonstrated better or similar effectiveness compared to the RT-LAMP (79.63%) and real-time RT-PCR (80.25%). Overall, the results showed that the RT-PSR assay offers high specificity and sensitivity for HCV detection with great potential for screening HCV in clinical blood samples.

The Effects of Packing and Cooling Stages on the Molded Parts in Injection Molding Process (사출 성형시 보압 및 냉각 과정이 성형품에 미치는 영향)

  • 구본흥;신효철;이호상
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.17 no.5
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    • pp.1150-1160
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    • 1993
  • The behavior of polystyrene in the strip cavity during the packing and cooling stages for an injection molding process is examined numerically. The mathematical model is based on the unified post-filling model and finite element/finite difference methods are used to solve simultaneously the continuity, momentum and energy equations coupled to an equation of state. Simulated results show that the density of the molded parts is lower in the core than at the skin, and that the hotter the melt or the higher the packing pressure, the higher the density in the core. The density variation during the packing stage comes up to 50% compared with the total density variation. Also, the density variation after gate sealing and the effect of cooling rate on the equation of state are negligible.

Numerical Study of Internal Flow in Twin Screw Extruder and Its Mixing Performance Analysis (이축 스크루 압출기내 유동의 수치 해석과 혼합 성능 분석)

  • Kim, Nak-Soo;Kim, Hong-Bum;Lee, Jae-Wook
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.30 no.1 s.244
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    • pp.32-41
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    • 2006
  • We analyzed the non-Newtonian and non-isothermal flow in the melt conveying zone in co-rotating and counter-rotating screw extruder system with the commercial code, STAR-CD, and compared the mixing performance with respect to screw speed and rotating direction. The viscosity of fluid was described by power-law model. The dynamics of mixing was studied numerically by tracking the motion of particles in a twin screw extruder system. The extent of mixing was characterized in terms of the residence time distribution and average strain. The results showed that high screw speed decreases the residence time but increases the shear rate. Therefore higher screw speed increases the strain and has better mixing performance. Counter-rotating screw extruder system and co-rotating screw extruder has the similar shear rate with the same screw speed in spite of different rotating direction. However, the counter-rotating screw has good mixing performance, which is resulted from longer residence time than that of co-rotating screw extruder.

Numerical analysis of internal flow and mixing performance in polymer extruder II: twin screw element

  • Kim, Nak-Soo;Kim, Hong-Bum;Lee, Jae-Wook
    • Korea-Australia Rheology Journal
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    • v.18 no.3
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    • pp.153-160
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    • 2006
  • We analyzed the non-Newtonian and non-isothermal flow with Carreau-Yasuda viscosity model in co-rotating and counter-rotating twin screw extruder systems. The mixing performances with respect to the screw speed, the screw pitch, and the rotating direction have been investigated. The dynamics of mixing was studied numerically by tracking the motions of particles. The extent of mixing was characterized in terms of the deformation rate, the residence time distribution, and the average strain. The results showed that the high screw speed decreases the residence time but increases the deformation rate. Small screw pitch increases the residence time. It is concluded that the high screw speed increases the dispersive mixing performance, while the small screw pitch increases the distributive mixing performance. Co-rotating screw extruder has the better conveying performance and the distributive mixing performance than counter-rotating screw extruder with the same screw speed and pitch. Co-rotating screw extruder developed faster transport velocity and it is advantageous the flow characteristics to the mixing that transfers polymer melt from one barrel to the other barrel.

Degradation of Functional Materials in Temperature Gradients - Thermodiffusion and the Soret Effect

  • Janek, Jurgen;Sann, Joachim;Mogwitz, Boris;Rohnke, Marcus;Kleine-Boymann, Matthias
    • Journal of the Korean Ceramic Society
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    • v.49 no.1
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    • pp.56-65
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    • 2012
  • Functional materials are often exposed to high temperatures and inherent temperature gradients. These temperature gradients act as thermodynamic driving forces for the diffusion of mobile components. The detailed consequences of thermodiffusion depend on the boundary conditions of the non-isothermal sample: Once the boundaries of the sample are inert and closed for exchange of the mobile components, thermodiffusion leads to their pile-up in the stationary state (the so called Soret effect). Once the system is open for an exchange of the mobile component, chemical diffusion adds to the Soret effect, and stationary non-zero component fluxes are additionally observed in the stationary state. In this review, the essential aspects of thermodiffusion and Soret effect in inorganic functional materials are briefly summarized and our current practical knowledge is reviewed. Major examples include nonstoichiometric binary compounds (oxides and other chalcogenides) and ternary solid solutions. The potential influence of the Soret effect on the long term stability of high temperature thermoelectrics is briefly discussed. Typical Soret coefficients for nonstoichiometric compounds are found to be of the order of (d${\delta}$/dT) ${\approx}$ 1%/K.

Catalyst Effects on Cross-linking of a Multi-Functional Fluoropolymer/Blocked-HMDI Blends (다기능성 함불소고분자/Blocked-HMDI 블렌드계의 가교화 반응에서의 촉매 영향)

  • Ahn, Won-Sool
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.13 no.5
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    • pp.2408-2413
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    • 2012
  • Effects of stanous catalyst on the cross-linking reaction characteristics of multi-functional fluoropolymer with blocked-hexamethylene diisocyanate(HMDI) were studied by dynamic DSC and non-isothermal thermogravimetric analysis (TGA). Results showed that cross-linking reaction occurred around $230-250^{\circ}C$ aftr the solvent and phenol, blocking agent, were removed upto the $150^{\circ}C$. It was considered that the reaction mechanism of the multi-functional fluoropolymer with HMDI might not be changed by the catalyst, however, the reaction rate became extremely faster upto to 100 times, showing the change of activation energy 81.8 kJ/mol for non-catalytic system to 61.7 kJ/mol for 1 phr catalytic system.

Prediction of the Forming Load of Non-Axisymmetric Isothermal Forging using Approximate Similarity Theory (근사 상사 이론을 이용한 비축대칭 등온 단조의 가공하중 예측)

  • 한정영;최철현;배원병;김영호;이종헌
    • Journal of the Korean Society for Precision Engineering
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    • v.17 no.1
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    • pp.204-208
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    • 2000
  • An approximate similarity theory has been applied to predict the forming load of non-axisymmetric forging of aluminum alloys through model material tests. The approximate similarity theory is applicable when strain rate sensitivity, geometrical size, and die velocity of model materials are different from those of real materials. Actually, the forming load of yoke, which is an automobile part made of aluminum alloys(Al-6061), is predicted by using this approximate similarity theory. Firstly, upset forging tests are have been carried out to determine the flow curves of three model materials and aluminum alloy(Al-6061), and a suitable model material is selected for model material test of Al-6061. And then hot forging tests of aluminum yokes have been performed to verify the forming load predicted from the model material, which has been selected from above upset forging tests. The forming loads of aluminum yoke forging predicted by this approximate similarity theory are in good agreement with the experimental results of Al-6061 and the results of finite element analysis using DEFORM-3D.

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Effect of temperature and blank holder force on non-isothermal stamp forming of a self-reinforced composite

  • Kalyanasundaram, Shankar;Venkatesan, Sudharshan
    • Advances in aircraft and spacecraft science
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    • v.3 no.1
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    • pp.29-43
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    • 2016
  • Composite materials are rapidly gaining popularity as an alternative to metals for structural and load bearing applications in the aerospace, automotive, alternate energy and consumer industries. With the advent of thermoplastic composites and advances in recycling technologies, fully recyclable composites are gaining ground over traditional thermoset composites. Stamp forming as an alternative processing technique for sheet products has proven to be effective in allowing the fast manufacturing rates required for mass production of components. This study investigates the feasibility of using the stamp forming technique for the processing of thermoplastic, recyclable composite materials. The material system used in this study is a self-reinforced polypropylene composite material (Curv$^{(R)}$). The investigation includes a detailed experimental study based on strain measurements using a non-contact optical measurement system in conjunction with stamping equipment to record and measure the formability of the thermoplastic composites in real time. A Design of Experiments (DOE) methodology was adopted to elucidate the effect of process parameters that included blank holder force, pre heat temperature and feed rate on stamp forming. DOE analyses indicate that feed rate had negligible influence on the strain evolution during stamp forming and blank holder force and preheat temperature had significant effect on strain evolution during forming.

Analysis of warm Deep Drawing of Magnesium Alloy Sheet (마그네슘 합금 판재의 온간 딥드로잉 해석)

  • Lee, M.H.;Kim, H.Y.;Kim, H.J.;Oh, S.I.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2007.05a
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    • pp.294-297
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    • 2007
  • Due to their low densities and high specific strength and stiffness, magnesium alloy sheets are very attractive lightweight materials for automotive and electrical products. However, the magnesium alloy sheets are usually formed at elevated temperature because of their poor formability at room temperature. To use of the magnesium alloy sheets for an industrial, their mechanical properties at elevated temperature and appropriate forming process conditions have to be developed. In this study, non-isothermal simulations of a square cup drawing from magnesium alloy sheets have been conducted to evaluate a proper forming process conditions such as the tool temperature, the tool shoulder radius, friction between the blank and the tools. According to this study, appropriate forming process conditions of square cup drawing at elevated temperature from magnesium alloy sheets are suggested.

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