• Title/Summary/Keyword: mixture densities

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Tensile Strength Variation of Binary Tablets Produced by Planetary Ball Milling (유성볼밀링으로 제조한 2성분 정제의 인장강도 변화)

  • Sim, Chol-Ho
    • Journal of Pharmaceutical Investigation
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    • v.38 no.1
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    • pp.1-8
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    • 2008
  • Planetary ball mill was used to decrease and control the particle size of excipients. The effects of the weight of sample and the revolution number of mill, and grinding time on the particle size of the ground sample were analyzed by response surface methodology. The optimum conditions for the milling of microcrystalline cellulose were 38.82 g of the weight of sample and 259 rpm of the revolution number of mill, and 45 minutes of grinding time. The predicted value of the particle size at the these conditions was $19.02{\mu}m$, of which the experimental value at the similar conditions was $18.68{\mu}m$. The tensile strength of tablets of single-component powders, such as microcrystalline cellulose, hydroxypropylmethyl cellulose and starch, binary mixtures and ground binary mixtures of these powder were measured at various relative densities. It was found that the logarithm of the tensile strength of the tablets was proportional to the relative density. A simple model, based upon Ryshkewitch-Duckworth equation that was originally proposed for porous materials, has been developed in order to predict the relationship between the tensile strength and relative density of ground binary tablets based on the properties of the constituent single-component powders. The validity of the model has been verified with experimental results for ground binary mixtures. It has demonstrated that this model can well predict the tensile strength of ground binary mixtures based upon the properties of single-component powders, such as true density, and the compositions. When the tensile strength of the mixture of microcrystalline cellulose hydroxypropylmethyl cellulose (90:10) and the ground mixture of them were compared, the tensile strength of the ground mixture decreased widely from 45.3 to 5.6% compared to the mixture in case the relative density of tablets was in the range of $0.7{\sim}0.9$. When the tensile strength of the mixture of microcrystalline cellulose starch (80:20) and the ground mixture of them were compared, the tensile strength of the ground mixture decreased widely from 31.0 to 11.6% compared to the mixture in case the relative density of tablets was in the range of $0.7{\sim}0.9$.

Colloidal Crystallization in Microgravity

  • Okubo, Tsuneo
    • Proceedings of the Korean Fiber Society Conference
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    • 2003.10a
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    • pp.5-6
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    • 2003
  • Kinetic study on the colloidal crystallization of single component and mixture of different sizes or densities of spheres was made in the exhaustively deionized suspensions and in microgravity, and compared with the results in normal gravity. Colloidal crystallization rates were retarded in microgravity for single component of spheres, whereas rates of alloy crystallization were enhanced substantially in microgravity. The rotational diffusion coefficients of colloids and the formation reaction rates of colloidal silica spheres were also studied in microgravity.

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A Penalized Likelihood Method for Model Complexity

  • Ahn, Sung M.
    • Communications for Statistical Applications and Methods
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    • v.8 no.1
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    • pp.173-184
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    • 2001
  • We present an algorithm for the complexity reduction of a general Gaussian mixture model by using a penalized likelihood method. One of our important assumptions is that we begin with an overfitted model in terms of the number of components. So our main goal is to eliminate redundant components in the overfitted model. As shown in the section of simulation results, the algorithm works well with the selected densities.

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Stability of Unsaturated Soil Slopes considering the Effect of Wetting Front Suction Loss

  • Jeong, Sang-Seom;Kim, Jae-Young
    • Proceedings of the Korean Geotechical Society Conference
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    • 2007.09a
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    • pp.502-513
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    • 2007
  • This paper describes the rainfall-induced slope failures caused by infiltration due to prolonged rainfall. The emphasis was on quantifying the effect of fine-grained contents which are influencing on the infiltration rate in the wetting front of initially unsaturated slopes during rainfall. Suction tests by tensiometer were performed for five mixture specimens with varying fine-grained contents and then, numerical analyses for the stability of unsaturated slopes are carried out for different relative densities and mixture portions based on the soil water characteristic curves obtained by GCTS pressure plate. It is shown that the fines are highly influenced on wetting front suction of unsaturated soil slopes. Based on the results, it is found that until 15% fine content is the limit showing different wetting front suction, beyond which the wetting band depth do not affect considerably the stability of unsaturated slopes.

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Experimental Study on Characteristics of Synergistic Effect of Fuel Mixing on Number Density and Size of Soot in Ethylene-base Counterflow Diffusion Flames by Laser Techniques

  • Choi, Jae-Hyuk
    • Journal of Advanced Marine Engineering and Technology
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    • v.33 no.3
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    • pp.378-386
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    • 2009
  • The effect of fuel mixing on soot structure with methane, ethane, and propane to ethylene-base counterflow diffusion flames has been investigated by measuring the volume fraction, number density, and particle size of soot by adopting the light extinction/scattering techniques. The experimental result showed that the mixing of ethane and propane in ethylene diffusion flame increased soot volume fraction while the mixing of methane decreased. As compare to the ethylene-base flame, the diameters of soot particles for mixture flames are slightly smaller. While the soot number densities for the mixture flames are much higher. Thus, the increase in the soot volume fraction can be attributed to the appreciably increased soot number density by the fuel mixing.

Holographic Polymer-Dispersed Liquid Crystals and Polymeric Photonic Crystals Formed by Holographic Photolithography

  • Kyu Thein;Meng Scott;Duran Hatice;Nanjundiah Kumar;Yandek Gregory R.
    • Macromolecular Research
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    • v.14 no.2
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    • pp.155-165
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    • 2006
  • The present article describes the experimental and theoretical observations on the formation of holographic, polymer-dispersed, liquid crystals and electrically switchable, photonic crystals. A phase diagram of the starting mixture of nematic liquid crystal and photo-reactive triacrylate monomer was established by means of differential scanning calorimetry (DSC) and cloud point measurement. Photolithographic patterns were imprinted on the starting mixture of LC/triacrylate via multi-beam interference. A similar study was extended to a dendrimer/photocurative mixture as well as to a single component system (tetra-acrylate). Theoretical modeling and numerical simulation were carried out based on the combination of Flory-Huggins free energy of mixing and Maier-Saupe free energy of nematic ordering. The combined free energy densities were incorporated into the time-dependent Ginzburg-Landau (Model C) equations coupled with the photopolymerization rate equation to elucidate the spatio-temporal structure growth. The 2-D photonic structures thus simulated were consistent with the experimental observations. Furthermore, 3-D simulation was performed to guide the fabrication of assorted photonic crystals under various beam-geometries. Electro-optical performance such as diffraction efficiency was evaluated during the pattern photopolymerization process and also as a function of driving voltage.

An Elliptical Basis Function Network for Classification of Remote-Sensing Images

  • Luo, Jian-Cheng;Chen, Qiu-Xiao;Zheng, Jiang;Leung, Yee;Ma, Jiang-Hong
    • Proceedings of the KSRS Conference
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    • 2003.11a
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    • pp.1326-1328
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    • 2003
  • An elliptical basis function (EBF) network is proposed in this study for the classification of remotely sensed images. Though similar in structure, the EBF network differs from the well-known radial basis function (RBF) network by incorporating full covariance matrices and uses the expectation-maximization (EM) algorithm to estimate the basis functions. Since remotely sensed data often take on mixture -density distributions in the feature space, the proposed network not only possesses the advantage of the RBF mechanism but also utilizes the EM algorithm to compute the maximum likelihood estimates of the mean vectors and covariance matrices of a Gaussian mixture distribution in the training phase. Experimental results show that the EM-based EBF network is faster in training, more accurate, and simpler in structure.

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Preparation of Proton-Conducting Gd-Doped Barium Cerate by Oxalate Coprecipitation Method

  • Yong Sung Choi;Soo Man Sim
    • The Korean Journal of Ceramics
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    • v.4 no.3
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    • pp.213-221
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    • 1998
  • $BaCe_{0.9}Gd_{0.1_O_{2.95}$ powder was synthesized by oxalate coprecipitation method. Precipitate with a stoichimetric ratio of the cations was prepared by adding a mixture of Ba, Ce and Gd nitrate solution to an oxalic acid solution at pH 4. Reaction between the constituent oxides to form a perovskite phase was initiated at $800^{\circ}C$ and a single phase $BaCe_{0.9}Gd_{0.1_O_{2.95}$ powder having good sinterability was obtained after calcination at $1000^{\circ}C$. Sintering green compacts of this powder for 6 h showed a considerable densification to start at $1100^{\circ}C$ and resulted in 93% and 97% relative densities at $1300^{\circ}$ and at $1450^{\circ}C$, respectively. Whereas the power compacts prepared by solid state reaction had lower relative densities, 78% at $1300^{\circ}$and 90% at $1450^{\circ}C$. Fine particles of $CeO_2$ second phase were observed in the surface of the sintered compacts. This was attributed to the evaporation of BaO from the surface that had been exposed during thermal etching.

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A Study on SiC Buffer Layer Prepared by Ultra High Vacuum Electron Cyclotron Resonance CVD (초고진공 전자공명 플라즈마를 이용한 SiC buffer layer 형성에 관한 연구)

  • Joen, Woo-Gon;Pyo, Jae-Hwak;Whang, Ki-Woong
    • Proceedings of the KIEE Conference
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    • 1995.11a
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    • pp.326-328
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    • 1995
  • SiC buffer layers were grown on Si(100) substrates by ultra-high-vacuum electron cryclotron resonance plasma (UHV ECR plasma) from $CH_4/H_2$ mixture at 700$^{\circ}C$. The electron densities and temperature were measured by single probe. The axial plasma potentials measured by emissive probe had the double layer structure at positive substrate bias. Piranha cleaning was carried out as ex-situ wet cleaning. Clean and smooth silicon surface were prepared by in-situ hydrogen plasma cleaning at 540$^{\circ}C$. A short exposure to hydrogen plasma transforms the Si surface from 1$\times$1 to 2$\times$1 reconstruction. It was monitored by reflection high energy electron diffraction (RHEED). The defect densities were analysed by the dilute Schimmel etching. The results showed that the substrate bias is important factor in hydrogen plasma cleaning. The low base pressure ($5\times10^{-10}$ torr) restrains the $SiO_2$ growth on silicon surface. The grown layers showed different characteristics at various substrate bias. RHEED and K-ray Photoelectron spectroscopy study showed that grown layer was SiC.

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Effect of relative density on the shear behaviour of granulated coal ash

  • Yoshimoto, Norimasa;Wu, Yang;Hyodo, Masayuki;Nakata, Yukio
    • Geomechanics and Engineering
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    • v.10 no.2
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    • pp.207-224
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    • 2016
  • Granulated coal ash (GCA), a mixture of the by-product from milling processes with a small amount of cement added, has recently come to be used as a new form of geomaterial. The shear strength and deformation behaviours of GCA are greatly determined by its relative density or void ratio. A series of drained triaxial compression tests were performed on cylindrical specimens of GCA at confining pressures of between 50 kPa and 400 kPa at initial relative densities of 50%, 70% and 80%. Experimental results show that a rise in relative density increases the peak shear strength and intensifies the dilation behaviour. The initial tangent modulus and secant modulus of the stress-strain curve increase with increasing initial relative density, whereas the axial and volumetric strains at failure decrease with level of initial relative density. The stress-dilatancy relationships of GCA at different relative densities and confining pressures display similar tendency. The dilatancy behaviour of GCA is modelled by the Nova rule and the material property N in Nova rule of GCA is much larger than that of natural sand.