• Title/Summary/Keyword: mixture process

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Development of the Real-time Concentration Measurement Method for Evaporating Binary Mixture Droplet using Surface Plasmon Resonance Imaging (표면플라즈몬공명 가시화 장치를 이용한 증발하는 이종혼합물 액적의 실시간 농도 가시화 기법 개발)

  • Jeong, Chan Ho;Lee, Hyung Ju;Choi, Chang Kyoung;Lee, Hyoungsoon;Lee, Seong Hyuk
    • Journal of ILASS-Korea
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    • v.26 no.4
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    • pp.212-218
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    • 2021
  • The present study aims to develop the Surface Plasmon Resonance (SPR) imaging system facilitating the real-time measurement of the concentration of evaporating binary mixture droplet (BMD). We introduce the theoretical background of the SPR imaging technique and its methodology for concentration measurement. The SPR imaging system established in the present study consists of a LED light source, a polarizer, a lens, and a band pass filter for the collimated light of a 589 nm wavelength, and a CCD camera. Based on the Fresnel multiple-layer reflection theory, SPR imaging can capture the change of refractive index of evaporating BMD. For example, the present study exhibits the visualization process of ethylene glycol (EG)-water (W) BMD and measures real-time concentration change. Since the water component is more volatile than the ethylene glycol component, the refractive index of EG-W BMD varies with its mixture composition during BMD evaporation. We successfully measured the ethylene glycol concentration within the evaporating BMD by using SPR imaging.

Variation of Nutritional and Antioxidant Characteristics of Extract of Lycium barbarum produced by using Different Extraction Processes

  • Ho-Jong You
    • Journal of the Korean Applied Science and Technology
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    • v.41 no.2
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    • pp.520-529
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    • 2024
  • Lycium barbarum extract has a high potential to be developed as a health functional food due to the various health-promoting effects of Lycium barbarum. This study analyzed changes in nutritional and functional components depending on the extraction solvent (purified water and a mixture of purified water and alcohol) and the condition of the sample. The nutritional components (carbohydrates, protein, fat, ash), organic acids, amino acids, total phenolic compounds, and total flavonoids of the extract produced during the extraction process were analyzed. The nutritional composition and functional substances of the extracts showed some differences depending on the type of solvent and the condition of the sample. The amounts of crude protein (7.61%), crude fat (1.63%), carbohydrate (90.22%), and ash (0.54%) of dried Lycium barbarum extract using purified water as a solvent were similar to those of the powder sample extract. The highest content of citric acid was 4.31 mg/mL, similar to the case of acetic acid, when the powder sample used a mixture of purified water and alcohol as a solvent. The highest amino acid content was 357.39 mg/mL when the powder sample was mixed with purified water and alcohol as a solvent. The total amount of phenolic compounds was 686.16 g/L when the powder sample was extracted with a mixture of purified water and alcohol as a solvent. The highest total flavonoid content was 111.32 g/L when the powder sample was extracted with a mixture of purified water and alcohol as a solvent.

Kimchi Preparation with Brined Chinese Cabbage and Seasoning Mixture Stored Separately (분리 저장한 절임배추와 김치속을 이용한 김치의 제조)

  • Park, Wan-Soo;Lee, In-Seon;Han, Young-Sook;Koo, Young-Jo
    • Korean Journal of Food Science and Technology
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    • v.26 no.3
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    • pp.231-238
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    • 1994
  • The brined Chinese cabbages and kimchi seasoning mixture were separately stored and used for preparation of kimchi and the alternative method of conventional kimchi-manufacturing process was investigated. Chinese cabbages brined with 3% and 7% salt contents were stored at $0^{\circ}C$ and $10^{\circ}C$, and kimchi seasoning mixture without salt was stored at $4^{\circ}C$ and $10^{\circ}C$. The changes in pH and total acid of the cabbages were significantly slowly for the brined cabbage of 7% salt and storage at $0^{\circ}C$. Microbial growth including lactic acid bacteria were also increased slowly at $0^{\circ}C$. But, pH and total acid content of the kimchi seasoning mixture were not changed significantly at both temperatures during storage. Sensory evaluation on the kimchi samples showed that the modified method of kimchi preparation with separately stored seasoning mixture and brined cabbages is useful industrially or at home.

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Effect of Cobalt Oxide on Carbothermal Reduction of Spray Dried Titanium-Cobalt-Oxygen Based Oxide Powder (분무건조법에 의해 제조된 Ti-Co-O계 산화물 분말의 환원/침탄반응에 미치는 코발트 산화물의 영향)

  • Lee, Gil-Geun;Kim, Chan-Young
    • Journal of Powder Materials
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    • v.12 no.5 s.52
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    • pp.336-344
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    • 2005
  • In the present study, the focus is on the effect of cobalt oxide powder in the carbothermal reduction of the titanium-cobalt-oxygen based oxide powder by solid carbon for the optimizing synthesis process of ultra fine TiC/Co composite powder. The titanium-cobalt-oxygen based oxide powder was prepared by the combination of the spray drying and desalting processes using the titanium dioxide powder and cobalt nitrate as the raw materials. The titanium-cobalt-oxygen based oxide powder was mixed with carbon black, and then this mixture was carbothermally reduced under flowing argon atmosphere. Changes in the phase structure and thermal gravity of the mixture during carbothermal reduction were analysed using XRD and TGA. Titanium-cobalt-oxygen based oxide powder desalted at $600^{\circ}C$ had a mixture of $TiO_2\;and\;Co_{3}O_4$. And the one desalted at $800^{\circ}C$ had a mixture of $TiO_2\;and\;CoTiO_3$. In the case of the former powder, the reduction of cobalt oxide powder in the titanium-cobalt-oxygen based oxide powder occurred at lower temperature than the latter one. However, the carbothermal reduction of titanium dioxide powder in the titanium-cobalt-oxygen based oxide powder with a mixture of $TiO_2\;and\;Co_{3}O_4$ occurred at higher temperature than the one with a mixture of $TiO_2\;and\;CoTiO_3$. And also, the former powder showed a lower TiC formation ability than the latter one.

Effects on fermentation of Corn-Broiler Excreta Silage by Addition of Corn-Meal (옥수수-계분 silage 제조시 옥수수 곡분 첨가가 silage발효에 미치는 영향)

  • 고영두;김재황;김두환;임용기
    • Journal of The Korean Society of Grassland and Forage Science
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    • v.10 no.3
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    • pp.172-178
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    • 1990
  • This experiment was conducted to enhance nutritional value of whole crop corn silage and increase mixture levels of broiler excreta by adding of corn meal. Treatments were included non mixture(control), adding 10, 20, 30% of broiler excreta and adding 10, 20, 30% of broiler excreta and corn meal as a fresh matter basis, respectively. One liter laboratory silos were prepared. The characteristics of fermentation and micro-organisms during the silage process were assessed. The results obtained are summarized as follows: 1. The crude fiber, NDF and ADF contents were high in whole crop corn(P(O.Ol), crude protein and crude ash contents were high in the broiler excreta(P<0.05), and NFE content was high in corn meal (P< 0.05). 2. Crude protein content of silage was increased(I'$NH_3$-N contents of silage were markedly increased with increasing levels of broiler excreta and corn meal, and was the highest in the 30% broiler excreta treatment(P$meal$ <0.05), and Flieg's value gains "very good" by showing organic acids. 5. Numbers of total bacteria and lactobacilli were $10^5$ to $10^7$ and $10^5$ to $10^6$ , respectively, and were similar in all treatment. Colliform was all but annihilated in the treatment with mixture of broiler excreta and corn rneal.orn rneal.

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Autoignition Characteristics of Limonene - Expanded Polystyrene Mixture (Limonene - Expanded Polystyrene 혼합물의 자연발화 특성)

  • 송영호;하동명;정국삼
    • Fire Science and Engineering
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    • v.18 no.1
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    • pp.1-6
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    • 2004
  • In the reutilization process using limonene, the organic solvent to reduce volume of EPS, the AIT was measured with the variation of concentration and volume of mixture, in order to present the fund-mental data on the fire hazard assessment of limonene - EPS mixture at storage and handling. And ignition zone was compared with non-ignition zone. The equation related to AIT, activation energy and ignition delay time, used by the most scientific basis for predicting AIT values, was suggested using linear regression analysis as ln t = 0.704/T-5.819. And the equation related to concentration of mixture and AIT was also suggested to predict ignition hazard of combustible mixture using nonlinear regression analysis as $T_m/=248.32+69.27X+172.60X^2$. It enabled to predict ignition temperature according to variation of ignition delay time and concentration of mixture by the suggested equations.

Combustion Enhancemen of Premixed Mixtures Using Laser-Induced Cavity Ignition (레이저 유도 공동 점화방식을 이용한 예혼합기 연소 특성 향상)

  • 모하메드하산;고영성;정석호
    • Transactions of the Korean Society of Automotive Engineers
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    • v.7 no.6
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    • pp.8-16
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    • 1999
  • In this study, a new type of laser-induced ignition using a conical cavity has been developed to utilize all the available incident laser energy. In the method, it is possibile to ignite combustible methane/air mixtures by directing a laser beam of a constant small diameter into a small conical cavity, without focusing the laser beam. Shadow graphs for the early stage of combustion process show that a hot gas jet is ejected from the cavity, especially with lean mixture. After a very show time, the hot gas jet finishes issuing and the flame behavior is quite similar to flame propagation initiated by a conventional spark ignition. The combustion process using the new method exhibits more rapid pressure increase and a higher maximum pressure rise than that of the center ignition using laser-induced spark, with significant decrease in the combustion time. Also, the new ignition method is numerically modeled to simulate the flame kernel development and subsequent combustion process using the KIVA-IIcode. The calculated results show satisfactory agreement with experimental results.

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Thermodynamic Correlations for Predicting the Properties of Coal-Tar Fractions and Process Analysys (석탄 유분에 대한 물성예측식 개발 및 공정에 대한 연구)

  • Oh, Jun Sung;Lee, Euy Soo;Park, Sang Jin
    • Korean Chemical Engineering Research
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    • v.43 no.4
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    • pp.458-466
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    • 2005
  • Full-scale utilizations of batch separation process often require knowledge about thermodynamics and correlation techniques of physical properties of complex mixture consisting of a great number of many unknown components. Various empirical correlations have been proposed to predict the physical properties mostly about the pseudocomponent of petroleum. In this study, one parameter correlations are developed for the calculations of the critical physical properties and ideal heat capacity of the pseudo-component of coal tar fractions. Developed model can provide a tool for the design and operations for the batch distillation of coal tar mixture.

A Study on the Synthesis of Fe-Si Alloy by Mechanical Alloying (기계적(機械的) 합금화(合金化) 방법(方法)에 의한 Fe-Si 합금제조(合金製造)에 관(關)한 연구(硏究))

  • Jun, Hoon;Hwang, Sung-Min;Lee, Sung-Man
    • Journal of Industrial Technology
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    • v.19
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    • pp.107-113
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    • 1999
  • The microstructural evolution during mechanical alloying of elemental Fe and Si powders, average composition $Fe_{30}Si_{70}$ and $Fe_{50}Si_{50}$, has been investigated by X-ray diffraction (XRD), Scanning electron microscopy (SEM) and Differential scanning calorimetry (DSC). Mechanical alloying was performed by using a SPEX 8000 Mixer/Mill under argon atmosphere with/without hexane as a process control agent (PCA). In the presence of PCA, the milling process was dominated by fracture resulting in the decrease in particle size to about $1{\mu}m$. The structural development with milling time depended on the average composition of starting powders. The mixture of $Fe_{50}Si_{50}$ and $Fe_{30}Si_{70}$ resulted in the formation of FeSi(${\varepsilon}$ - phase) and $FeSi_2$(${\beta}$ - phase), respectively. In the case of $Fe_{33.3}Si_{66.7}$, a mixture and $FeSi_2({\beta})$ was formed. These results were discussed by considering the thermodynamics and kinetics concerning the milling process.

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A Study on Development Process of Evaporating Diesel Spray (증발디젤분무의 발달 과정에 관한 연구)

  • Yeom, Jeong-Kuk;Park, Jong-Sang;Chung, Sung-Sik;Ha, Jong-Yul;Kim, Si-Pom
    • Transactions of the Korean Society of Automotive Engineers
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    • v.15 no.3
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    • pp.141-146
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    • 2007
  • In this study, the effects of change in ambient gas viscosity on spray structure have been investigated in the high temperature and pressure field. To analyze the structure of evaporative diesel spray is important in speculation of mixture formation process. Emissions of diesel engines can be reduced by the control of the mixture formation process. Therefore, this study examines the evaporating spray structure in the constant volume chamber. The viscosity of ambient gas was selected as the experimental parameter, is changed from 21.7 mPa s to 32.1 mPa s by changing in ambient gas temperature. In order to obtain images of the liquid and vapor-phase of injected spray, exciplex fluorescence method was used in this study. The liquid and vapor-phase images were taken with 35mm still camera and CCD camera, respectively. Consequentially, it could be confirmed that the distribution of vapor concentration is more uniform in the case of the ambient gas with high viscosity than in that of the ambient gas with low viscosity.