• 제목/요약/키워드: nano fiber

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Multiple effects of nano-silica on the pseudo-strain-hardening behavior of fiber-reinforced cementitious composites

  • Hossein Karimpour;Moosa Mazloom
    • Advances in nano research
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    • 제15권5호
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    • pp.467-484
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    • 2023
  • Despite the significant features of fiber-reinforced cementitious composites (FRCCs), including better mechanical, fractural, and durability performance, their high content of cement has restricted their use in the construction industry. Although ground granulated blast furnace slag (GGBFS) is considered the main supplementary cementitious material, its slow pozzolanic reaction stands against its application. The addition of nano-sized mineral modifiers, including nano-silica (NS), is an alternative to address the drawbacks of using GGBFS. The main object of this empirical and numerical research is to examine the effect of NS on the strain-hardening behavior of cementitious composites; ten mixes were designed, and five levels of NS were considered. This study proposes a new method, using a four-point bending test to assess the use of nano-silica (NS) on the flexural behavior, first cracking strength, fracture energy, and micromechanical parameters including interfacial friction bond strength and maximum bridging stress. Digital image correlation (DIC) was used for monitoring the initiation and propagation of the cracks. In addition, to attain a deep comprehension of fiber/matrix interaction, scanning electron microscope (SEM) analysis was used. It was discovered that using nano-silica (NS) in cementitious materials results in an enhancement in the matrix toughness, which prevents multiple cracking and, therefore, strain-hardening. In addition, adding NS enhanced the interfacial transition zone between matrix and fiber, leading to a higher interfacial friction bond strength, which helps multiple cracking in the composite due to the hydrophobic nature of polypropylene (PP) fibers. The findings of this research provide insight into finding the optimum percent of NS in which both ductility and high tensile strength of the composites would be satisfied. As a concluding remark, a new criterion is proposed, showing that the optimum value of nano-silica is 2%. The findings and proposed method of this study can facilitate the design and utilization of green cementitious composites in structures.

광소자 정렬용 극초정밀 다축 위치 제어장치 개발 (Development of Multi-axis Nano Positioning Stage for Optical Alignment)

  • 정상화;이경형;차경래;김현욱;최석봉;김광호;박준호
    • 한국정밀공학회:학술대회논문집
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    • 한국정밀공학회 2004년도 추계학술대회 논문집
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    • pp.304-307
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    • 2004
  • As optical fiber communication grows, the fiber alignment become the focus of industrial attention. This greatly influence the overall production rates for the opto-electric products. We proposed multi-axis nano positioning stage for optical fiber alignment. This device has 3 DOF translation and sub nanometer resolution. This nano stage consist of 3 PZT-driven flexure stages which are stacked parallel. The displacement of it is measured with capacitance gauge and is controlled by computer-embedded main controller. The design process of flexure stage using FEM is proposed and the performance evaluation of this system is verified with experiments.

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광섬유 국소화 표면 플라즈몬 공명 센서를 위한 광섬유 표면상의 금 나노 입자 특성 분석 (Characterization of gold nanoparticles on optical fiber for localized surface plasmon resonance sensor)

  • 이훈;이승기
    • 센서학회지
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    • 제18권3호
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    • pp.226-233
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    • 2009
  • In this study, the optical properties of localized surface plasmon resonance sensor using optical fiber was analyzed as the variation of a size and surface density of gold nano particles on the etched optical fiber surface. It is shown that a size and surface density of gold nano particles on optical fiber surface are controlled by $Na_3$ citrate quantity and pH of gold colloid solution. To measure the sensitivity, peak wavelength of absorbance spectrum was detected as the reflective index of the solution. The sensor sensitivity is linearly dependent on the size and surface densities of gold nano particles from the results of optical experiments.

Advances in liquid crystalline nano-carbon materials: preparation of nano-carbon based lyotropic liquid crystal and their fabrication of nano-carbon fibers with liquid crystalline spinning

  • Choi, Yong-Mun;Jung, Jin;Hwang, Jun Yeon;Kim, Seung Min;Jeong, Hyeonsu;Ku, Bon-Cheol;Goh, Munju
    • Carbon letters
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    • 제16권4호
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    • pp.223-232
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    • 2015
  • This review presents current progress in the preparation methods of liquid crystalline nano-carbon materials and the liquid crystalline spinning method for producing nano-carbon fibers. In particular, we focus on the fabrication of liquid crystalline carbon nanotubes by spinning from superacids, and the continuous production of macroscopic fiber from liquid crystalline graphene oxide.

Preparation of Nano Disperse Dyes from Nanoemulsions and Their Dyeing Properties on Ultramicrofiber Polyester

  • Choi Jae-Hong;Kang Min-Ju
    • Fibers and Polymers
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    • 제7권2호
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    • pp.169-173
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    • 2006
  • Six nano disperse dyes were prepared using corresponding O/W nanoemulsions which were obtained with sodium laurylsulphate and caprylic triglyceride. The average particle size of the dyes prepared were in the range of $110{\sim}130nm$. Exhaust dyeing using nano dyes resulted in low exhaustion yields of $17{\sim}26%$ on regular polyester fiber and $28{\sim}38%$ on ultramicrofiber polyester. The observed low exhaustion yields of nano disperse dye can be explained by the solubilization of dye particles into surfactant micelles as well as the high stability of the nanoemulsions, these might reduce the capacity of dye uptake onto the fibers. However, higher K/S values of dyeings with nano dyes on ultramicrofiber sites compared to those on regular polyester sites suggested their potential to be more efficient dyes for finer denier microfiber polyesters.

Strength Increase of Medium Temperature-carbonized PAN Nano Fibers Made by Mechano-electrospinning

  • Kim, J.H.;Bajaj, B.;Yoon, S.J.;Kim, S.H.;Lee, J.R.
    • Composites Research
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    • 제26권3호
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    • pp.160-164
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    • 2013
  • In this study, the effect of phosphoric acid (PA) as a fiber spinning aid on the strength increase of polyacrylonitrile (PAN) nano-fibers by using modified mechano-electrospinning technologies has been analyzed. The medium carbonization temperature of $800^{\circ}C$ has been selected for the future economic production of these new materials. The concentration of PAN in dimethyl sulfoxide (DMSO) was fixed as 5 wt%. The weight fraction of PA was selected as being 2%, 4%, 6%, and 8% in comparison to PAN. These solutions have been used to make the nanofibers. The mechano-electrospinning apparatus installed in KRICT was made by our own design. By using this apparatus the continous and highly aligned precursor nano-fibers have been obtained. The bundle of 50 well aligned nano diameter continuous fibers with the diametr of 10 microns with 6 wt% phosphoric acid for addition showed maximum mechanical properties of 1.6 GPa as tensile strength and 300 GPa as Young's modulus. The weight of final product can be increased 19%, which can improve the economical benefits for the application of these new materials.

나노입자 코팅 탄소섬유 강화 복합재료의 전기전도도 향상 (Improvement of Electrical Conductivity of Carbon-Fiber Reinforced Plastics by Nano-particles Coating)

  • 서성욱;하만석;권오양;최흥섭
    • Composites Research
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    • 제23권6호
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    • pp.1-6
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    • 2010
  • 복합재 항공기 동체의 낙뢰손상방지를 목적으로 탄소섬듐-주석 산화물(ITO) 나노입자를 코팅함으로써 탄소섬유강화플라스틱(CFRP) 복합재료의 전기전도도를 향상하였다. 탄소섬유에 코팅된 ITO 나노입자는 10~40%의 농도로 콜로이드 상태에서 분사되었다. CFRP의 전기전도도는 코팅 후 3배 이상 증가하였으며 현재 B-787 복합재 항공기 동체에 사용 중인 기술인 금속메쉬를 CFRP 외층에 매몰한 경우보다도 높은 전기전도도를 얻을 수 있었으며, 나노입자 코팅으로 섬유-기지 계면에 미지는 악영향은 발견되지 않았다. 모의 낙뢰에 의한 손상영역은 각각 다른 처리를 한 재료와 조건에 따라 초음파 C-scan 이미지로 확인하였다. ITO 40% 코팅 시편의 경우 전기전도도는 B-787 샘플의 경우보다 높았지만 낙뢰에 의한 손상영역의 크기는 거의 비슷한 수준이었다.

폴리카보실란으로부터 제조된 탄화규소 중공사의 미세구조제어 (Nano-Structure Control of SiC Hollow Fiber Prepared from Polycarbosilane)

  • 신동근;공은배;조광연;권우택;김영희;김수룡;홍준성;류도형
    • 한국세라믹학회지
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    • 제50권4호
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    • pp.301-307
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    • 2013
  • SiC hollow fiber was fabricated by curing, dissolution and sintering of Al-PCS fiber, which was melt spun the polyaluminocarbosilane. Al-PCS fiber was thermally oxidized and dissolved in toluene to remove the unoxidized area, the core of the cured fiber. The wall thickness ($t_{wall}$) of Al-PCS fiber was monotonically increased with an increasing oxidation curing time. The Al-PCS hollow fiber was heat-treated at the temperature between 1200 and $2000^{\circ}C$ to make a SiC hollow fibers having porous structure on the fiber wall. The pore size of the fiber wall was increased with the sintering temperature due to the decomposition of the amorphous $SiC_xO_y$ matrix and the growth of ${\beta}$-SiC in the matrix. At $1400^{\circ}C$, a nano porous wall with a high specific surface area was obtained. However, nano pores grew with the grain growth after the thermal decomposition of the amorphous matrix. This type of SiC hollow fibers are expected to be used as a substrate for a gas separation membrane.