• Title/Summary/Keyword: no reference

Search Result 2,206, Processing Time 0.032 seconds

Absorbance Elevation of Orimax Blue 2N, Orimax Green 151, Quinizarin, Topasol (P-250) and Lubricant (P-8) on the Spectrophotometric Analysis of Unimark 1494 DB (식별제(Unimark 1494DB) 정량시험에서 파란색 색소(Orimax Blue 2N, Orimax Green 151), Quinizarin, 토파졸(P-250) 및 윤활유 원료(P-8)의 흡광도상승 효과)

  • Lee, Ji-Yun;Kim, Chang-Jong
    • YAKHAK HOEJI
    • /
    • v.50 no.5
    • /
    • pp.313-321
    • /
    • 2006
  • There are three kinds of liquid petroleum marker which is extracted by the basic or acidic, and both developer. Korean marker, Unimark 1494 DB (marker) have been spectrophotometrically analysed by the determination of absorbance at 582 nm after base extraction by Unimark 1494 DB Developer C-5 (developer). Some blue dyes which have same reactive radical of marker and can be changed deep blue color in base developer extraction (BDE), may be increased absorbance at 582 nm, but dyes or markers which can be increased the absorbance, were not unclear. In this experiment, effects of three dyes or marker such as Orimax Green 151 (the mixture of CI Solvent Yellow 16 and CI Solvent Blue 70), quinizarin and Orimax Blue 2N (CI Solvent Blue 35), and two solvent such as topasol (P-250) and lubricant (P-8) on the absorbance were studied by HITACHI Recording Spectrophotometer U-3300. It shows that all of them increased absorbance at 582 nm after BDE. Absorbance at 582 nm can be showed 0.0544 by Orimax Green 151 at the concentration of 3.96 mg/l, quinizarin at the concentration of 1.38 mg/l, and Orimax Blue 2N at the concentration of 2.73 mg/l in the artificial petroleum (normal diesel oil: topasol: lubricant=2 : 4: 4), respectively. Absorbance, 0.0544 indicates that concentration of marker is 1.64 mg/l in the reference curves, respectively. And also these results can be showed that the artificial petroleum have about 10% cheep fuel such as kerosene which have marker (16.0 mg/l). Absorbance of P-250 was 0.01361-0.22842 depending upon the purchasing date, and that of P-8 was 0.05644. pH of developer was 14.83, and so this result indicates that Unimark 1494 DB is a base extractable petroleum marker, phenylazophenol (US Patent No. 5,252,106). In the BDE, the slight color of Orimax Blue 2N, Orimax Green 151 and quinizarin in artificial petroleum changed to deep bright blue color, respectively. These result indicate that the absorbance at 582 nm by BDE may be increased not only by azo, diazo, amine and ketone (anthraquinone, coumarin) dyes or markers, but also the contaminants of P-250 and P-8 which have same as reactive radical of dyes or markers.

Separation and Recovery for the Analysis of Radioiodine in RI Wastes (RI 폐기물 내 방사성요오드 분석을 위한 분리 및 회수)

  • Kang, Sang-Hoon;Han, Sun-Ho;Lee, Heung-N.;Jee, Kwang-Yong;Lee, In-Koo
    • Journal of Nuclear Fuel Cycle and Waste Technology(JNFCWT)
    • /
    • v.5 no.4
    • /
    • pp.267-272
    • /
    • 2007
  • Various kinds of RI wastes are discharged from licensed organizations of radioisotopes les such as hospitals and clinic organizations, educational organizations, research institutions, and public organizations. Radioiodines such as $^{125}I\;and\;^{131}I$ are radioisotopes mainly used in nuclear medicine and industry. A method for the determination of radioiodines in RI wastes has been applied to measure low level activity using acid decomposition method and HPGe gamma ray spectrometer. Prior to analysis of real samples, $^{131}I$ reference solution and 10 g of yellow tissue paper was added to flask in mantle and was heated in 100 mL of 0.4 N $K_2Cr_2O_7$ and 100 mL of 9 M $H_2SO_4$, and then distilled after adding 10 mL of 30% $H_2PO_3$ and 1 mL of 30% $H_2O_2$. The condensed iodine by circulator was extracted into $CCl_4$, then back-extracted into the aqueous phase with 10 mL of 5% $K_2SO_2$ solution. Finally, $^{131}I$ was measured at 364.48 keV using HPGe gamma ray spectrometer after precipitation and filtration. Chemical yield of three steps such as acid decomposition process, chemical separation process, and precipitation and filtration process was more han 94% respectively, MDA(Minimum Detectable Activity) of $^{131}I$ at this analytical condition was 0.6 Bq/g.

  • PDF

Quality Characteristics of Kimchi Added with Green Tea Powder (분말녹차 첨가 김치의 품질 특성)

  • Ko, Young-Tae;Lee, Su-Hyun
    • Applied Biological Chemistry
    • /
    • v.50 no.4
    • /
    • pp.281-286
    • /
    • 2007
  • The effects of green tea powder (GTP) on kimchi quality were evaluated by investigating acid production, growth of lactic acid bacteria, sensory properties, and several volatile odor components of GTP-added kimchi. The concentrations of GTE added to kimchi were 0.2, 0.4, 0.6 and 1.2% (w/w) of salted Chinese cabbage. The pH of kimchi with higher amounts of added GTP increased with ripening. The acidity of unripened kimchi or kimchi ripened for one day generally increased with the addition of GTP, while that of kimchi ripened for two or three days generally decreased with the addition of GTP. Addition of GTP had no significant effect on the lactic acid bacterial count of kimchi. Scores of overall acceptability, taste and odor of 0.2 or 0.4% GTP-added kimchi were higher than those of other samples, whereas scores of color decreased with increasing amount of GTP added to kimchi. Texture of kimchi added with higher amounts of GTP and ripened for two or three days resulted in lower score than the reference sample. Diallyl sulfide and methyl trisulfide were newly produced with the ripening of kimchi, and the amounts of some volatile odor components in kimchi were changed during ripening.

THE LONGITUDINAL GROWTH CHANGES OF CRANIOFACIAL STRUCTURE IN KOREAN ADULT (DURING THE AGE OF 24 TO 31) (성인 두개안면골의 성장변화(24세에서 31세까지))

  • Sohn, Dong-Seok;Park, Hyo-Sang;Bae, Sung-Min;Sung, Jae-Hyun
    • The korean journal of orthodontics
    • /
    • v.27 no.6 s.65
    • /
    • pp.917-927
    • /
    • 1997
  • Recently, according to the Increase of adult patient, it is neccessory to understand the growth changes of adult after cessation of active pubertal growth in clinical orthodontics. The purpose of this study was to investigate the growth changes of craniofacial structure after active growth period(adult) in order to use as reference in clinical orthodontics. Authors followed the 40 sample(male 25, female 15) from 24 to 31 years of age. By analysing the serial cephalograms, authors could get the following findings. $\cdot$ The mandible rotated clockwise in female, but not in male, and no incremental growth change in both genders. $\cdot$ The anterior facial height and lower anterior facial height were increased in both genders, the increase of lower anterior facial height exceed the posterior facial height increase in female. $\cdot$ The cranial base was stable throughout observation period. $\cdot$ The upper incisors uprighted slightly in female. $\cdot$ There were great the individual variation in the growth change of craniofacial structure in adult.

  • PDF

Analysis on mandibular movement using the JT-3D system (JT-3D system을 이용한 하악의 운동 분석)

  • Song, Joo-Hun;Kim, Ryeo-Woon;Byun, Jae-Joon;Kim, Hee-Jung;Heo, Yu-ri;Lee, Gyeong-Je
    • Journal of Dental Rehabilitation and Applied Science
    • /
    • v.36 no.2
    • /
    • pp.80-87
    • /
    • 2020
  • Purpose: This study aims to measure the mandibular movement using JT-3D system and provide a range of mandibular movement that can serve as a good reference for diagnosing the temporomandibular disorder. Materials and Methods: This study was conducted in 60 young male and female adults. The maximum opening and closing movement was recorded using JT-3D system, and by regarding 5 times of repetitive movement as 1 cycle of movement, total 3 cycles of movement were recorded. During the maximum opening, vertical position of lower jaw, antero-posterior position, lateral deflection position, and maximum opening distance were recorded. To evaluate the reproducibility of JT-3D system, statistical analysis were conducted (α = 0.05). Results: During the maximum opening, the average value appeared at 31.56 mm vertically and 24.42 mm rearwardly, lateral deflection position 0.72 mm, and maximum opening distance 40.32 mm. There was no statistical significance in all measured values for three cycles of movement recorded with JT-3D system (P > 0.05). Conclusion: During the maximum opening, the average value appeared at 0.72 mm in lateral deflection position and the maximum opening distance at 40.32 mm, and the analysis on the maximum opening of lower jaw using JT-3D system showed sufficiently reproducible results.

Gender, Residential Areas, Retirement Transitions, and Psychological Well-Being of the Elderly (은퇴가 심리적 안녕에 미치는 영향에 관한 종단적 연구: 노인의 성과 거주지역을 중심으로)

  • Yoon, Hyun-Sook;Lee, Mi-Jin
    • Korean Journal of Social Welfare
    • /
    • v.58 no.4
    • /
    • pp.197-217
    • /
    • 2006
  • This study examined whether a relationship between retirement transitions and psychological well-being of the elderly may differ by gender and residential areas, and whether associative factors of psychological well-being may vary by gender and residential areas. The sample included 1,124 older adults aged 60 and over, which derived from the first wave and the third wave data of the "Aging and the Quality of Life of the Elderly in Korea: A Longitudinal Study" living in Seoul and Chuncheon. The total sample was divided into four sub-samples(urban male elders, rural male elders, urban female elders, and rural female elders) to answer research questions. Psychological well-being was measured by measured by the PGCMS developed by Lawton, and a retirement variable had four categories: being continuously non-retired, newly retired, newly non-retired, and being continuously retired with a reference group of being continuously non-retired. Multivariate OLS regression was run separately for the four groups. For urban male elders, retirement transition was associated with worse psychological well-being whereas no relationship between retirement transitions and psychological well-being was found for rural male elders, urban female elders, and rural female elders. Associative factors of psychological well-being varied by gender and residential areas. The findings implies that a relationship between retirement transitions and psychological well-being of the elderly may differ by gender and residential areas, and these differential effects of retirement transitions may be attributable to different life experiences and economic activities through a life course and different roles after retirement. Also, different associative factors of psychological well-being for the four sub-samples reflect variations in their different life course.

  • PDF

Ecological Risk Assessment of Pharmaceuticals in the Surface Water Near a Pharmaceutical Manufacturing Complex in Korea (제약단지 인접 지역 지표수의 잔류 의약물질 생태위해성평가)

  • Park, Suhyun;Kang, Habyeong;Shin, Hyesoo;Ryoo, Ilhan;Choi, Kyungho;Kho, Younglim;Park, Kyunghwa;Kim, Kyungtae;Ji, Kyunghee
    • Journal of Environmental Health Sciences
    • /
    • v.46 no.1
    • /
    • pp.45-64
    • /
    • 2020
  • Objectives: Limited information is available on the presence and associated ecological risks of pharmaceutical residues in aquatic environments near pharmaceutical manufacturing areas in Korea. In this study, we investigated the current state of pharmaceutical contamination and its associated ecological risks in streams near a pharmaceutical manufacturing complex. Methods: Seven pharmaceuticals (acetaminophen, clarithromycin, diclofenac, diphenhydramine, ibuprofen, mefenamic acid and roxithromycin) were measured in water samples collected from the streams near a pharmaceutical manufacturing complex. A predicted no-effect concentration (PNEC) was derived using either the assessment factor method or species sensitivity distribution method. In addition, a hazard quotient for each pharmaceutical was calculated by dividing its measured environmental concentration by its PNEC. Results: Samples collected downstream from the wastewater treatment plant (WWTP) had higher concentrations of pharmaceuticals than those collected from the reference site (upstream). Moreover, pharmaceutical concentrations were greater in ambient water than in the final effluent from the WWTP, which suggested that non-point sources were contributing to the contamination of the ambient water environment. Some of the target pharmaceuticals exhibited a hazard quotient >1, indicating that their potential ecological effects on the aquatic environment near the pharmaceutical industrial area should not be ignored. Conclusion: This study demonstrated that the pharmaceutical manufacturing area was contaminated with residual drugs, and that there was a possible non-point source near the WWTP effluent discharge area. The results of this study will aid in the development of management plans for pharmaceuticals, particularly in hotspots such as pharmaceutical industrial sites and their vicinities.

Quality Characteristics of Muffins containing Beet Powder (비트 가루 첨가량에 따른 머핀의 품질특성)

  • Seo, Eun-Ok;Ko, Seng-Hye
    • Culinary science and hospitality research
    • /
    • v.20 no.1
    • /
    • pp.27-37
    • /
    • 2014
  • This study examines the quality characteristics of the muffins made by adding 3%, 6%, and 9% of beet powder, comparing with the reference group. The result showed that there has been no significant difference in the ash content from the groups added with 3% and 9% of beet powder. The height of muffins appeared to be 4.7~5.0 cm, which didn't show any significant difference among the samples. The volume of beet muffins has shown significant difference among the samples (p<0.001). From the measurement result by scanning electron microscope (SEM), the samples had thick cellular walls and coarse pores because there was less gluten content with increased beet powder. From the chromaticity measurement result, L value and b-value decreased, while a-value increased with increased beet powder. From the texture measurement result, hardness increased with increased beet powder. Adhesiveness appeared to be getting lower with increased beet powder. Also, there was significant difference among the samples for cohesiveness (p<0.001). Gumminess got higher in the samples added with 3% and 6% of beet powder, and the highest chewiness was shown in the sample group added with 3% of beet powder. From the sensory evaluation result, overall acceptance has appeared in order of 6% > 9% > 3% > 0%.

Preliminary Checklist For Vertical Extension of Elevator in Apartment Buildings (공동주택의 엘리베이터 수직 확장 공사를 위한 사전 검토항목)

  • Park, Jin-Gu;Lee, Chan-Sik
    • Proceedings of the Korean Institute Of Construction Engineering and Management
    • /
    • 2008.11a
    • /
    • pp.813-816
    • /
    • 2008
  • The increasing number of vehicles owned by individuals in association with the rising income resulted in an acute shortage of parking spaces. We are not only seeing a serious traffic congestion arising from the vehicles parked in the streets adjacent to apartment buildings, but also the social issues of not being able to properly prepare for the emergency such as breakout of fires. Although remodeling of old apartment buildings are being discussed in measures to these problems, the research of parking space expansion is still insufficient. In a survey on remodeling of old apartment buildings, over 30 percent of those who answered cited the parking space as the most needed improvement and said they preferred direct entry as a way to expand parking space among lateral underground expansion methods. The direct entry is a method in which one directly enters the apartment house from the parking lot through the elevator and it requires extended operation of elevators. However, because there are no established systematic processes for elevator extension and works of such kinds are not common, elevator extension works are being done in an inefficient manner. In this research we reanalyzed the processes in order to present the items to be examined for more efficient elevator extension works, and through interviews of experts in the field, we produced the examination items by process from the perspectives of management and technology. This research will be used as a reference material for elevator extension works associated with expanding underground parking lot of apartment buildings.

  • PDF

Interlaminar Fracture Toughness of Hybrid Composites Inserted with Different Kinds of Non-Woven Tissues : Part I-Mode I (종류가 다른 부직포가 삽입된 하이브리드 복합재료의 층간파괴인성 : Part I-Mode I)

  • Jeong, Jong-Seol;Cheong, Seong-Kyun
    • Transactions of the Korean Society of Mechanical Engineers A
    • /
    • v.37 no.4
    • /
    • pp.497-502
    • /
    • 2013
  • In this study, the interlaminar fracture toughness in mode I of a hybrid composite inserted with different types of non-woven tissues was determined. The interlaminar fracture toughness in mode I is obtained by a double cantilever beam test. The experiment is performed using three types of non-woven tissues: 8 $g/m^2$ of carbon tissue, 10 $g/m^2$ of glass tissue, and 8 $g/m^2$ of polyester tissue. Considering a specimen with no non-woven tissue as a reference, the interlaminar fracture toughness in mode I of specimens inserted with non-woven carbon and glass tissues decreases by as much as 6.3% and 11.4%, respectively. However, the fracture toughness of a hybrid composite specimen inserted with non-woven polyester tissue increases by as much as 69.4%. It is considered that the specimen inserted with non-woven polyester tissue becomes cheaper, and lighter, and the value of the fracture toughness becomes much greater than that of the non-woven carbon tissue.